Comparison of commercially available reagents for fluorination of steroid 3,5-dienol acetates

Organic Process Research and Development

Volumn 1, Issue 3, 1997, Pages 217-221

  Reydellet Casey, Valérie ^a   Knoechel, Donald J ^a   Herrinton, Paul M ^a  

^a PFIZER INC   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0031528281     PISSN: 10836160     EISSN: None     Source Type: Journal    
DOI: 10.1021/op960045d     Document Type: Article

References (8)

1. Fried, J.; Sabo, E. F. J. Am. Chem. Soc. 1954, 76, 1455.
2. Bowers, A.; Cuellar Ibanez, L.; Ringold, H. J. Tetrahedron 1959, 7, 138.
3. Bowers, A.; Cuellar Ibanez, L.; Denot, E.; Becerra, R. J. Am. Chem. Soc. 1960, 82, 4001.
4. (a) Magerlein, B. J.; Pike, J. E.; Jackson, R. W.; Vandenberg, G. E.; Kagan, F. J. Org. Chem. 1964, 29, 2982.
5. (b) Timko, J. M. DE 3226164, Feb 3, 1983, US Appl. 286306, July 24, 1981.
6. (c) Osawa, Y.; Neeman, M. J. Org. Chem. 1967, 32, 3055.
7. Hesse, R. H. Isr. J. Chem. 1978, 17, 60.
8. For a review of electrophilic NF fluorinating reagents, see: Lal, G. S.; Pez, G. P.; Syvret, R. G. Chem. Rev. 1996, 96, 1737.