A molecular structure of mixed valence biruthenocenium (RuIIRuIV) salts [RuIICp(C5H4C5H4)CpRuIVL]2+(BF-4)2 (L = NCCH3, N(CH)4N)

Journal of Organometallic Chemistry

Volumn 549, Issue 1-2, 1997, Pages 13-23

  Watanabe, Masanobu ^a   Motoyama, Izumi ^a   Takayama, Toshio ^a   Sato, Masaru ^b  

^a KANAGAWA UNIVERSITY   (Japan)

^b SAITAMA UNIVERSITY   (Japan)

Author keywords

Metallocene; Mixed valence; Ruthenocene; X ray diffraction

Indexed keywords

EID: 0031577807     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(97)00230-1     Document Type: Article

References (42)

1. [1] K. Kirchner, K.S. Kwan, H. Taube, J. Chem. Soc. 113 (1991) 7039; K. Kirchner, K.S. Kwan, H. Taube, Inorg. Chem. 32 (1993) 4947; K. Kirchner, K. Mereiter, R. Schmid, J. Chem. Soc., Chem. Commun. (1994) 161; K. Kirchner, K. Merreiter, A. Umfahre, R. Schmid, Organometallics 13 (1994) 1886; K. Kirchner, K. Merreiter, K. Mauthner, R. Schmid, Organometallics 13 (1994) 3405; K. Mauthner, K. Merreiter, R. Schmid, K. Kirchner, Organometallics 13 (1994) 5054.
2. [1] K. Kirchner, K.S. Kwan, H. Taube, J. Chem. Soc. 113 (1991) 7039; K. Kirchner, K.S. Kwan, H. Taube, Inorg. Chem. 32 (1993) 4947; K. Kirchner, K. Mereiter, R. Schmid, J. Chem. Soc., Chem. Commun. (1994) 161; K. Kirchner, K. Merreiter, A. Umfahre, R. Schmid, Organometallics 13 (1994) 1886; K. Kirchner, K. Merreiter, K. Mauthner, R. Schmid, Organometallics 13 (1994) 3405; K. Mauthner, K. Merreiter, R. Schmid, K. Kirchner, Organometallics 13 (1994) 5054.
3. [1] K. Kirchner, K.S. Kwan, H. Taube, J. Chem. Soc. 113 (1991) 7039; K. Kirchner, K.S. Kwan, H. Taube, Inorg. Chem. 32 (1993) 4947; K. Kirchner, K. Mereiter, R. Schmid, J. Chem. Soc., Chem. Commun. (1994) 161; K. Kirchner, K. Merreiter, A. Umfahre, R. Schmid, Organometallics 13 (1994) 1886; K. Kirchner, K. Merreiter, K. Mauthner, R. Schmid, Organometallics 13 (1994) 3405; K. Mauthner, K. Merreiter, R. Schmid, K. Kirchner, Organometallics 13 (1994) 5054.
4. [1] K. Kirchner, K.S. Kwan, H. Taube, J. Chem. Soc. 113 (1991) 7039; K. Kirchner, K.S. Kwan, H. Taube, Inorg. Chem. 32 (1993) 4947; K. Kirchner, K. Mereiter, R. Schmid, J. Chem. Soc., Chem. Commun. (1994) 161; K. Kirchner, K. Merreiter, A. Umfahre, R. Schmid, Organometallics 13 (1994) 1886; K. Kirchner, K. Merreiter, K. Mauthner, R. Schmid, Organometallics 13 (1994) 3405; K. Mauthner, K. Merreiter, R. Schmid, K. Kirchner, Organometallics 13 (1994) 5054.
5. [1] K. Kirchner, K.S. Kwan, H. Taube, J. Chem. Soc. 113 (1991) 7039; K. Kirchner, K.S. Kwan, H. Taube, Inorg. Chem. 32 (1993) 4947; K. Kirchner, K. Mereiter, R. Schmid, J. Chem. Soc., Chem. Commun. (1994) 161; K. Kirchner, K. Merreiter, A. Umfahre, R. Schmid, Organometallics 13 (1994) 1886; K. Kirchner, K. Merreiter, K. Mauthner, R. Schmid, Organometallics 13 (1994) 3405; K. Mauthner, K. Merreiter, R. Schmid, K. Kirchner, Organometallics 13 (1994) 5054.
6. [1] K. Kirchner, K.S. Kwan, H. Taube, J. Chem. Soc. 113 (1991) 7039; K. Kirchner, K.S. Kwan, H. Taube, Inorg. Chem. 32 (1993) 4947; K. Kirchner, K. Mereiter, R. Schmid, J. Chem. Soc., Chem. Commun. (1994) 161; K. Kirchner, K. Merreiter, A. Umfahre, R. Schmid, Organometallics 13 (1994) 1886; K. Kirchner, K. Merreiter, K. Mauthner, R. Schmid, Organometallics 13 (1994) 3405; K. Mauthner, K. Merreiter, R. Schmid, K. Kirchner, Organometallics 13 (1994) 5054.
7. [2] K. Kirchner, K. Mereiter, R. Schmid, H. Taube, Inorg. Chem. 32 (1993) 1430.
8. [3] K. Kirchner, K. Mereiter, R. Schmid, H. Taube, Inorg. Chem. 32 (1993) 5553.
9. [4] K. Hashidzume, H. Tobita, H. Ogino, Organometallics 14 (1995) 1187.
10. [5] H. Ogino, H. Tobita, K. Hashidzume, M. Shimoi, J. Chem. Soc. Chem. Commun. (1989) 828.
