Mass Discrimination in the Analysis of Polydisperse Polymers by MALDI Time-of-Flight Mass Spectrometry. 1. Sample Preparation and Desorption/Ionization Issues

Analytical Chemistry

Volumn 69, Issue 20, 1997, Pages 4169-4175

  Schriemer, David C ^a   Li, Liang ^a  

^a UNIVERSITY OF ALBERTA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

DESORPTION; DISPERSIONS; IONIZATION; MASS SPECTROMETRY; MOLECULAR WEIGHT; POLYMER BLENDS; SPECTRUM ANALYSIS;

LASER DESORPTION; MASS DISCRIMINATION; POLYDISPERSE POLYMERS;

ORGANIC POLYMERS;

EID: 0031572678     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac9702610     Document Type: Article

References (54)

1. Bahr, U.; Deppe, A.; Karas, M.; Hillenkamp, F. Anal. Chem. 1992, 64, 2866-2869.
2. Juhasz, P.; Costello, C. E. Rapid Commun. Mass Spectrom. 1993, 7, 343-351.
3. Whittal, R. M.; Li, L.; Lee, S.; Winnik, M. A. Macromol. Rapid Commun. 1996, 17, 59-64.
4. Lee, S.; Winnik, M. A.; Whittal, R. M.; Li, L. Macromolecules 1996, 29, 3060-3072.
5. Jackson, A. T.; Yates, H. T.; Scrivens, J. H.; Critchley, G.; Brown, J.; Green, M. R.; Bateman, R. H. Rapid Commun. Mass Spectrom. 1996, 10, 1668-1674.
6. Weidner, S.; Kuhn, G.; Just, U. Rapid Commun. Mass Spectrom. 1995, 9, 697-702.
7. Danis, P. O.; Karr, D. E.; Westmoreland, D. G.; Piton, M. C.; Christie, D. I.; Clay, P. A.; Kable, S. H.; Gilbert, R. G. Macromolecules 1993, 26, 6684-6685.
8. Burger, H. M.; Muller, H.-M; Seebach, D.; Bornsen, K. O.; Schar, M.; Widmer, M. Macromolecules 1993, 26, 4783-4790.
9. Weidner, S.; Kuhn, G.; Friedrich, J.; Schroder, H. Rapid Commun. Mass Spectrom. 1996, 10, 40-46.
10. Weidner, S.; Kuhn, G.; Friedrich, J.; Unger, W.; Lippitz, A. Rapid Commun. Mass Spectrom. 1996, 10, 727-732.
11. Wilczek-Vera, G.; Danis, P. O.; Eisenberg, A. Macromolecules 1996, 29, 4036-4044.
12. Schriemer, D. C.; Whittal, R. M.; Li, L. Macromolecules 1997, 30, 1955-1963.
13. Lloyd, P. M.; Suddaby, K. G.; Varney, J. E.; Scrivener, E.; Derrick, P. J.; Haddleton, D. M. Eur. Mass. Spectrom. 1995, 1, 293-300.
14. Danis, P. O.; Karr, D. E. Macromolecules 1995, 28, 8548-8551.
15. Danis, P. O.; Karr, D. E.; Xiong, Y.; Owens, K. G. Rapid Commun. Mass Spectrom. 1996, 10, 862-868.
16. Danis, P. O.; Karr, D. E. Org. Mass Spectrom. 1993, 28, 923-925.
17. Schriemer, D. C.; Li, L. Anal. Chem. 1996, 68, 2721-2725.
18. Montaudo, G.; Montaudo, M. S.; Puglisi, C.; Samperi, F. Rapid Commun. Mass Spectrom. 1994, 8, 1011-1015.
19. Cottrell, J. S.; Koerner, M.; Gerhards, R. Rapid Commun. Mass Spectrom. 1995, 9, 1562-1564.
20. Montaudo, G.; Montaudo, M. S.; Puglisi, C.; Samperi, F. Rapid Commun. Mass Spectrom. 1995, 9, 453-460.
21. Mowat, I. A.; Donovan, R. J. Rapid Commun. Mass Spectrom. 1995, 9, 82-90.
22. Belu, A. M.; DeSimone, J. M.; Linton, R. W.; Lange, G. W.; Friedman, R. M. J. Am. Soc. Mass Spectrom. 1996, 7, 11-24.
23. Danis, P. O.; Karr, D. E.; Simonsick, W. J.; Wu, D. T. Macromolecules 1995, 28, 1229-1232.
24. Colby, S. M.; King, T. B.; Reilly, J. P. Rapid. Commun. Mass Spectrom. 1994, 8, 865-868.
25. Brown, R. S.; Lennon, J. J. Anal. Chem. 1995, 67, 1998-2003.
26. Whittal, R. M.; Li, L. Anal. Chem. 1995, 67, 1950-1954.
27. Vestal, M. L.; Juhasz, P.; Martin, S. A. Rapid Commun. Mass Spectrom. 1995, 9, 1044-1050.
