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0343011079
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note
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2 in ether at room temperature afforded a complex mixture.
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11
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0342576813
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note
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The d.e.'s of 6 and 7 were determined by capillary GLC (OV-1, 25 m). The authentic samples of the mixtures of their diastereomers were synthesized from the corresponding racemic ketones and PD.
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12
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3242857105
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For a review of asymmetric cyclopropanation reactions using chiral metal catalysts, see: Pfaltz, A., Acc. Chem. Res. 1993, 26, 339. For some recent examples of asymmetric cyclopropanations of olefins and diazo compounds using chiral metal catalysts, see:
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Pfaltz, A.1
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For reviews, see: (a) Reissig, H.-U., Topics in Current Chemistry', Springer-Verlag, Berlin-Heidelberg, 1988, vol. 144, pp. 73-135.
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