Synthesis and structural characterisation of a novel tris-methylene bridged compound (NO)4Fe2Se(μ-CH2)3

Journal of Organometallic Chemistry

Volumn 540, Issue 1-2, 1997, Pages 165-168

  Mathur, Pradeep ^a   Bala, Manimaran ^a   Hossain, Md Munkir ^a   Rheingold, Arnold L ^b   Liable Sands, Louise M ^b   Yap, Glenn P A ^b  

^a INDIAN INSTITUTE OF TECHNOLOGY BOMBAY   (India)

^b UNIVERSITY OF DELAWARE   (United States)

Author keywords

Alkylidene clusters; Chalcogen

Indexed keywords

EID: 0031206066     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(97)00134-4     Document Type: Article

References (37)

1. [1] K.H. Whitmire, J. Coord. Chem. 17 (1988) 95; L. Linford, H.G. Raubenheimer, Adv. Organomet. Chem. 32 (1991) 1; N.A. Compton, R.J. Errington, N.C. Norman, Adv. Organomet. Chem. 31 (1990) 91.
2. [1] K.H. Whitmire, J. Coord. Chem. 17 (1988) 95; L. Linford, H.G. Raubenheimer, Adv. Organomet. Chem. 32 (1991) 1; N.A. Compton, R.J. Errington, N.C. Norman, Adv. Organomet. Chem. 31 (1990) 91.
3. [1] K.H. Whitmire, J. Coord. Chem. 17 (1988) 95; L. Linford, H.G. Raubenheimer, Adv. Organomet. Chem. 32 (1991) 1; N.A. Compton, R.J. Errington, N.C. Norman, Adv. Organomet. Chem. 31 (1990) 91.
4. [2] D. Seyferth, G.B. Womack, Organometallics 5 (1986) 2360; D. Seyferth, G.B. Womack, R.S. Henderson, M. Cowie, B.M. Hames, Organometallics 5 (1986) 1568; D. Seyferth, R.S. Henderson, L.-C. Song, G.B. Womack, J. Organomet. Chem. 292 (1985) 9.
5. [2] D. Seyferth, G.B. Womack, Organometallics 5 (1986) 2360; D. Seyferth, G.B. Womack, R.S. Henderson, M. Cowie, B.M. Hames, Organometallics 5 (1986) 1568; D. Seyferth, R.S. Henderson, L.-C. Song, G.B. Womack, J. Organomet. Chem. 292 (1985) 9.
6. [2] D. Seyferth, G.B. Womack, Organometallics 5 (1986) 2360; D. Seyferth, G.B. Womack, R.S. Henderson, M. Cowie, B.M. Hames, Organometallics 5 (1986) 1568; D. Seyferth, R.S. Henderson, L.-C. Song, G.B. Womack, J. Organomet. Chem. 292 (1985) 9.
7. [3] P. Mathur, D. Chakrabarty, Md.M. Hossain, R.S. Rashid, J. Organomet. Chem. 420 (1991) 79; P. Mathur, D. Chakrabarty, Md.M. Hossain, J. Organomet. Chem. 401 (1991) 167; P. Mathur, P. Sekar, C.V.V. Satyanarayana, M.F. Mahon, Organometallics 14 (1995) 2115.
8. [3] P. Mathur, D. Chakrabarty, Md.M. Hossain, R.S. Rashid, J. Organomet. Chem. 420 (1991) 79; P. Mathur, D. Chakrabarty, Md.M. Hossain, J. Organomet. Chem. 401 (1991) 167; P. Mathur, P. Sekar, C.V.V. Satyanarayana, M.F. Mahon, Organometallics 14 (1995) 2115.
9. [3] P. Mathur, D. Chakrabarty, Md.M. Hossain, R.S. Rashid, J. Organomet. Chem. 420 (1991) 79; P. Mathur, D. Chakrabarty, Md.M. Hossain, J. Organomet. Chem. 401 (1991) 167; P. Mathur, P. Sekar, C.V.V. Satyanarayana, M.F. Mahon, Organometallics 14 (1995) 2115.
10. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
11. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
12. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
13. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
14. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
15. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
16. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
17. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
18. [4] R.C. Brady, R. Pettit, J. Am. Chem. Soc. 102 (1980) 6181; R.H. Grubbs, in G. Wilkinson, F.G.A. Stone, E.W. Abel (Eds.), Comprehensive Organometallic Chemistry, vol. 9, Pergamon Press, Oxford, 1982, Chap. 54, p. 499; L.R. Gilliom, R.H. Grubbs, J. Am. Chem. Soc. 108 (1986) 733; W.J. Feast, V.C. Gibson, K.J. Ivin, A.M. Kenwright, E. Khosravi, J. Chem. Soc., Chem. Commun. (1994) 1399; T.J. Katz, S.J. Lee, J. Am. Chem. Soc. 102 (1980) 422; A.F. Dyke, S.A.R. Knox, P.J. Naish, G.E. Taylor, J. Chem. Soc., Chem. Commun. (1980) 203; M. Brookhart, J.R. Tucker, G.R. Hush, J. Am. Chem. Soc. 105 (1983) 258; L.F. Cannizo, R.H. Grubbs, J. Org. Chem. 50 (1985) 2316; L.E. Clawson, S.L. Buchwald, R.H. Grubbs, J. Am. Chem. Soc. 25 (1984) 5733.
19. [5] C. Zheng, Y. Apeloig, R. Hoffmann, J. Am. Chem. Soc. 110 (1988) 749; C.P. Casey, J.D. Audett, Chem. Rev. 86 (1986) 339; J.E. Hahn, Progr. Inorg. Chem. 31 (1984) 205.
20. [5] C. Zheng, Y. Apeloig, R. Hoffmann, J. Am. Chem. Soc. 110 (1988) 749; C.P. Casey, J.D. Audett, Chem. Rev. 86 (1986) 339; J.E. Hahn, Progr. Inorg. Chem. 31 (1984) 205.
21. [5] C. Zheng, Y. Apeloig, R. Hoffmann, J. Am. Chem. Soc. 110 (1988) 749; C.P. Casey, J.D. Audett, Chem. Rev. 86 (1986) 339; J.E. Hahn, Progr. Inorg. Chem. 31 (1984) 205.
22. [6] P. Mathur, V.D. Reddy, J. Organomet. 387 (1990) 193; P. Mathur, V.D. Reddy, R. Bohra, J. Organomet. Chem. 401 (1991) 339; P. Mathur, V.D. Reddy, K. Das, U.C. Sinha, J. Organomet. Chem. 409 (1991) 255; P. Mathur, B. Manimaran, Md.M. Hossain, R. Shanbag, J. Murthy, I.S. Saranathan, C.V.V. Satyanarayana, M.M. Bhadbhade, J. Organomet. Chem. 490 (1995) 173; P. Mathur, B. Manimaran, Md.M. Hossain, C.V.V. Satyanarayana, V.G. Puranik, S.S. Tavale, J. Organomet. Chem. 493 (1995) 251.
23. [6] P. Mathur, V.D. Reddy, J. Organomet. 387 (1990) 193; P. Mathur, V.D. Reddy, R. Bohra, J. Organomet. Chem. 401 (1991) 339; P. Mathur, V.D. Reddy, K. Das, U.C. Sinha, J. Organomet. Chem. 409 (1991) 255; P. Mathur, B. Manimaran, Md.M. Hossain, R. Shanbag, J. Murthy, I.S. Saranathan, C.V.V. Satyanarayana, M.M. Bhadbhade, J. Organomet. Chem. 490 (1995) 173; P. Mathur, B. Manimaran, Md.M. Hossain, C.V.V. Satyanarayana, V.G. Puranik, S.S. Tavale, J. Organomet. Chem. 493 (1995) 251.
