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Fortney, A.D.1
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0011161005
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3 indicated that the methyl doublet at δ 1.15 ppm shifted downfield at a greater rate than the methyl doublet at δ 1.10 ppm. One interpretation might be that the signal at δ 1.15 belongs to the pro-R methyl group and the signal at δ 1.10 belongs to the pro-S methyl group (Figure 1), and thus the major diastereomer has the structure shown. However, since stereochemical interpretations of non-rigid systems based on lanthanide induced shifts should be treated with caution, these assignments can only be considered as tentative. Sullivan, G. R. J. Am. Chem. Soc. 1976, 98, 7162-9.
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12
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12
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39
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0011194377
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W = 0.053 and GOF = 1.48
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W = 0.053 and GOF = 1.48.
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40
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0011234485
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and references therein
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3 complexes see: Ref. 22b; Young, V. G., Jr.; Dasgupta, B.; Donaldson, W. A. J. Chem. Cryst. 1996, 26, 569-71 and references therein. Howell, J. A. S.; Bell, A. G.; O'Leary, P. J.; McArdle, P.; Dunningham, D.; Stephenson, G. R.; Hastings, M. Organometallics 1994, 13, 1806-12; Wang, J.-L.; Ueng, C.-H.; Cheng, S.-J.; Yeh, M.-C. P. Organometatlics 1994, 13, 4453-61; Nakanishi, S.; Yamamoto, H.; Otsuji, Y.; Nakazumi, H. Tetrahedron: Asymmetry 1993, 4, 1969-72.
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3 complexes see: Ref. 22b; Young, V. G., Jr.; Dasgupta, B.; Donaldson, W. A. J. Chem. Cryst. 1996, 26, 569-71 and references therein. Howell, J. A. S.; Bell, A. G.; O'Leary, P. J.; McArdle, P.; Dunningham, D.; Stephenson, G. R.; Hastings, M. Organometallics 1994, 13, 1806-12; Wang, J.-L.; Ueng, C.-H.; Cheng, S.-J.; Yeh, M.-C. P. Organometatlics 1994, 13, 4453-61; Nakanishi, S.; Yamamoto, H.; Otsuji, Y.; Nakazumi, H. Tetrahedron: Asymmetry 1993, 4, 1969-72.
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0000999679
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3 complexes see: Ref. 22b; Young, V. G., Jr.; Dasgupta, B.; Donaldson, W. A. J. Chem. Cryst. 1996, 26, 569-71 and references therein. Howell, J. A. S.; Bell, A. G.; O'Leary, P. J.; McArdle, P.; Dunningham, D.; Stephenson, G. R.; Hastings, M. Organometallics 1994, 13, 1806-12; Wang, J.-L.; Ueng, C.-H.; Cheng, S.-J.; Yeh, M.-C. P. Organometatlics 1994, 13, 4453-61; Nakanishi, S.; Yamamoto, H.; Otsuji, Y.; Nakazumi, H. Tetrahedron: Asymmetry 1993, 4, 1969-72.
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43
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0027291062
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3 complexes see: Ref. 22b; Young, V. G., Jr.; Dasgupta, B.; Donaldson, W. A. J. Chem. Cryst. 1996, 26, 569-71 and references therein. Howell, J. A. S.; Bell, A. G.; O'Leary, P. J.; McArdle, P.; Dunningham, D.; Stephenson, G. R.; Hastings, M. Organometallics 1994, 13, 1806-12; Wang, J.-L.; Ueng, C.-H.; Cheng, S.-J.; Yeh, M.-C. P. Organometatlics 1994, 13, 4453-61; Nakanishi, S.; Yamamoto, H.; Otsuji, Y.; Nakazumi, H. Tetrahedron: Asymmetry 1993, 4, 1969-72.
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-
3 complexes of 2,4-pentadienoic acid and of 2,4-hexadienoic acid by fractional crystallization of the diastereomeric α-methylbenzylammonium salts has been reported: Musco, A.; Palumbo, R.; Paiaro, G. Inorg. Chim. Acta 1971, 5, 157-60; de Montarby, L.; Tourbah, H.; Grée, R. Bull. Soc. Chim. Fr. 1989, 419-32.
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(1971)
Inorg. Chim. Acta
, vol.5
, pp. 157-160
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Musco, A.1
Palumbo, R.2
Paiaro, G.3
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48
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-
0001054994
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-
3 complexes of 2,4-pentadienoic acid and of 2,4-hexadienoic acid by fractional crystallization of the diastereomeric α-methylbenzylammonium salts has been reported: Musco, A.; Palumbo, R.; Paiaro, G. Inorg. Chim. Acta 1971, 5, 157-60; de Montarby, L.; Tourbah, H.; Grée, R. Bull. Soc. Chim. Fr. 1989, 419-32.
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(1989)
Bull. Soc. Chim. Fr.
, pp. 419-432
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-
De Montarby, L.1
Tourbah, H.2
Grée, R.3
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49
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-
0003034253
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-
(b) The chiral-auxiliary directed asymmetric complexation of dienamides derived from sorbaldehyde has been reported: Pearson, A. J.; Chang, K.; McConville, D. B.; Youngs, W. J. Organometallics 1994, 13, 4-5.
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(1994)
Organometallics
, vol.13
, pp. 4-5
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Pearson, A.J.1
Chang, K.2
McConville, D.B.3
Youngs, W.J.4
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51
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-
0000144214
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24. Djedaini, F.; Grée, D.; Martelli, J.; Grée, R.; Leroy, L.; Bolard, J.; Toupet, L. Tetrahedron Lett. 1989, 30, 3781-4.
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(1989)
Tetrahedron Lett.
, vol.30
, pp. 3781-3784
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Djedaini, F.1
Grée, D.2
Martelli, J.3
Grée, R.4
Leroy, L.5
Bolard, J.6
Toupet, L.7
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