Determination of the main hydrolysis product of O-ethyl S-2-diisopropylaminoethyl methylphosphonothiolate, ethyl methylphosphonic acid, in human serum

Journal of Chromatography B: Biomedical Applications

Volumn 689, Issue 2, 1997, Pages 327-333

  Katagi, M ^a   Nishikawa, M ^a   Tatsuno, M ^a   Tsuchihashi, H ^a  

^a OSAKA PREFECTURE UNIVERSITY   (Japan)

Author keywords

Ethyl methylphosphonic acid; O Ethyl S 2 diisopropylamonoethyl methylphosphonothiolate

Indexed keywords

METHYLPHOSPHONIC ACID; METHYLPHOSPHONOTHIOIC ACID S (2 DIISOPROPYLAMINOETHYL) O ETHYL ESTER;

ARTICLE; CALIBRATION; CONTROLLED STUDY; DERIVATIZATION; DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG HYDROLYSIS; GAS CHROMATOGRAPHY; HUMAN; HUMAN TISSUE; MASS SPECTROMETRY; NORMAL HUMAN; PRIORITY JOURNAL; QUANTITATIVE ASSAY;

CHOLINESTERASE INHIBITORS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; HYDROLYSIS; INDICATORS AND REAGENTS; ORGANOPHOSPHORUS COMPOUNDS; ORGANOSILICON COMPOUNDS; ORGANOTHIOPHOSPHORUS COMPOUNDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 0031581895     PISSN: 15726495     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0378-4347(96)00356-8     Document Type: Article

References (27)

1. [1] World Health Organization, Health Aspects of Chemical and Biological Weapons, Report of a WHO Group of consultants, Geneva, 1970.
2. [2] J.A.F. Compton, Military Chemical and Biological Agents, Chemical and Toxicological Properties, Telford Press, Caldwell, NJ, USA, 1987.
3. [3] J. Epstein, J.J. Callahan and V.E. Bauer, Phosphorus, 4 (1974) 157.
4. [4] J. Epstein, J.J. Kaminski, N. Bodor, R. Enever, J. Sowa and T. Higuchi, J. Org. Chem., 43 (1978) 2816.
5. [5] Y.C. Yang, L.L. Szafraniec, W.T. Beaudry and D.K. Rohrbaugh, J. Am. Chem. Soc., 112 (1990) 6621.
6. [6] Y.C. Yang, L.L. Szafraniec and W.T. Beaudry, J. Org. Chem., 58 (1993) 6964.
7. [7] A.T. Tu, Chemistry (in Japanese), 50 (1996) 480.
8. [8] Ch.E. Kientz, A. Verweij, H.L. Boter, A. Poppema, R.W. Frei, G.J. de jong and U.A.Th. Brinkman, J. Chromatogr., 467 (1989) 385.
9. [9] P.C. Bossle, D.J. Reutter and E.W. Sarver, J. Chromatogr., 407 (1987) 399.
10. [10] A.F. Kingery and H.E. Allen, Anal. Chem., 66 (1994) 155.
11. [11] S.A. Oehrle and P.C. Bossle, J. Chromatogr. A, 692 (1995) 247.
12. [12] E.R.J. Wils and A.G. Hulst, J. Chromatogr., 454 (1988) 261.
13. [13] D.J. Howells, J.L. Hambrook, D. Utley and J. Woodage, Pestic. Sci., 4 (1973) 239.
14. [14] A. Verweij, C.E.A.M. Degenhardt and H.L. Boter, Chemosphere, 3 (1979) 115.
15. [15] A. Verweij, H.L. Boter and C.A.A.M. Degenhardt, Science, 204 (1979) 616.
16. [16] C.G. Daughton, A.M. Cook and M. Alexander, J. Agric. Food Chem., 27(1979) 1375.
17. [17] C.G. Daughton, A.M. Cook and M. Alexander, Anal. Chem., 51 (1979) 1949.
18. [18] P.C. Bossle, J.J. Martin, E.W. Sarver and H.Z. Sommer, J. Chromatogr., 267 (1983) 209.
19. [19] M.C. Roach, L.W. Ungar, R.N. Zare, L.M. Reimer, D.L. Pompliano and J.W. Frost, Anal. Chem., 59 (1987) 1056.
20. [20] D.J. Harvey and M.G. Horning, J. Chromatogr., 79 (1973) 65.
21. [21] D.R. Maithews, W.D. Shults, M.R. Guerin and J.A. Dean, Anal. Chem., 43 (1971) 1582.
22. [22] G. Bauer and W. Vogt, Anal. Chem., 53 (1981) 917.
23. [23] P. Hirsjrvi, J.K. Miettinen, J. Paasivirta and E. Kanolahti (Editors), Trace analysis of Chemical Warfare Agents. I. An Approach to the Environmental Monitoring of Nerve Agents, Ministry of Foreign Affairs of Finland, Helsinki, 1981, pp. 27, 28, 37-39, 59-64, 72-79, 90-99.
24. [24] P. Hirsjrvi, J.K. Miettinen and J. Paasivirta (Editors), Identification of Degradation Products of Potential Organophosphorus Warfare Agents. An Approach for the Standardization of Techniques and Reference Data, Ministry of Foreign Affairs of Finland, Helsinki, 1981, pp. 3-10, 18-30 and appendices.
25. [25] J.G. Purdon, J.G. Pagotto and R.K. Miller, J. Chromatogr., 475 (1989) 261.
26. [26] J.Å. Tornes and B.A. Johnsen, J. Chromatogr., 467 (1989) 129.
27. [27] V. Bardarov and M. Mitewa, J. Chromatogr., 462 (1989) 233.