Synthesis and reactions of the first lead-sulfur double-bond compounds, plumbanethiones

Chemistry Letters

Volumn , Issue 3, 1997, Pages 277-278

  Kano, Naokazu ^a   Tokitoh, Norihiro ^a   Okazaki, Renji ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0031491663     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1997.277     Document Type: Article

References (24)

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16. H. Suzuki, N. Tokitoh, S. Nagase, and R. Okazaki, J. Am. Chem. Soc., 116, 11578 (1994); N. Tokitoh, T. Matsumoto, and R. Okazaki, Chem. Lett., 1995, 1087; N. Tokitoh, T. Matsumoto, K. Manmaru, and R. Okazaki, J. Am. Chem. Soc., 115, 8855 (1993); T. Matsumoto, N. Tokitoh, and R. Okazaki, Angew. Chem., Int. Ed. Engl., 33, 2316 (1994); N. Tokitoh, M. Saito, and R. Okazaki, J. Am. Chem. Soc., 115, 2065 (1993); M. Saito, N. Tokitoh, and R. Okazaki, J. Organomet. Chem., 499, 43 (1995).
17. H. Suzuki, N. Tokitoh, S. Nagase, and R. Okazaki, J. Am. Chem. Soc., 116, 11578 (1994); N. Tokitoh, T. Matsumoto, and R. Okazaki, Chem. Lett., 1995, 1087; N. Tokitoh, T. Matsumoto, K. Manmaru, and R. Okazaki, J. Am. Chem. Soc., 115, 8855 (1993); T. Matsumoto, N. Tokitoh, and R. Okazaki, Angew. Chem., Int. Ed. Engl., 33, 2316 (1994); N. Tokitoh, M. Saito, and R. Okazaki, J. Am. Chem. Soc., 115, 2065 (1993); M. Saito, N. Tokitoh, and R. Okazaki, J. Organomet. Chem., 499, 43 (1995).
18. H. Suzuki, N. Tokitoh, S. Nagase, and R. Okazaki, J. Am. Chem. Soc., 116, 11578 (1994); N. Tokitoh, T. Matsumoto, and R. Okazaki, Chem. Lett., 1995, 1087; N. Tokitoh, T. Matsumoto, K. Manmaru, and R. Okazaki, J. Am. Chem. Soc., 115, 8855 (1993); T. Matsumoto, N. Tokitoh, and R. Okazaki, Angew. Chem., Int. Ed. Engl., 33, 2316 (1994); N. Tokitoh, M. Saito, and R. Okazaki, J. Am. Chem. Soc., 115, 2065 (1993); M. Saito, N. Tokitoh, and R. Okazaki, J. Organomet. Chem., 499, 43 (1995).
19. H. Suzuki, N. Tokitoh, S. Nagase, and R. Okazaki, J. Am. Chem. Soc., 116, 11578 (1994); N. Tokitoh, T. Matsumoto, and R. Okazaki, Chem. Lett., 1995, 1087; N. Tokitoh, T. Matsumoto, K. Manmaru, and R. Okazaki, J. Am. Chem. Soc., 115, 8855 (1993); T. Matsumoto, N. Tokitoh, and R. Okazaki, Angew. Chem., Int. Ed. Engl., 33, 2316 (1994); N. Tokitoh, M. Saito, and R. Okazaki, J. Am. Chem. Soc., 115, 2065 (1993); M. Saito, N. Tokitoh, and R. Okazaki, J. Organomet. Chem., 499, 43 (1995).
20. N. Tokitoh, N. Kano, K. Shibata, and R. Okazaki, Organometallics, 14, 3121 (1995).
21. We have reported that the thioketone analogues of group 14 elements dimerize when they do not bear a sufficiently bulky group on their group 14 elements. See ref. 5.
22. + 1156.5438.
23. The molecular structures for 4b and 5b were also determined by preliminary X-ray crystallographic analysis. The results of the X-ray crystallographic analysis will be published elsewhere.
24. The main product is TbtH. The minor products are an unidentifiable complex mixture.