Mass spectrometric identification of Si-O-H(g) species from the reaction of silica with water vapor at atmospheric pressure

Journal of the American Ceramic Society

Volumn 80, Issue 4, 1997, Pages 1009-1012

  Opila, Elizabeth J ^a,b,c   Fox, Dennis S ^a,b   Jacobson, Nathan S ^a,b  

^a NASA GLENN RESEARCH CENTER   (United States)

^b AMERICAN CERAMIC SOCIETY   (United States)

^c CLEVELAND STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ATMOSPHERIC PRESSURE; HIGH TEMPERATURE EFFECTS; HYDRIDES; IONS; MASS SPECTROMETRY; OXYGEN; PRESSURE EFFECTS; VAPOR PRESSURE; VAPORS;

FRAGMENT IONS;

SILICA;

EID: 0031117473     PISSN: 00027820     EISSN: None     Source Type: Journal    
DOI: 10.1111/j.1151-2916.1997.tb02935.x     Document Type: Article

References (19)

1. G. W. Morey and J. M. Hesselgesser, "The Solubility of Quartz and Some Other Substances in Superheated Steam at High Pressures," Trans. ASME, 865-75 (1951).
2. G. R. B. Elliot, "Gaseous Hydrated Oxides, Hydroxides, and Other Hydrated Molecules," UCRL-1831, University of California, Berkeley, CA, June, 1952.
3. E. L. Brady, "Chemical Nature of Silica Carried by Steam," J. Phys. Chem., 57, 706-10 (1953).
4. O. Glemser and H. G. Wendlandt, "Gaseous Hydroxides"; pp. 215-58 in Advances in Inorganic Chemistry and Radiochemistry, Vol. 5. Academic Press, New York, 1963.
5. O. H. Krikorian, "Thermodynamics of the Silica-Steam System"; p. 481 in Symposium on Engineering with Nuclear Explosives (Las Vegas, NV, January 14-16, 1970), Vol. 1, unpublished.
6. M. C. Cheng and I. B. Cutler, "Vaporization of Silica in Steam Atmosphere," J. Am. Ceram. Soc., 62 [11-12] 593-96 (1979).
7. 2O Gas on Volatilities of Planet-Forming Major Elements: I. Experimental Determination of Thermodynamic Properties of Ca-, Al-, and Si-Hydroxide Gas Molecules and Its Application to the Solar Nebula," Geochim. Cosmochim. Acta, 56, 511-32 (1992).
8. 2," J. Chem. Phys., 101 [7] 6076-79 (1994).
9. C. A. Stearns, F. J. Kohl, G. C. Fryburg, and R. A. Miller; pp. 303-55 in NBS Special Publication, No. 561, Characterization of High Temperature Vapors and Gases. National Bureau of Standards, Washington, DC, 1978.
10. 2O and Gaseous NaCl," J. Electrochem. Soc., 124 [11] 1738-43 (1977).
11. N. S. Jacobson, M. J. McNallan, and Y. Y. Lee, "Mass Spectrometric Observations of Metal Oxychlorides Produced by Oxidation-Chlorination Reactions," Metall. Trans. A, 17A, 1223-28 (1986).
12. N. S. Jacobson, "Application of an Atmospheric Pressure Sampling Mass Spectrometer to Chlorination Reactions," NASA TM-87270, 1986.
13. R. C. Weast (Ed.), CRC Handbook of Chemistry and Physics, 60th ed.; p. D-196. CRC Press, Boca Raton, FL, 1979-80.
14. J. E. Marra, E. R. Kreidler, N. S. Jacobson, and D. S. Fox, "Reactions of Silicon-Based Ceramics in Mixed Oxidation Chlorination Environments," J. Am. Ceram. Soc., 71 [12] 1067-73 (1988).
15. J. E. Marra, E. R. Kreidler, N. S. Jacobson, and D. S. Fox, "Direct Mass Spectrometric Identification of Silicon Oxychloride Compounds," J. Electrochem. Soc., 135 [6] 1571-74 (1988).
16. R. T. Grimley, "Mass Spectrometry"; pp. 195-243 in The Characterization of High-Temperature Vapors. Edited by J. L. Margrave. Wiley, New York, 1967.
17. H. M. Rosenstock, K. Draxl, B. W. Steiner, and J. T. Herron, Journal of Physical and Chemical Reference Data, Vol. 6, Supplement 1, Energetics of Gaseous Ions. American Chemical Society and American Institute for Physics, New York, 1977.
18. O. H. Krikorian, "Predictive Calculations of Volatilities of Metals and Oxides in Steam-Containing Environments," High Temp. - High Pressures, 14, 387-97 (1982).
19. E. J. Opila and R. E. Hann, "Paralinear Oxidation of CVD SiC in Water Vapor," J. Am. Ceram. Soc., 80 [1] 197-205 (1997).