Synthesis of high surface area titania powders via basic hydrolysis of titanium(IV) isopropoxide

Powder Technology

Volumn 92, Issue 3, 1997, Pages 233-239

  Khalil, Kamal M S ^a   Zaki, Mohamed I ^b  

^a SOHAG UNIVERSITY   (Egypt)

^b KUWAIT UNIVERSITY   (Kuwait)

Author keywords

Calcination; Hydrolysis; Surface area; Titania powders

Indexed keywords

ADSORPTION ISOTHERMS; AMMONIA; CALCINATION; GAS ADSORPTION; HYDROLYSIS; NITROGEN; POWDERS; SOLVENTS; SYNTHESIS (CHEMICAL); TEXTURES; TRANSMISSION ELECTRON MICROSCOPY; X RAY POWDER DIFFRACTION;

HEPTANE; ISOPROPANOL; TITANIUM ISOPROPOXIDE;

TITANIUM DIOXIDE;

TITANIUM DIOXIDE;

ARTICLE; DRUG SYNTHESIS; INFRARED SPECTROPHOTOMETRY; POWDER; SURFACE PROPERTY; TEMPERATURE; THERMOGRAVIMETRY; TRANSMISSION ELECTRON MICROSCOPY; X RAY DIFFRACTION;

EID: 0031214832     PISSN: 00325910     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0032-5910(97)03250-6     Document Type: Article

References (28)

1. K.M.S. Khalil, T. Baird, M.I. Zaki, A.A. El-Samahy and A.M. Awad, Colloids Surf., (1997) in print.
2. K. Nishiwaki, N. Kakuta, A. Ueno and H. Nakabayashi, J. Catal., 118 (1989) 498.
3. S. Nishimoto, B. Ohtani, H. Kajiwara and T. Kagiya, J. Chem. Soc. Faraday Trans. 1, 81 (1985) 61.
4. K. Kohno, J. Mater. Sci., 27 (1992) 658.
5. K. Morishige, F. Kanno, S. Ogawara and S. Sasaki, J. Phys. Chem., 89 (1985) 4404.
6. H.Y. Ha, S.W. Nam, T.H. Lim, I.H. Oh and S.A. Hong, Membrane Sci., 111 (1996) 81.
7. D.C.M. Dutoit, M. Schneider and A. Baiker, J. Catal., 153 (1995) 165.
8. R. Hutter, T. Mallat and A. Baiker, J. Catal., 157 (1995) 665.
9. J.H. Kwak, S.J. Cho and R. Ryoo, Catal. Lett., 37 (1996) 217.
10. B. Lantelme, M. Dumon, C. Mai and J.P. Pascault, J. Non-Cryst. Solids, 194 (1996) 63.
11. C. Sanchez, J. Livage, M. Henry and F. Babonneau, J. Non-Cryst. Solids, 100 (1988) 65.
12. M.I. Zaki, B. Vielhaber and H. Knözinger, J. Phys. Chem., 90 (1986) 3176.
13. J,V. Smith (ed.), X-ray Powder Data File, American Society for Testing and Materials (ASTM), Philadelphia, PA, 1960.
14. International Union of Pure and Applied Chemistry, IUPAC, Pure Appl. Chem., 57 (1985) 603.
15. B. Brunauer, P.H. Emmett and E. Teller, J. Am. Chem. Soc., 60 (1938) 309.
16. C. Orr and J.M. Dalla Valle, Fine Particles Measurement, Macmillan, New York, 1959, p. 271.
17. S.J. Gregg and K.S.W. Sing, Adsorption, Surface Area and Porosity, Academic Press, London, 1982.
18. K.S.W. Sing, in J.M. Thomas and R.M. Lambert (eds.), Characterization of Catalysts, Wiley, New York, 1980, p.12.
19. S.A.A. Mansour, G.A.M. Hussein and M.I. Zaki, Thermochim. Acta, 150 (1989) 153.
20. K. Nakamoto, Infrared and Roman Spectra of Inorganic and Coordination Compounds, Wiley, New York, 3rd edn., 1978, pp. 132-135.
21. J.A. Gadsden, Infrared Spectra of Minerals and Related Inorganic Compounds, Butterworths, London, 1975, p.15.
22. H. Schmidt, J. Non-Cryst. Solids, 100 (1988) 51.
23. C.J. Brinker and G.W. Scherer, Sol-Gel Science, The Physics and Chemistry of Sol-Gel Processing, Academic Press, London, 1990, p. 20.
24. G.W. Scherer and J.C. Luong, J. Non-Cryst. Solids, 63 (1984) 163.
25. G. Feat and N. Levine, J. Colloid Interface Sci., 54 (1976) 34.
26. M.T. Harris, R.R. Brunson and C.H. Byers, J. Non-Cryst. Solids, 121 (1990) 397.
27. J. Ragai, Chem. Tech. Biotechnol. A, 35 (1985) 263.
28. C.J. Brinker and D.M. Haaland, J. Am. Ceram. Soc., 66 (1983) 758.