Synthesis, electrochemistry, structure, and magnetic susceptibility of 5-tert-butyl-1,3-bis-(1,2,3,5-dithiadiazolyl)benzene. Structural effect of the bulky substituent

Canadian Journal of Chemistry

Volumn 76, Issue 1, 1998, Pages 85-93

  Beekman, Richard A ^a   Boeré, René T ^a   Moock, Klaus H ^b   Parvez, Masood ^c  

^a UNIVERSITY OF LETHBRIDGE   (Canada)

^b AUSTRALIAN NATIONAL UNIVERSITY   (Australia)

^c UNIVERSITY OF CALGARY   (Canada)

Author keywords

Bulky substituent; Crystal structure; Diradical; Dithiadiazole; Magnetic susceptibility

Indexed keywords

ANTIFERROMAGNETISM; CRYSTAL SYMMETRY; DIAMAGNETISM; ELECTROCHEMISTRY; MAGNETIC PERMEABILITY; PARAMAGNETISM; SYNTHESIS (CHEMICAL);

CURIE WEISS LAW;

AROMATIC COMPOUNDS;

EID: 0031649179     PISSN: 00084042     EISSN: None     Source Type: Journal    
DOI: 10.1139/v97-213     Document Type: Article

References (35)

1. (a) R.T. Oakley. Can. J. Chem. 71, 1775 (1993);
2. (b) A.W. Cordes, R.C. Haddon, and R.T. Oakley. In The chemistry of inorganic ring systems. Edited by R. Steudel. Elsevier, Amsterdam. 1992. p. 295;
3. (c) A.J. Banister and J.M. Rawson. In The chemistry of inorganic ring systems. Edited by R. Steudel. Elsevier, Amsterdam. 1992. p. 323;
4. (d) J.M. Rawson, A.J. Banister, and I. Lavender. Adv. Heterocycl. Chem. 62, 137 (1995).
5. A. Vegas, A. Pérez-Salazar, A.J. Banister, and R.G. Hey. J. Chem. Soc. Dalton Trans. 1812 (1980).
6. A.W. Cordes, R.C. Haddon, and R.T. Oakley. Adv. Mater. 6, 798 (1994).
7. C.D. Bryan, A.W. Cordes, R.M. Fleming, N.A. George, S.H. Glarum, R.C. Haddon, C.D. MacKinnon, R.T. Oakley, T.T.M. Palstra, and A.S. Perel. J. Am. Chem. Soc. 117, 6880 (1995).
8. C.D. Bryan, A.W. Cordes, R.C. Haddon, R.G. Hicks, D.K. Kennepohl, C.D. MacKinnon, R.T. Oakley, T.T.M. Palstra, A.S. Perel, S.R. Scott, L.F. Schneemeyer, and J.V. Waszczak. J. Am. Chem. Soc. 116, 1205 (1994).
9. M.P. Andrews, A.W. Cordes, D.C. Douglass, R.M. Fleming, S.H. Glarum, R.C. Haddon, P. Marsh, R.T. Oakley, T.T.M. Palstra, L.F. Schneemeyer, G.W. Trucks, R. Tycko, J.V. Waszczak, K.M. Young, and N.M. Zimmerman. J. Am. Chem. Soc. 113, 3559 (1991).
10. A.W. Cordes, R.C. Haddon, R.T. Oakley, L.F. Schneemeyer, J.V. Waszczak, K.M. Young, and N.M. Zimmerman. J. Am. Chem. Soc. 113, 582 (1991).
11. C.D. Bryan, A.W. Cordes, J.D. Goddard, R.C Haddon, R.G. Hicks, C.D. MacKinnon, R.C. Mawhinney, R.T. Oakley, T.T.M. Palstra, and A.S. Perel. J. Am. Chem. Soc. 118, 330 (1996).
12. A.W. Cordes, R.C. Haddon, R.G. Hicks, D.K. Kennepohl, R.T. Oakley, T.T.M. Palstra, L.F. Schneemeyer, S.R. Scott, and J.V. Waszczak. Chem. Mater. 5, 820 (1993).
13. W.M. Davis, R.G. Hicks, R.T. Oakley, B. Zhao, and N.J. Taylor. Can. J. Chem. 71, 180 (1993).