28. Lehrle, R. S.; Sarson, D. S. Rapid Commun. Mass Spectrom. 1995, 91-92.
29. Dogruel, D.;. Nelson, R. W.; Williams, P. Rapid Commun. Mass Spectrom. 1996, 10, 801-804.
30. Yates, H. T.; Scrivens, J.; Jackson, T.; Deery, M. In Proceedings of the 44th ASMS Conference on Mass Spectrometry and Allied Topics; May 12-16, Portland, OR, 1996; p 903.
31. Jackson, A. T.; Yates, H. T.; MacDonald, W. A.; Scrivens, J. H.; Critchley, G.; Brown, J.; Deery, M. J.; Jennings, K. R.; Brookes, C. J. Am. Soc. Mass Spectrom. 1997, 8, 132-139.
32. Cottrell, J. S.; Dwyer, J. L. In Proceedings of the 44th ASMS Conference on Mass Spectrometry and Allied Topics; May 12-16, Portland, OR, 1996; p 900.
33. Kassis, C. M.; Belu, A. M.; DeSimone, J. M.; Linton, R. W.; Lange, G. W.; Friedman, R. M. In Proceedings of the 44th ASMS Conference on Mass Spectrometry and Allied Topics; Portland, OR, 1996; p 1096.
34. Mowat, I. A.; Donovan, R. J.; Monaghan, J. J. In Proceedings of the 44th ASMS Conference on Mass Spectrometry and Allied Topics; May 12-16, Portland, OR, 1996; p 897.
35. Pastor, S.; Wilkins, C. L. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1996, 37, 284-285.
36. Von Helden, G.; Wyttenbach, T.; Bowers, M. T. Science 1995, 267, 1483-1485.
37. Montaudo, G.; Scamporrino, E.; Vitalini, D.; Mineo, P. Rapid Commun. Mass Spectrom. 1996, 10, 1551-1559.
38. Tang, X.; Dreifuss, P. A.; Vertes, A. Rapid Commun. Mass Spectrom. 1995, 9, 1141-1147.
39. Larsen, B. S.; Simonsick, W. J.; McEwen, C. N. J. Am. Soc. Mass Spectrom. 1996, 7, 287-292.
40. Axelsson, J.; Scrivener, E.; Haddleton, D. M.; Derrick, P. J. In Proceedings of the 44th ASMS Conference on Mass Spectrometry and Allied Topics; May 12-16, Portland, OR, 1996; p 895.
41. Martin, K.; Spickermann, J.; Rader, H. J.; Mullen, K. Rapid Commun. Mass Spectrom. 1996, 10, 1471-1474.
42. Jackson, C.; Larsen, B.; McEwen, C. Anal. Chem. 1996, 68, 1303-1308.
43. McEwen, C.; Jackson, C.; Larsen, B. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1996, 37, 314-315.
44. Guttman, C. M. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1996, 37, 837-838.
45. McEwen, C.; Jackson, C.; Larsen, B. In Proceedings of the 43rd ASMS Conference on Mass Spectrometry and Allied Topics; May 21-26, Atlanta, GA, 1995; p 23.
46. Montaudo, G.; Montaudo, M. S.; Puglisi, C.; Samperi, F. Rapid Commun. Mass Spectrom. 1995, 9, 1158-1163.
47. Danis, P. O.; Saucy, D. A.; Huby, F. J. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1996, 37, 311-312.
48. Schriemer, D. C.; Whittal, R. M.; Li, L. In Proceedings of the 44th ASMS Conference on Mass Spectrometry and Allied Topics; May 12-16, Portland, OR, 1996; p 896.
49. Whittal, R. M.; Schriemer, D. C.; Li, L. Anal. Chem. 1997, 69, 2734-2741.
50. Dreisewerd, K.; Schurenberg, M.; Karas, M.; Hillenkamp, F. Int. J. Mass Spectrom. Ion Processes 1995, 141, 127-148.
51. Hillenkamp, F.; Karas, M.; Beavis, R. C.; Chait, B. T. Anal. Chem. 1991, 63, 1193A-1203A.
52. Fractionation of Synthetic Polymers: Principles and Practices; Tung, L. H., Ed.; Marcel Dekker: New York, 1977.
53. Determination of Molecular Weight; Cooper, A. R., Ed.; John Wiley and Sons: New York, 1989; Vol. 103.
54. Harnett, D. L. Statistical Methods; 3rd ed.; Addison-Wesley Publishing: Reading, MA, 1982.