Room-temperature synthesis of silicate mesoporous MCM-41-type materials: Influence of the synthesis pH on the porosity of the materials obtained

Microporous Materials

Volumn 10, Issue 1-3, 1997, Pages 137-147

  Voegtlin, A C ^a   Matijasic, A ^a   Patarin, J ^a   Sauerland, C ^b   Grillet, Y ^b   Huve, L ^c  

^a CNRS   (France)

^b du 141eme RIA   (France)

^c Centre de Recherche de Grand Couronne   (France)

Author keywords

29Si MAS NMR spectroscopy; Ar adsorption; Isothermal microcalorimetry; MCM 41 materials; N2 adsorption; Synthesis

Indexed keywords

AMORPHIZATION; CALCINATION; CALORIMETRY; CONDENSATION; GAS ADSORPTION; HEAT TREATMENT; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PH EFFECTS; POROSITY; POROUS MATERIALS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

ISOTHERMAL MICROCALORIMETRY; MESOPOROUS MATERIALS; POLYCONDENSATION;

SILICA;

EID: 0031165389     PISSN: 09276513     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0927-6513(97)00003-5     Document Type: Article

References (26)

1. C.T. Kresge, M.E. Leonowicz, W.J. Roth, J.C. Vartuli, J.S. Beck, Nature 359 (1992) 710
2. J.S. Beck, J.C. Vartuli, W.J. Roth, M.E. Leonowicz, C.T. Kresge, K.D. Schmitt, C.T.W. Chu, D.H. Olson, E.W. Sheppard, S.B. McCullen, J.B. Higgins, J.L. Schlenker, J. Am. Chem. Soc. 114 (1992) 10834
3. A. Monnier, F. Schüth, Q. Huo, D. Kumar, D. Margolese, R.S. Maxwell, G.D. Stucky, M. Krishnamurty, P. Petroff, A. Firouzi, M. Janicke, B.F. Chmeka, Science 261 (1993) 1299
4. K.J. Edler and J.W. White, J. Chem. Soc., Chem. Commun., (1995) 155.
5. C.Y. Chen, S.L. Burkett, H.X. Li, M.E. Davis, Microporous Mater. 2 (1993) 27
6. A. Matijasic, A.C. Voegtlin, J. Patarin, J.L. Guth and L. Huve, J. Chem. Soc., Chem. Commun., (1996) 1123.
7. R. Schmidt, M. StÖcker, E. Hansen, D. Akporiaye, O.H. Ellestad, Microporous Mater. 3 (1995) 443
8. J. Rouquerol, J. Thermochim. Acta 144 (1989) 209
9. M. Boudellal, PhD Thesis, Université de Provence Aix Marseille I, Marseille, France, 1979.
10. Y. Grillet, F. Rouquerol, J. Rouquerol, J. Chim. Phys. 74 (1977) 179
11. Y. Grillet, F. Rouquerol, J. Rouquerol, J. Chim. Phys. 7-8 (1977) 778
12. J.H. de Boer, in D.H. Everett and F.S. Stone (Eds.), The Structure and Properties of Porous Materials, Butterworths, London, 1958, p. 68.
13. S.J. Gregg and K.S.W. Sing, Adsorption, Surface Area and Porosity, Academic Press, London, 1982.
14. E.P. Barrett, L.G. Joyner, P.H. Halenda, J. Am. Chem. Soc. 73 (1951) 373
15. A.C. Voegtlin, F. Ruch, J.L. Guth, J. Patarin and L. Huve, Microporous Mater., in press.
16. S. Brunauer, P.H. Emmett, E. Teller, J. Am. Chem. Soc. 60 (1938) 309
17. L. Gurvitsch, J. Phys. Chem. Soc. Russ. 47 (1915) 805
18. K.S.W. Sing, D.H. Everett, R.A.W. Haul, L. Moscou, R.A. Pierotti, J. Rouquerol, T. Siemieniewska, Pure Appl. Chem. 57 (1985) 603
19. K.S.W. Sing, J. Porous Mater. 2 (1995) 5
20. P.J.M. Carrott and K.S.W. Sing, in K.K. Unger, J. Rouquerol, K.S.W. Sing and H. Kral (Eds.), Characterization of Porous Solids, Stud. Surf. Sci. Catal., Vol. 39, Elsevier, Amsterdam, 1988, p. 77.
21. K.S.W. Sing, Chemistry and Industry, 1967, p. 829.
22. M.J. Torralvo, Y. Grillet, F. Rouquerol, J. Rouquerol, J. Chim. Phys. 77 (2) (1980) 125
23. P.L. Llewellyn, Y. Grillet, J. Patarin, A.C. Faust, Microporous Mater. 1 (1993) 247
24. J. Rouquerol, F. Rouquerol, C. Peres, Y. Grillet, M. Boudellal, in S.J. Gregg, K.S.W. Sing and H.F. Stoekli, (Eds.), Characterization of Porous Solids, Society of Chemical Industry, London, 1979, p. 107.
25. A.V. Kiselev, Disc. Faraday 40 (1965) 205
26. D. Atkinson, P.J.M. Carrott, Y. Grillet, J. Rouquerol and K.S.W. Sing, in A.I. Liapis, D.H. Everett and K.S.W. Sing, (Eds.), Fundamentals of Adsorption, Engineering Foundation, New York, 1987 p. 89.