Direct on-line coupling of capillary HPLC with 1H NMR spectroscopy for the structural determination of retinyl acetate dimers: 2D NMR spectroscopy in the nanoliter scale

Analytical Chemistry

Volumn 69, Issue 7, 1997, Pages 1421-1425

  Schlotterbeck, Götz ^a   Tseng, Li Hong ^a   Händel, Heidrun ^a   Braumann, Ulrich ^b   Albert, Klaus ^a  

^a UNIVERSITY OF TÜBINGEN   (Germany)

^b Bruker Analytik GmbH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ESTERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOMERIZATION; MIXTURES; MOLECULAR STRUCTURE; SPECTROSCOPIC ANALYSIS;

KITOLS; ONE DIMENSIONAL; RETINYL ACETATE DIMERS; TWO DIMENSIONAL;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

RETINOL ACETATE;

ARTICLE; DIMERIZATION; DRUG STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MICROANALYSIS; NUCLEAR MAGNETIC RESONANCE; TECHNIQUE;

EID: 0031127896     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac960902b     Document Type: Article

References (20)

1. Hatada, K.; Ute, K.; Kitayama, T.; Nishimura, T.; Kashiyama, M.; Fujimoto, N. Polym. Bull. 1990, 23, 549-554.
2. Albert, K.; Braumann, U.; Streck, R.; Spraul, M.; Ecker, R. Fresenius' J. Anal. Chem. 1995, 352, 521-528.
3. Sidelmann, U. G.; Gavaghan, C.; Carless, H. A. J.; Spraul, M.; Hoffmann, M.; Lindon, J. C.; Wilson, I. D.; Nicolson, J. K. Anal. Chem. 1995, 67, 4441-4445.
4. Spraul, M.; Hofmann, M.; Dvortsak, P.; Nicholson, J. K.; Wilson, I. D. Anal. Chem. 1993, 65, 327-330.
5. Albert, K.; Schlotterbeck, G.; Braumann, U.; Händel, H.; Spraul, M.; Krack, G. Angew. Chem., Int. Ed. Engl. 1995, 34, 1014-1016.
6. Pursch, M.; Strohschein, S.; Händel, H.; Albert, K. Anal. Chem. 1996, 68, 386-393.
7. Albert, K.; Bayer, E. HPLC Detection Newer Methods; VCH: New York, 1992; pp 197-229.
8. Albert, K. J. Chromatogr. A 1995, 703, 123-147.
9. Behnke, B.; Schlotterbeck, G.; Tallarek, U.; Strohschein, S.; Tseng, L. H.; Keller, T.; Albert, K.; Bayer, E. Anal. Chem. 1996, 68, 1110-1115.
10. Wu, N.; Peck, T. L.; Webb, A. G.; Magin, R. L.; Sweedler, J. V. Anal. Chem. 1994, 66, 3849-3857.
11. Peck, T. L.; Magin, R. L.; Lauterbur, P. C. J. Magn. Reson. B 1995, 108, 114-124.
12. Wu, N.; Peck, T. L.; Webb, A. G.; Magin, R. L.; Sweedler, J. V. J. Am. Chem. Soc. 1994, 116, 7929-7930.
13. Olson, D. L.; Peck, T. L.; Webb, A. G.; Magin, R. L.; Sweedler, J. V. Science 1995, 270, 1967-1969.
14. Pritchard, H.; Wilkinson, H.; Edisbury, J. R.; Morton, R. A. Biochem. J. 1937, 31, 258-265.
15. Burger, B. V.; Garbers, C. F. J. Chem. Soc., Perkin Trans. 1 1973, 590-595.
16. Mousseron-Canet, J. C. Bull. Soc. Chim. Fr. 1966, 3043-3044.
17. Pfoertner, K. H.; Englert, G.; Schoenholzer, P. Tetrahedron 1988, 44, 1039-1052.
18. Mousseron-Canet, M.; Lerner, D.; Mani, J. C. Bull. Soc. Chim. Fr. 1968, 4639-4645.
19. Tsukida, K.; Ito, M. J. Nutr. Sci. Vitaminol. 1980, 26, 319-322.
20. Albert, K.; Schlotterbeck, G.; Tseng, L. H.; Braumann, U. J. Chromatogr. A 1996, 750, 303-309.