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3
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0001674261
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Cason, J.; Rinehart, K. L., Jr.; Thornton, S. D., Jr. J. Org. Chem. 1953, 18, 1594.
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(1953)
J. Org. Chem.
, vol.18
, pp. 1594
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Cason, J.1
Rinehart K.L., Jr.2
Thornton S.D., Jr.3
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9
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0343874529
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Lhommet, G.; Eskenazi, C.; Maitte, P. C. R. Hebd. Seances Acad. Sci., Ser.C 1974, 279, 263.
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(1974)
C. R. Hebd. Seances Acad. Sci., Ser.C
, vol.279
, pp. 263
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Lhommet, G.1
Eskenazi, C.2
Maitte, P.3
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11
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0343874528
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The bath should be filled with water containing some 3-5% detergent. In our laboratory, we use Decon 90 which permits much more even cavitation in the bath water
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The bath should be filled with water containing some 3-5% detergent. In our laboratory, we use Decon 90 which permits much more even cavitation in the bath water.
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-
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13
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0003467672
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March, John Wiley & Sons: New York
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March, J. Advanced Organic Chemistry, 4th ed., John Wiley & Sons: New York, 1992, 931. The formation and structure of the condensation compound is described and shown on this page.
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(1992)
Advanced Organic Chemistry, 4th Ed.
, vol.931
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-
March, J.1
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15
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0000512023
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Rieke, R. D.; Li, P. T. -J.; Burns, T. P.; Uhm, S. T. J. Org. Chem. 1981, 46, 4323.
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(1981)
J. Org. Chem.
, vol.46
, pp. 4323
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-
Rieke, R.D.1
Li, P.T.-J.2
Burns, T.P.3
Uhm, S.T.4
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18
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0000989934
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Petrier, C.; de Souza Barbosa, J. C.; Dupuy, C.; Luche, J. -L. J. Org. Chem. 1985, 50, 5761.
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(1985)
J. Org. Chem.
, vol.50
, pp. 5761
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Petrier, C.1
De Souza Barbosa, J.C.2
Dupuy, C.3
Luche, J.-L.4
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19
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0000916741
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Petrier, C.; Luche, J. -L.; Dupuy, C. Tetrahedron Lett. 1984, 25, 3463.
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(1984)
Tetrahedron Lett.
, vol.25
, pp. 3463
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Petrier, C.1
Luche, J.-L.2
Dupuy, C.3
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22
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0842340096
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Gaudmear, M.; Burgi, A. E.; Baccar, B. J. Organomet. Chem. 1985, 280, 165.
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(1985)
J. Organomet. Chem.
, vol.280
, pp. 165
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Gaudmear, M.1
Burgi, A.E.2
Baccar, B.3
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25
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0000870115
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Yeh, M. C. P.; Chen, H. G.; Knochel, P. Org. Synth. 1991, 70, 195.
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(1991)
Org. Synth.
, vol.70
, pp. 195
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Yeh, M.C.P.1
Chen, H.G.2
Knochel, P.3
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26
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0343874526
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note
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A solution of zinc (5.0 mmol), 1,2-dibromoethane (1.1 mmol), acetonitrile (1.0 mmol) and ethyl bromoacetate (1.2 mmol) in 4 mL dry THF was sonicated for two hours and the major product was a self-condensation compound as well as the desired product which had a 15% yield.
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27
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0342568749
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1H-NMR
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1H-NMR.
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29
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0028831796
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Stadtmuller, H.; Greve, B.; Lennick, K.; Chair, A.; Knochel, P. Synthesis 1995, 69.
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(1995)
Synthesis
, vol.69
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-
Stadtmuller, H.1
Greve, B.2
Lennick, K.3
Chair, A.4
Knochel, P.5
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30
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0343874521
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note
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2 (0.5 mmol), 2-bromobenzonitrile (1.0 mmol) and ethyl bromoacetate (1.0 mmol) in 4 mL dry THF was sonicated for two hours and β-amino ester (Entry 8) was produced with a 60% yield and a small amount of self-condensation compound.
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