Preparative enantioseparation on polysaccharide phase using microporous silica as a support

Chirality

Volumn 10, Issue 7, 1998, Pages 573-577

  Tiritan, Maria E ^a   Cass, Quezia B ^a   Del Alamo, Aurora ^b   Matlin, Stephen A ^b   Grieb, Sally J ^b  

^a FEDERAL UNIVERSITY OF SÃO CARLOS   (Brazil)

^b UNIVERSITY OF WARWICK   (United Kingdom)

Author keywords

Carbohydrate carbamate; Chiral preparative; Hexahelicene; Silica; Sulphoxides

Indexed keywords

AMYLOSE; CARBAMIC ACID DERIVATIVE; CELLULOSE; HEXAHELICEN 7 YL ACETIC ACID METHYL ESTER; POLYCYCLIC AROMATIC COMPOUND; POLYSACCHARIDE; SILICON DIOXIDE; SULFOXIDE; UNCLASSIFIED DRUG;

CHIRAL CHROMATOGRAPHY; CONFERENCE PAPER; DRUG PURITY; ENANTIOMER; PRIORITY JOURNAL; STEREOCHEMISTRY;

EID: 0031657678     PISSN: 08990042     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1520-636X(1998)10:7<573::AID-CHIR4>3.0.CO;2-3     Document Type: Conference Paper

References (17)

1. Subramanian, G. A Practical Approach to Chiral Separation by Liquid Chromatography, 1st ed. Weiheim: VHC, 1994.
2. Francotte, E. Contribution of preparative chromatographic resolution to the investigation of chiral phenomena. J. Chromatogr. 666:564-601, 1994.
3. Hurt, A.J., Tan, S.C. Drug chirality and its clinical significance. Drugs 52(Suppl. 5):1-12, 1996.
4. Taylor, D.T., Maher, K. Chiral separation by high-performance liquid chromatography. J. Chromatogr. Sci. 5:67-85, 1992.
5. Okamoto, Y., Kaida, Y. Resolution by high-performance liquid chromatography using polysaccharide carbamate and benzoate as chiral stationary phases. J. Chromatogr. A 666:403-419, 1994.
6. Matlin, S.A., Tiritan, M.E., Crawford, A.J., Cass, Q.B., Boyd, D.R. HPLC with carbohydrate carbamate chiral phase: influence of chiral phase structure on enantioselectivity. Chirality 6:135-140, 1994.
7. Matlin, S.A., Tiritan, M.E., Cass, Q.B., Boyd, D.R. Enantiomeric resolution of chiral sulfoxides on polysaccharide phases by HPLC. Chirality 8:147-152, 1996.
8. Cass, Q.B., Degani, A.L.G., Tiritan, M.E., Matlin. S.A. Curran, D.P., Balog, A. Enantiomeric resolution by HPLC of axial chiral amides using amylose tris [(S)-1-phenylethylcarbamate]. Chirality 9:109-112, 1997.
9. Okamoto, Y., Kaida, Y. Optical resolution by high performance liquid chromatography (HPLC) using polysaccharide derivatives as chiral stationary phases. J. Synthet. Org. Chem. Jpn. 51:41-53, 1993.
10. Okamoto, Y., Kawashima, M., Hatada, K. Chromatographic resolution: XI. Controlled chiral recognition of cellulose trisphenylcarbamate derivatives supported on silica gel. J. Chromatogr. 363:173-186, 1986.
11. Dingenen, J., Kinkel, J.N. Preparative chromatographic resolution of racemates on chiral stationary phases on laboratory and production scales by closed-loop recycling chromatography. J. Chromatogr. A 666: 627-650, 1994.
12. Miller, L., Honda, D., Fronek, R., Howe, K. Examples of preparative chromatography on amylose-based chiral stationary phase in support of pharmaceutical research. J. Chromatogr. A 658:429-435, 1994.
13. Masurel, D., Wainer, I.W. Analytical and preparative high-performance liquid chromatographic separation of the enantiomers of isofosfamide, cyclophosphamide and trifosfamide and their determination in plasma. J. Chromatogr. 490:133-143, 1989.
14. Miller, L. Analytical and preparative resolution of enantiomers of verapamil and noverapamil using a cellulose-based chiral stationary phase in the reversed-phase mode. J. Chromatogr. 648:381-388, 1995.
15. Del Alamo, A. Studies of Hexalelicene Bonded Phases for the HPLC Resolution of Enantiomers. PhD Thesis, Chemistry Department, Warwick University, Warwick, UK, June, 1995.
16. Tiritan, M.E. Resolução Enantiomérica de Sulfóxidos Quirais por CLAE, em Carbamatos de Polissacarídeos. PhD Thesis, Departamento de Química, Universidade Federal de São Carlos, Brazil, March, 1996.
17. Porch, B. Some specific problems in the practice of preparative high-performance liquid chromatography. J. Chromatogr. A 658:179-194, 1994.