A practical guide to solid-state NMR of half-integer quadrupolar nuclei with some applications to disordered systems

Geoderma

Volumn 80, Issue 3-4, 1997, Pages 271-306

  Kentgens, A P M ^a  

^a RADBOUD UNIVERSITY NIJMEGEN   (Netherlands)

Author keywords

Alumina; Aluminosilicate; Clays; MAS NMR; MQMAS; Quadrupolar nuclei

Indexed keywords

MAGIC ANGLE SPINNING; NUCLEAR MAGNETIC RESONANCE; QUADRUPOLAR MUCLEI;

EID: 0031474502     PISSN: 00167061     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0016-7061(97)00056-6     Document Type: Article

References (35)

1. Abragam, A., 1963. Principles of Nuclear Magnetism. Oxford University Press, Oxford.
2. 27 Al MAS NMR of catalysts and minerals. Appl. Magn. Reson. 4, 179.
3. Amoureux, J.P., Fernandez, C., Steuernagel, S., 1996a. Z-filtering in MQMAS NMR. J. Magn. Reson. A 123, 116.
4. Amoureux, J.P., Fernandez, C., Frydman, L., 1996b. Optimized multiple-quantum magic-angle spinning experiments on half-integer quadrupoles. Chem. Phys. Lett. 259, 397.
5. Andrew, E.R., Tunstall, D.P., 1961. Spin-lattice relaxation in imperfect cubic crystals and in non-cubic crystals. Proc. Phys. Soc. 78, 1.
6. Brown, S.P., Heyes, S.J., Wimperis, S., 1996. Two-dimensional MAS Multiple-Quantum NMR of quadrupolar nuclei, removal of inhomogeneous second-order broadening. J. Magn. Reson. A 119, 280.
7. Cohen, M.H., Reif, F., 1957. Quadrupole effects in nuclear magnetic resonance studies of solids. In: Seitz, F., Turnbull, D. (Eds.), Solid State Physics: Advances in Research and Applications, Vol. 5. Academic Press, New York, pp. 321-438.
8. Freude, D., Haase, J., 1993. Quadrupole effects in solid-state nuclear nagnetic resonance. In: Diehl, P., Fluck, E., Günther, H., Kosfeld, R., Seelig, J. (Eds.), NMR. Basic Principles and Progress, Vol. 29. Springer, Berlin, pp. 1-90.
9. Frydman, L., Harwood, J.S., 1995. Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR. J. Am. Chem. Soc. 117, 5367.
10. Haase, J., Conradi, M.S., 1993. Sensitivity enhancement for NMR of the central transition of quadrupolar nuclei. Chem. Phys. Lett. 209, 287.
11. 27Al MAS NMR by high speed satellite transition spectroscopy. J. Magn. Reson. 99, 353.
12. Jakobsen, H.J., Skibsted, J., Bildsoe, H., Nielsen, N.C., 1989. MAS NMR spectra of satellite transitions for quadrupolar nuclei in solids. J. Magn. Reson. 85, 173.
13. Kentgens, A.P.M., 1991. Quantitative excitation of half-integer quadrupolar nuclei by a frequency-stepped adiabatic half-passage. J. Magn. Reson. 95, 619.
14. Kentgens, A.P.M., 1993. Off-resonance nutation NMR spectroscopy of half-integer quadrupolar nuclei. J. Magn. Reson. A 104, 302.
15. Kentgens, A.P.M., Lemmens, J.J.M., Geurts, F.M.M., Veeman, W.S., 1987. Two-dimensional solid-state nutation NMR of half-integer quadrupolar nuclei. J. Magn. Reson. 71, 62.
16. 27Al nuclear magnetic resonance spectroscopy. Solid State Nucl. Magn. Reson. 3, 315.
17. 23Na NMR spectroscopy of solids. Interpretation of quadrupolae interaction parameters and chemical shifts. J. Phys. Chem. 98, 1544.
18. 3, hydrotreating catalyst precursors. J. Phys. Chem. 100, 16336.
19. Kundla, E., Samoson, A., Lippmaa. E., 1981. High resolution NMR of quadrupolar nuclei in rotating solids. Chem. Phys. Lett. 83, 229.
20. Liao, M.Y., Chew, B.G.M., Zax, D.B., 1995. Noise excitation of half-integer quadrupolar spins at high fields. Chem. Phys. Lett. 242, 89.
21. Llor, A., Virlet, J., 1988. Towards high-resolution NMR of more nuclei in solids: Samplespinning with time-dependent spinner axis angle. Chem. Phys. Lett. 152, 248.
22. Lucken, E.A., 1969. Nuclear Quadrupole Coupling Constants. Academic Press, New York.
23. 27Al MAS NMR in crystalline YAG. J. Magn. Reson. 90, 231.
24. Medek, A., Harwood, J.S., Frydman, L., 1995. Multiple-quantum magic-angle spinning NMR: A new method for the study of quadrupolar nuclei in solids. J. Am. Chem. Soc. 117, 12779.
25. Mueller, K.T., Sun, B.Q., Chingas, G.C., Zwanziger, J.W., Terao, T., Pines. A., 1990. Dynamicangle spinning of quadrupolar nuclei. J. Magn. Reson. 86, 470.
26. 27 MAS, MQMAS and off-resonance nutation NMR study of aluminium containing silica-based sol-gel materials. Solid State Nucl. Magn. Reson. (in press).
27. Samoson, A., 1985. Satellite transition high resolution NMR of quadrupolar nuclei in powders. Chem. Phys. Lett. 119, 29.
28. Samoson, A., Lippmaa, E., 1983. Central transition NMR excitation spectra of half-integer quadrupole nuclei. Chem. Phys. Lett. 100, 205.
29. Samoson, A., Lippmaa, E., 1988. 2D NMR nutation spectroscopy in solids. J. Magn. Reson. 79, 255.
30. Samoson, A., Kundla, E., Lippmaa, E., 1982. High resolution MAS-NMR of quadrupolar nuclei in powders. J. Magn. Reson. 49, 350.
31. Samoson, A., Lippmaa, E., Pines, A., 1988. High-resolution solid-state NMR. Averaging of second-order effects by means of a double-rotor. Mol. Phys. 65, 1013.
32. 3 glasses. J. Phys. Chem. 95, 4483.
33. 27Al NMR techniques to structure determination in solids. Appl. Magn. Reson. 4, 1.
34. Sun, B.Q., Baltisberger, J.H., Wu, Y., Samoson, A., Pines, A., 1992. Sidebands in Dynamic Angle Spinning (DAS) and Double Rotation (DOR) NMR. Solid State Nucl. Magn. Reson. 1, 267.
35. Vogels, R.J.M.J., 1996. Non-hydrothermally synthesised trioctahedral smectites. Ph.D. thesis, Utrecht.