24. [6] P. Mathur, V.D. Reddy, J. Organomet. 387 (1990) 193; P. Mathur, V.D. Reddy, R. Bohra, J. Organomet. Chem. 401 (1991) 339; P. Mathur, V.D. Reddy, K. Das, U.C. Sinha, J. Organomet. Chem. 409 (1991) 255; P. Mathur, B. Manimaran, Md.M. Hossain, R. Shanbag, J. Murthy, I.S. Saranathan, C.V.V. Satyanarayana, M.M. Bhadbhade, J. Organomet. Chem. 490 (1995) 173; P. Mathur, B. Manimaran, Md.M. Hossain, C.V.V. Satyanarayana, V.G. Puranik, S.S. Tavale, J. Organomet. Chem. 493 (1995) 251.
25. [6] P. Mathur, V.D. Reddy, J. Organomet. 387 (1990) 193; P. Mathur, V.D. Reddy, R. Bohra, J. Organomet. Chem. 401 (1991) 339; P. Mathur, V.D. Reddy, K. Das, U.C. Sinha, J. Organomet. Chem. 409 (1991) 255; P. Mathur, B. Manimaran, Md.M. Hossain, R. Shanbag, J. Murthy, I.S. Saranathan, C.V.V. Satyanarayana, M.M. Bhadbhade, J. Organomet. Chem. 490 (1995) 173; P. Mathur, B. Manimaran, Md.M. Hossain, C.V.V. Satyanarayana, V.G. Puranik, S.S. Tavale, J. Organomet. Chem. 493 (1995) 251.
26. [6] P. Mathur, V.D. Reddy, J. Organomet. 387 (1990) 193; P. Mathur, V.D. Reddy, R. Bohra, J. Organomet. Chem. 401 (1991) 339; P. Mathur, V.D. Reddy, K. Das, U.C. Sinha, J. Organomet. Chem. 409 (1991) 255; P. Mathur, B. Manimaran, Md.M. Hossain, R. Shanbag, J. Murthy, I.S. Saranathan, C.V.V. Satyanarayana, M.M. Bhadbhade, J. Organomet. Chem. 490 (1995) 173; P. Mathur, B. Manimaran, Md.M. Hossain, C.V.V. Satyanarayana, V.G. Puranik, S.S. Tavale, J. Organomet. Chem. 493 (1995) 251.
27. [7] P. Mathur, B. Manimaran, R. Trivedi, Md.M. Hossain, M. Arabatti, J. Organomet. Chem. 515 (1996) 155.
28. [8] W.A. Herrmann, I. Bernal, Angew. Chem., Int. Ed. Engl. 16 (1977) 172.
29. [9] A.I. Vogel, Textbook of Practical Organic Chemistry, ELBS, Longman, 4th ed., 1984.
30. [10] P. Mathur, D. Chakrabarty, Md.M. Hossain, R.S. Rashid, V. Rugmini, A.L. Rheingold, Inorg. Chem. 31 (1992) 1106.
31. [11] P. Mathur, R. Trivedi, Md.M. Hossain, S.S. Tavale, V.G. Puranik, J. Organomet. Chem. 491 (1995) 291.
32. [12] P. Mathur, Md.M. Hossain, Organometallics 12 (1993) 2398.
33. [13] P. Mathur, Md.M. Hossain, K. Das, U.C. Sinha, J. Chem. Soc., Chem. Commun. (1993) 46.
34. [14] P. Mathur, Md.M. Hossain, S. Umbarkar, C.V.V. Satyanarayana, V.G. Puranik, J. Organomet. Chem. 506 (1996) 313.
35. [15] P. Mathur, B. Manimaran, C.V.V. Satyanarayana, B. Varghese, J. Organomet. Chem. 527 (1997) 83.
36. [16] V.W. Day, D.A. Lesch, T.B. Rauchfuss, J. Am. Chem. Soc. 104 (1982) 1290.
37. [17] R.A. Andersen, R.A. Jones, G. Wilkinson, M.B. Hursthouse, K.M.A. Malik, J. Chem. Soc., Chem. Commun. (1977) 865.