11. [6] M. Watanabe, I. Motoyama, M. Shimoi, H. Sano, J. Organomet. Chem. 517 (1996) 115.
12. [7] M. Watanabe, I. Motoyama, M. Shimoi, T. Iwamoto, Inorg. Chem. 33 (1994) 2518.
13. [8] M. Watanabe, T. Iwamoto, A. Kubo, S. Kawata, H. Sano, I. Motoyama, Inorg. Chem. 31 (1992) 177.
14. [9] M. Watanabe, T. Iwamoto, H. Sano, I. Motoyama, J. Organomet. Chem. 442 (1992) 309.
15. [10] M. Watanabe, T. Iwamoto, H. Sano, I. Motoyama, J. Coord. Chem. 26 (1992) 223; M. Watanabe, T. Iwamoto, H. Sano, I. Motoyama, Inorg. Chem. 32 (1992) 5223.
16. [10] M. Watanabe, T. Iwamoto, H. Sano, I. Motoyama, J. Coord. Chem. 26 (1992) 223; M. Watanabe, T. Iwamoto, H. Sano, I. Motoyama, Inorg. Chem. 32 (1992) 5223.
17. [11] M. Watanabe, I. Motoyama, T. Takayama, M. Shimoi, H. Sano, J. Organomet. Chem. 496 (1995) 87.
18. [12] TEXSAN, Crystal Structure Analysis package, Molecular Structure Corporation, 1985.
19. [13] D.T. Cromer, J.T. Waber, International Table for X-ray Crystallography, Vol. IV, The Kynoch Press, Birmingham, UK, Table 2.2A (1974).
20. [14] J.A. Ibers, W.C. Hamilton, Acta Crystallogr. 17 (1964) 781.
21. [15] D.C. Creagh, W.J. McAuiey, International Table for X-ray Crystallography, Vol. C, Kluwer Academic Publishers, Boston. Table 4.2.6.8, pp. 219-222, 1992.
22. [16] T.A. Annan, A. Ozarowski, Z. Tianand, D.G. Tuck, J. Chem. Soc. Dalton Trans. 2931 (1992); T.A. Annan, Z. Tian, D.G. Tuck, J. Chem. Soc. Dalton Trans. (1991) 19; M.K. Khan, R.C. Steevensz, D.G. Tuck, J.G. Noltes, P.W.R. Corfield, Inorg. Chem. 19 (1980) 3407.
23. [16] T.A. Annan, A. Ozarowski, Z. Tianand, D.G. Tuck, J. Chem. Soc. Dalton Trans. 2931 (1992); T.A. Annan, Z. Tian, D.G. Tuck, J. Chem. Soc. Dalton Trans. (1991) 19; M.K. Khan, R.C. Steevensz, D.G. Tuck, J.G. Noltes, P.W.R. Corfield, Inorg. Chem. 19 (1980) 3407.
24. [16] T.A. Annan, A. Ozarowski, Z. Tianand, D.G. Tuck, J. Chem. Soc. Dalton Trans. 2931 (1992); T.A. Annan, Z. Tian, D.G. Tuck, J. Chem. Soc. Dalton Trans. (1991) 19; M.K. Khan, R.C. Steevensz, D.G. Tuck, J.G. Noltes, P.W.R. Corfield, Inorg. Chem. 19 (1980) 3407.
25. [17] C. Landgrafe, W.S. Sheldrick, J. Chem. Soc., Dalton Trans. (1996) 989; W. Luginbuhl, P. Zbinden, P.A. Pittet, T. Armbruster, H.B. Btirgi, A.E. Merbach, A. Ludi, Inorg. Chem. 30 (1991) 2350.
26. [17] C. Landgrafe, W.S. Sheldrick, J. Chem. Soc., Dalton Trans. (1996) 989; W. Luginbuhl, P. Zbinden, P.A. Pittet, T. Armbruster, H.B. Btirgi, A.E. Merbach, A. Ludi, Inorg. Chem. 30 (1991) 2350.
27. [18] P.E. Riley, C.E. Capshew, R. Pettit, R.E. Davis, Inorg. Chem. 17 (1978) 408.
28. [19] M. Sato, K. Suzuki, H. Asano, M. Sekino, Y. Kawata, J. Organometal. Chem. 470 (1994) 263.
29. [20] S.A. Koch, M. Millar, J. Am. Chem. Soc. 105 (1983) 3362.
30. [21] C.C. Costain, J. Chem. Phys. 29 (1958) 864.
31. [22] T.C. Wright, G. Wilkinson, M. Motevalli, M.B. Hursthouse, J. Chem. Soc., Dalton Trans. (1986) 2017.
32. [23] Private Communication.
33. [24] L. Pauling, The Nature of the Chemical Bond, 3rd ed., Cornell University Press, 1960.
34. [25] E.H. Rodd, Chemistry of Carbon Compounds 1-A, Ch. 6, p. 357, 1951.
35. [26] M.W. Droege, W.D. Harman, H. Taube, Inorg. Chem. 26 (1987) 1309.
36. [27] P.A. Lay, H. Magnuson, H. Taube, Inorg. Chem. 27 (1988) 2364.
37. [28] C. Creutz, H. Taube, J. Am. Chem. Soc. 91 (1969) 3988.
38. [29] C. Creutz, H. Taube, J. Am. Chem. Soc. 95 (1973) 1086.
39. [30] M.J. Begley, P. Hubbeerstey, J. Stroud, J. Chem. Soc., Dalton, Trans. (1996) 2323.
40. [31] S. Kitagawa, M. Munakata, T. Tanimura, Inorg. Chem. 31 (1992) 1714.
41. [32] C.L. Klein, R.J. Majeste, L.W. Trefonas, C. O'Connor, Inorg. Chem. 21 (1982) 1891.
42. [33] S. Kitagawa, M. Munakata, T. Tanimura, Chem. Lett. (1991) 623.