14. A.W. Cordes, R.C. Haddon, R.G. Hicks, R.T. Oakley, and T.T.M. Palstra. Inorg. Chem. 31, 1802 (1992).
15. A.W. Cordes, R.C. Haddon, R.G. Hicks, D.K. Kennepohl, R.T. Oakley, L.F. Schneemeyer, and J.V. Waszczak. Inorg. Chem. 32, 1554 (1993).
16. A.J. Banister, N. Bricklebank, W. Clegg, M.R.J. Elsegood, C.I. Gregory, I. Lavender, J.M. Rawson, and B.K. Tanner. J. Chem. Soc. Chem. Commun. 679 (1995).
17. A.J. Banister, N. Bricklebank, I. Lavender, J.M. Rawson, C.I. Gregory, B.K. Tanner, W. Clegg, M.R.J. Elsegood, and F. Palacio. Angew. Chem. Int. Ed. Engl. 35, 2533 (1996).
18. R.T. Boeré and K.H. Moock. J. Am. Chem. Soc. 117, 4775 (1995).
19. M.A. McCall, J.R. Caldwell, H.G. Moore, and H.M. Beard. J. Macromol. Sci. Chem. A3, 911 (1969).
20. R.T. Boeré, R.G. Hicks, and R.T. Oakley. Inorg. Synth. 21, 94 (1997).
21. K.H. Moock and M.H. Rock. J. Chem. Soc. Dalton Trans. 2459 (1993).
22. R.T. Boeré, K.H. Moock, and M.Z. Parvez. Z. Anorg. Allg. Chem. 520, 1589 (1994).
23. C.M. Aherne, A.J. Banister, I.B. Gorrell, M.I. Hansford, Z.V. Hauptman, A.W. Luke, and J.M. Rawson. J. Chem. Soc. Dalton Trans. 967 (1993).
24. P. Del Bel Belluz, A.W. Cordes, E.M. Kristof, P.V. Kristof, S.W. Liblong, and R.T. Oakley. J. Am. Chem. Soc. 111, 9276 (1989).
25. J.B. Flanagan, S. Margel, A.J. Bard, and F.C. Anson. J. Am. Chem. Soc. 100, 4248 (1978).
26. F. Weller, F. Schmock, and K. Dehnicke. Z. Naturforsch. B: Chem. Sci. 44, 548 (1989).
27. A.W. Cordes, C.D. Bryan, W.M. Davis, R.H. de Laat, S.H. Glarum, J.D. Goddard, R.C. Haddon, R.G. Hicks, D.K. Kennepohl, R.T. Oakley, S.R. Scott, and N.P.C. Westwood. J. Am. Chem. Soc. 115, 7232 (1993).
28. F.A. Cotton and G. Wilkinson. Advanced inorganic chemistry. 3rd ed. Wiley, New York. 1972. p. 288.
29. P.A. Cox. Electronic structure and chemistry of solids. Oxford University Press, Oxford. 1987. p. 134.
30. D.T. Cromer and J.T. Waber. International tables for X-ray crystallography. Vol. IV. The Kynoch Press, Birmingham, England. 1974. Table 2.2 A.
31. D.C. Creagh and W.J. McAuley. International tables for crystallography. Vol C. Edited by A.J.C. Wilson. Kluwer Academic Publishers, Boston. 1992. Table 4.2.6.8, pp. 219-222.
32. H.-F. Fan. Structure analysis programs with intelligent control. Rigaku Corporation, Tokyo. 1991.
33. P.T. Beurskens, G. Admiraal, G. Beurskens, W.P. Bosman, R. de Gelder, R. Israel, and J.M.M. Smits. The DIRDIF-94 program system. Technical Report of the Crystallography Laboratory, University of Nijmegen, The Netherlands. 1992.
34. TEXSAN. Single-crystal structure analysis software. Molecular Structure Corporation, The Woodlands, Texas. 1994.
35. E.J. Gabe, Y. LePage, J.P. Charland, F.L. Lee, and P.S. White. J. Appl. Crystallogr. 22, 348 (1989).