Identification of cyclopentenyl fatty acids by 1H and 13C nuclear magnetic resonance

JAOCS, Journal of the American Oil Chemists' Society

Volumn 74, Issue 6, 1997, Pages 727-730

  Blaise, Pierre ^a   Farines, Marie ^a   Soulier, Jacques ^a  

^a UNIVERSITÉ DE PERPIGNAN   (France)

Author keywords

2D NMR; 1H and 13C NMR; Chaulmoogric acid; Flacourtiaceae; Gorlic acid; HPLC; Hydnocarpic acid; Hydnocarpus seed oil; Identification; TLC Ag+

Indexed keywords

FLACOURTIACEAE; HYDNOCARPUS;

AROMATIC COMPOUNDS; ESTERS; GAS CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIPIDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; THIN LAYER CHROMATOGRAPHY; VEGETABLE OILS;

CHAULMOOGRIC ACID; GORLIC ACID; HYDNOCARPIC ACID; HYDNOCARPUS SEED OIL;

FATTY ACIDS;

EID: 0031165565     PISSN: 0003021X     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11746-997-0209-7     Document Type: Article

References (16)

1. Badami, R.C., and K.B. Patil, Structure and Occurrence of Unusual Fatty Acids in Minor Seed Oils, Prog. Lipids Res. 19:119-153 (1981).
2. Ucciani, E., Nouveau Dictionnaire des Huiles Végétales, edn. Lavoisier, Paris. 1995, p. 273.
3. Mangold, H.K., and F. Spener, in Lipids and Lipid Polymers in Higher Plants, edited by M. Teveni and H.K. Lichtenthaler, Springer-Verlag, Berlin, 1977, p. 85.
4. Abdel-Moety, E.M., Cyclopentenyl Fatty Acids as Starting Materials for Preparing New Active Substances, Fette Seifen Anstrichm. 83:65-70 (1981).
5. Christie, W.W., E.Y. Brecany, and V.K.S. Shukla, Analysis of Seed Oils Containing Cyclopentenyl Fatty Acids by Combined Chromatographic Procedures, Lipids 24:116-120 (1989).
6. Christie, W.W., D. Rebello, and R.T. Holman, Mass Spectrometry of Derivatives of Cyclopentenyl Fatty Acids, Ibid. 4:229-231 (1969).
7. Zhang, J.Y., H.Y. Wang, Q.T. Yu, X.J. Yu, B.N. Liu, and Z.H. Huang, The Structures of Cyclopentenyl Fatty Acids in the Seed Oils of Flacourtiaceae Species by GC-MS of Their 4,4-Dimethyloxazoline Derivatives, Ibid. 66:242-246 (1989).
8. Shukla, V.K.S., E.M. Abdel-Moety, E. Larsen., and H. Egsgaard, Identification of Cyclopentenyl Fatty Acids by Gas-Liquid Chromatography and Mass Spectrometry, Chem. Phys. Lipids 25:285-290 (1979).
9. 13C NMR Spectroscopy of Lipids, in Advances in Lipid Methodology - Two, edited by W.W. Christie, The Oily Press, Dundee, 1993, pp. 1-28.
10. 13C NMR Spectroscopy, in New Trends in Lipids and Lipoprotein Analysis, edited by J.L. Sebedio and E.G. Perkins, AOCS Press, Champaign, 1995, pp. 250-264.
11. Cecchi, G., S. Biasini, and J. Castano, Methanolyse Rapide des Huiles en Solvant, Rev. Fr. Corps Gras 32:163-164 (1985).
12. Aubert-Mammou, C., M. Magliozzi, M. Farines, and J. Soulier, Les Triacylglycérols de l'Huile de Graines de Sysimbre (Sysimbrium sp. L., Brassicaceae), Oleagineux Corps Gras Lipides 3:65-69 (1996).
13. 13C Nuclear Magnetic Resonance of the Olefinic and Carbonyl Carbons of Edible Vegetable Oils, J. Am. Oil Chem. Soc. 67:487-494 (1990).
14. 13C Nuclear Magnetic Resonance Spectroscopy, Ibid. 72:293-297 (1995).
15. 13C NMR. A Technique for the Study of Lipid Structure and Composition, Prog. Lipid Res. 33:19-28 (1994).
16. 13C NMR, in Lipid Analysis. A Practical Approach, edited by R.J. Hamilton and S. Hamilton, OIRL Press, Oxford, 1992, pp. 243-262.