NMR spectral assignment of substituted salicylaldoximes by inverse pulse techniques with z-gradient selection: Correlation of NMR parameters with substituent constants

Magnetic Resonance in Chemistry

Volumn 35, Issue 11, 1997, Pages 778-784

  Kolehmainen, Erkki ^a   Gawinecki, Ryszard ^b   Ośmiałowski, Borys ^b   Trzebiatowska, Katarzyna ^b  

^a UNIVERSITY OF JYVÄSKYLÄ   (Finland)

^b UNIVERSITY OF TECHNOLOGY AND LIFE SCIENCES   (Poland)

Author keywords

13C HMQC; 13C NMR; 1H; 1H NMR; 1H,15N HMBC with z gradient selection; Salicylaldoximes; Substituent effect

Indexed keywords

HYDROGEN BONDS;

13C HMQC; 13C NMR; 1H; 1H NMR; 1H,15N HMBC WITH Z-GRADIENT SELECTION; PULSE TECHNIQUE; SALICYLALDOXIME; SPECTRAL ASSIGNMENTS; SUBSTITUENT CONSTANTS; SUBSTITUENT EFFECT;

HYDROGEN;

EID: 0031512858     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(sici)1097-458x(199711)35:11<778::aid-omr174>3.3.co;2-a     Document Type: Article

References (29)

1. E. Kolehmainen, K. Laihia, D. Rasała and R. Gawinecki, Magn. Reson. Chem. 29, 878 (1991).
2. D. Rasała and R. Gawinecki, Magn. Reson. Chem. 30, 740 (1992).
3. E. Kolehmainen, K. Laihia, K. Rissanen, D. Rasała and R. Gawinecki, Magn. Reson. Chem. 30, 527 (1992).
4. D. Rasała and R. Gawinecki, Magn. Reson. Chem. 31, 38 (1993).
5. E. Kolehmainen, K. Laihia, R. Kauppinen, R. Gawinecki and D. Rasała, Magn. Reson. Chem. 31, 659 (1993).
6. I. Pejković-Tadić, M. Hranislavljević-Jakovljević, S. Nešić, C. Pascual and W. Simon, Helv. Chim. Acta 48, 1157 (1965).
7. G. Cerioni and A. Plumitallo, Magn. Reson. Chem. 31, 320 (1993).
8. G. V. Rutkovskii, Yu. A. Ignatev and A. V. Begunov, Zh. Org. Khim. 18, 2215 (1982).
9. G. V. Rutkovskii and V. P. Zmeikov, Zh. Org. Khim. 23, 142 (1987).
10. M. S. Gordon, S. A. Sojka and J. G. Krause, J. Org. Chem. 49, 97 (1984).
11. A. Danoff, M. Franzen-Sieveking, R. L. Lichter and S. N. Y. Fanso-Free, Org. Magn. Reson. 12, 83 (1979).
12. P. W. Westerman, R. E. Botto and J. D. Roberts, J. Org. Chem., 43, 2590 (1978).
13. E. E. Snell and S. I. Dimari, in Enzymes, edited by P. D. Boyer, Vol. 2, pp. 355-370. Academic Press, New York (1970).
14. Ch. Chang, T.-L. Shieh and H. G. Floss, J. Med. Chem. 20, 176 (1977).
15. W. C. Baird and R. L. Shriner, J. Am. Chem. Soc. 86, 3142 (1964).
16. B. S. Furniss, A. J. Hannaford, V. Rogers, P. W. G. Smith and A. R. Tatchel, Vogel's Textbook of Practical Organic Chemistry, p. 811. Longman, London (1981).
17. J. Meisenheimer, P. Zimmermann and U. v. Kummer, Liebigs Ann. Chem. 446, 205 (1925).
18. R. Stoermer, Liebigs Ann. Chem. 312, 237 (1900).
19. H. Biltz and K. Stepf, Chem. Ber. 37, 4022 (1904).
20. K. Auwers and A. J. Walker, Chem. Ber. 31, 3037 (1899).
21. J. Shinoda, J. Chem. Soc. 1983 (1927).
22. E. Ott and E. Nauen, Chem. Ber. 55, 920 (1922).
23. A. Bax, R. H. Griffey and B. L. Hawkins, J. Magn. Reson. 55, 301 (1983).
24. A. Bax and S. Subramanian, J. Magn. Reson. 67, 565 (1986).
25. A. Bax and M. F. Summers, J. Am. Chem. Soc. 108, 2093 (1986).
26. O. Exner, in Correlation Analysis in Chemistry; Recent Advances, edited by N. B. Chapman and J. Shorter, pp. 439-540. Plenum Press, New York (1978).
27. H. C. Brown and Y. Okamoto, J. Am. Chem. Soc, 80, 4979 (1958).
28. C. G. Swain and E. C. Lupton, J. Am. Chem. Soc. 90, 4328 (1968).
29. N. B. Smith and T. W. Proulx, Org. Magn. Reson. 8, 567 (1976).