Synthesis of tritium-labelled N(τ)-methylhistamine for the improvement of extraction efficiency of (nτ)-methylhistamine from biological fluids

Applied Radiation and Isotopes

Volumn 48, Issue 9, 1997, Pages 1187-1191

  Iwashina, Takashi ^a   Scott, Paul G ^a   Tredget, Edward E ^a,b  

^a UNIVERSITY OF ALBERTA   (Canada)

^b UNIVERSITY OF ALBERTA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

AMINES; BODY FLUIDS; CHROMATOGRAPHIC ANALYSIS; EXTRACTION; HYDROLYSIS; ORGANIC SOLVENTS; PURIFICATION; SILANES; SILICA; SODIUM COMPOUNDS; SYNTHESIS (CHEMICAL); TRITIUM;

FACILE PURIFICATION; HUMAN PLASMA; METHYLHISTAMINE; URINE;

RADIOACTIVE TRACERS;

HISTAMINE; N METHYLHISTAMINE; TRITIUM;

ARTICLE; BLOOD LEVEL; HISTAMINE BLOOD LEVEL; HISTAMINE RELEASE; HUMAN; PRIORITY JOURNAL; PURIFICATION; URINE LEVEL;

CHEMISTRY, ANALYTICAL; HUMANS; ISOTOPE LABELING; METHYLATION; METHYLHISTAMINES; RADIOPHARMACEUTICALS; TRITIUM;

EID: 0031231505     PISSN: 09698043     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0969-8043(96)00310-7     Document Type: Article

References (23)

1. Beaven A. M., Jacoben S. and Horakova Z. (1971) Modification of the enzymatic isotopic assay of histamine and its application to measurement of histamine in tissues, serum and urine. Clin. Chim. Acta 37, 91.
2. Black W. J. and Granellin R. C. (1974) Naming of substituted histamines. Experientia 30, 111.
3. 14C histamine in subjects with bronchial ashma. J. Allergy 38, 290.
4. Granerus G. and Wass U. (1984) Urinary excretion of histamine, methylhistamine (1-MeHi) and methylimidazoleacetic acid (MeImAA) in mastocytosis: comparison of new HPLC methods with other present methods. Agents Actions 14, 341.
5. Hough B. L., Philip L. S. and Domino F. E. (1979) Gas chromatography-mass spectrometric characteristics and assay of tele-methylhistamine. Anal. Biochem. 96, 56.
6. Ind P. W., Barnes P. J., Lhoste M. J., Causon R. and Dollery C. T. (1983) Measurement of plasma histamine in asthma. Clin. Allergy 13, 61.
7. Ind P. W., Broun M. J., Lhoste M. J., Macquin I. and Dollery C. T. (1982) 1. Determination of histamine and its metabolites. Concentration effect relationships of infused histamine in normal volunteers. Agents Actions 12, 12.
8. Keyzer J. J., De Monchy Jan G. R., Van Doormaal J. J. and Van Voorst Vader P. C. (1983) Improved diagnosis of mastocytosis by measurement of urinary histamine metabolites. N. Engl. J. Med. 309, 1603.
9. t-methylhistamine in plasma and urine by isotope dilution mass fragmentography. Clin. Chem. Acta 113, 165.
10. Kischer C. W., Bunce III H. and Shetlar R. M. (1978) Mast cell analysis in hypertrophic scars, hypertrophic scars treated with pressure and mature scars. J. Invest. Dermatol. 70, 355.
11. Kluim-Nelemans H. C., Jansen J. S., Breukelman H., Wolthers B. G., Kroon H. M. and Willemze R. (1992) Response to interferon alpha-2b in a patient with systemic mastocytosis. N. Engl. J. Med. 326, 619.
12. Lott S. R., Chauman S. V. and Stammer H. C. (1979) Trimethylsilyl iodide as a peptide deblocking agent. J.C.S. Chem. Commun. 495, 0.
13. Maslinski C. (1975) Histamine and its metabolism in mammals part II: catabolism of histamine and histamine liberation. Agents Actions 5, 181.
14. t-methylhistamine in human plasma and urine by gas chromatography-mass spectrometry. J. Chromatogr., Biomed. Appl, 221, 1.
15. t-methylhistamine excretion in man. J. Chromatogr. 567, 289.
16. 4, chondroitin sulfate E proteoglycan, β-hexosaminidase, and histamine from cultured bone marrow-derived mouse mast cells. J. Exp. Med. 157, 189.
17. 13C NMR spectroscopy. Can. J. Biochem. 55, 576.
18. Schayer W. R. (1959) Catabolism of physiological quantities of histamine in vivo. Phys. Rev. 39, 116.
19. Schayer R. W. and Karjala S. A. (1956) Ring N methylation; a major route of histamine metabolism. J. Biol. Chem. 221, 307.
20. Snyder H. S., Baldessarini J. R. and Axelrod J. (1966) A sensitive and specific enzymatic isotopic assay for tissue histamine. J. Pharmac. Exp. Ther. 153, 544.
21. Swahn C.-G. and Sedvall G. (1981) Identification and determination of tele-methylhistamine in cerebrospinal fluid by gas chromatography-mass spectrometry. J. Neurochem. 37, 461.
22. Tarbell D. S., Yamamoto Y. and Pope M. B. (1972) New method to prepare N-t-butoxycarbonyl derivatives and the corresponding sulfur analogs from di-t-butyl dicarbonate or di-t-butyl dicarbonates and amino acids. Proc. Natn. Acd. Sci. U.S.A. 69, 730.
23. Wollin A. and Navert H. (1985) Quantitation of histamine and some of its basic methylated metabolites in biological materials by gas-liquid chromatography. Anal. Biochem 145, 73.