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(c) Pirrung, M. C.; Krishnamurthy, N.; Nunn, D. S.; McPhail, A. T. J. Am. Chem. Soc. 1991, 113, 4910.
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(d) Paquette, L. A.; Trova, M. P.; Luo, J.; Clough, A. E.; Anderson, L. B. Ibid 1990, 112, 228.
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(e) Paquette, L. A.; Wang, T.-Z.; Luo, J.; Cottrell, C. E.; Clough, A. E.; Anderson, L. B. Ibid 1990, 112, 239
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8
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2. Selected methods for cyclooctatetraene synthesis: From cyclooctanes: (a) Lyttle, M. H.; Streitwieser, A. ; Miller, M. J. J. Org. Chem. 1989, 54, 2331.
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(b) Miller, M. J.; Lyttle, M. H.; Streitwieser, Jr., A. Ibid 1981, 46, 1977.
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(d) Paquette, L. A.; Photis, J. M.; Gifkins, K. B.; Clardy, J. J. Am. Chem. Soc. 1975, 97, 3536.
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via heteroatom extrusion: (i) Gottesfeld, M. R.; Masoudi, F. A.; Hansen, D. E.; Tetrahedron Lett., 1992, 33, 447.
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(j) Paquette, L. A.; Ley, S. V.; Meisinger, R. H.; Russell, R. K.; Oku, M. J. Am. Chem. Soc. 1974, 96, 5806.
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18
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0002454476
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Liebeskind, L. S., Ed.; JAI Press, Greenwich
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3. For an overview of metal-promoted higher-order cycloaddition, see: Rigby, J. H. in "Advances in Metal-Organic Chemistry," Liebeskind, L. S., Ed.; JAI Press, Greenwich: 1995, Vol. 4, pp. 89-127.
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5. Rigby, J. H.; Ateeq, H. S.; Krueger, A. C. Tetrahedron Lett. 1992, 33, 5873.
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6. (a) Chaffee, K.; Kuo, P.; Sheridan, J. B.; Barbieri, A.; Aistars, A.; Lalancette, R. A.; Ostrander, R. L.; Rheingold, A. L. J. Am. Chem. Soc. 1995, 117, 1900.
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(b) Rigby, J. H.; Ateeq, H. S.; Charles, N. R.; Henshilwood, J. A.; Short, K. M.; Sugathapala, P. M. Tetrahedron 1993, 49, 5495.
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(c) Fischler, I.; Grevels, F.-W.; Leitich, J.; Özkar, S. Chem. Ber. 1991, 124, 2857.
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7. Rigby, J. H.; Warshakoon, N. C.; Heeg, M. J. J. Am. Chem. Soc. 1996, 118, 6044.
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25
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0011201748
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note
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13C NMR, IR) and analytical (combustion analysis and/or HRMS) data consistant with the assigned structure.
-
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26
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0011160380
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9. (a) Paquette, L. A.; Hanzawa, Y.; Hefferon, G. J.; Blount, J. F. J. Org. Chem. 1982, 47,. 265.
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Blount, J.F.4
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