Preparation and properties of a 3,3-dialkyldithiirane

Tetrahedron Letters

Volumn 38, Issue 8, 1997, Pages 1431-1434

  Ishii, Akihiko ^a   Umezawa, Kazuyo ^a   Nakayama, Juzo ^a  

^a SAITAMA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

BICYCLO[3.2.1]OCTANE DERIVATIVE; ORGANOSULFUR DERIVATIVE;

ARTICLE; DRUG PURIFICATION; DRUG SYNTHESIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IN VITRO STUDY; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION ANALYSIS; STEREOCHEMISTRY; ULTRAVIOLET SPECTROPHOTOMETRY;

EID: 0031584923     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00040-3     Document Type: Article

References (20)

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2. 1. For reviews, see: Senning, A.; Hansen, H. C.; Abdel-Megeed, M. F.; Mazurkiewicz, W.; Jensen, B. Tetrahedron 1986, 42, 739-746; Senning, A. Sulfur Lett. 1986, 4, 213-216; Senning, A. Sulfur Lett. 1990, 11, 83-86.
3. 1. For reviews, see: Senning, A.; Hansen, H. C.; Abdel-Megeed, M. F.; Mazurkiewicz, W.; Jensen, B. Tetrahedron 1986, 42, 739-746; Senning, A. Sulfur Lett. 1986, 4, 213-216; Senning, A. Sulfur Lett. 1990, 11, 83-86.
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6. 3. a) Ishii, A.; Akazawa, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem. Int. Ed. Engl. 1994, 33, 777-779.
7. b) Ishii, A.; Akazawa, T.; Ding, M.-X.; Honjo, T.; Nakayama, J.; Hoshino, M.; Shiro, M. J. Am. Chem. Soc. 1993, 115, 4914-4915.
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11. 4. Huisgen, R.; Rapp, J. J. Am. Chem. Soc. 1987, 109, 902-903.
12. 5. Maier, G.; Roth, C.; Schmitt, R. K. Chem. Ber. 1985, 118, 704-721.
13. 6. Pfeffer, P. E.; Foglia, T. A.; Barr, P. A.; Schmeltz, I.; Silbert, L. S. Tetrahedron Lett. 1972, 4063-4066; Shaw, J. E.; Kunerth, D. C.; Sherry, J. J. Tetrahedron Lett. 1973, 689-692. HMPA was employed as the solvent in the literatures.
14. 6. Pfeffer, P. E.; Foglia, T. A.; Barr, P. A.; Schmeltz, I.; Silbert, L. S. Tetrahedron Lett. 1972, 4063-4066; Shaw, J. E.; Kunerth, D. C.; Sherry, J. J. Tetrahedron Lett. 1973, 689-692. HMPA was employed as the solvent in the literatures.
15. 7. Weagley, R. J.; Gibson, H. W. Synthesis 1986, 552-554.
16. 8. Pedersen, B. S.; Scheibye, S.; Nilsson, N. H.; Lawesson, S.-O. Bull. Soc. Chim. Belg. 1978, 87, 223-228.
17. 9. The pH of the aqueous layer was adjusted to 6 every 2 h by addition of 1M KOH.
18. +, 41), 284 (2), 252 (42), 112 (100), and 57 (77).
19. 11. Determination of the geometry of the E- and Z-thioketone S-oxide will be discussed elsewhere.
20. 12. Chew, M.; Harpp, D. N. Tetrahedron Lett. 1992, 33, 45-48.