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15
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4143112388
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note
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In the experiment on NaCl crystallites, the rf nutation rate of the pulse was set to 50.0 kHz.
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17
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4143099211
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note
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This is the minimum phase cycling for I = 3/2 nuclei, and 6-fold phase cycling is needed in the third pulse for the case of I = 5/2 nuclei to suppress the coherence transfer to -1 from not only triple-quantum but also quintuple-quantum coherence.
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19
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33644757144
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20
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85085781025
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note
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1 dimension of 2D spectra.
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-
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22
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0001505878
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Nagayama, K.; Kumar, A.; Wüthrich, K.; Ernst, R. R. J. Magn. Reson. 1980, 40, 321.
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23
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0001098946
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25
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85085782032
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-
note
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0 in the denominator of the second term is a sufficiently good approximation, which gives faster line-shape calculation under the constraint.
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27
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85085781604
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note
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1 dimension in order to obtain better S/N spectra and to avoid rounding errors in the shearing treatment caused by the limited digital resolution.
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28
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84989111458
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Massiot, D.; Kahn-Harari, A.; Michel, D.; Muller, D.; Taulelle, F. Magn. Reson. Chem. 1990, 28, S82.
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Massiot, D.1
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Taulelle, F.5
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29
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85085782440
-
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note
-
2 This seems to be due to a difference in hydration state or polymorphic form between the samples. (personal information from Dr. L. Frydman, University of Illinois and Dr. C. Jäger, University of Jena).
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-
-
-
30
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85085781133
-
-
note
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1 dimension folded back.
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-
-
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31
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85085780852
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-
note
-
1 value at the peak from the theoretically expected value is considered to be almost within the experimental error.
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