Steroid profiling

Annals of Clinical Biochemistry

Volumn 34, Issue 1, 1997, Pages 32-44

  Honour, John W ^a  

^a UNIVERSITY COLLEGE LONDON HOSPITALS   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

CORTICOSTERONE; HYDROCORTISONE; STEROID;

ADRENAL DISEASE; AMNION FLUID ANALYSIS; CALIBRATION; CLINICAL CHEMISTRY; COST BENEFIT ANALYSIS; GAS CHROMATOGRAPHY; HUMAN; LABORATORY TEST; MASS SPECTROMETRY; METHODOLOGY; PRIORITY JOURNAL; QUALITY CONTROL; REVIEW; STEROID ANALYSIS; STEROID BLOOD LEVEL; STEROID METABOLISM; STEROID URINE LEVEL;

EID: 0031022902     PISSN: 00045632     EISSN: None     Source Type: Journal    
DOI: 10.1177/000456329703400106     Document Type: Review

References (49)

1. Honour JW, Brook CGD. Clinical indications for the use of urinary steroid profiles in neonates and childhood. Ann Clin Biochem 1997; 34: 45-54 [this issue]
2. Wudy SA, Wachter UA, Homoki J, Teller WM. Androgen metabolism assessment by routine gas chromatography/mass spectrometry profiling of plasma steroids: Part 1. Unconjuaated steroids. Steroids 1992; 57: 319-24
3. Saenger P, Klonari Z, Black SM, Compagne N, Mellon SH, Fleischer A, et al. Prenatal diagnosis of lipoid congenital adrenal hyperplasia. J Clin Endocr Metab 1995; 80: 200-5
4. Honour JW, Tourniaire J, Biglieri EG, Shackleton CHL. Urinary steroid excretion in 17-hydroxylase deficiency. J Steroid Biochem 1987; 9: 495-505
5. Homoki J, Roitman E, Shackleton CHL. Characterization of the major steroids present in amniotic fluid obtained between the 15th and 17th weeks of gestation. J Steroid Biochem 1983; 19: 1060-8
6. Vestergaard P, Sayegh JF, Mowat JH, Hemmingsen L. Estimation after multi-column chromatography of common urinary neutral steroids with an application to the assay of 17-oxosteroids. Acta endocrinol (Kbh) 1978; Suppl 217
7. Honour JW, Kelnar CJH, Brook CGD. Urine steroid excretion rates in childhood reflect growth and activity of the adrenal cortex. Acta endocrinol 1991; 124: 219-24
8. Shackleton CHL, Gustafsson J-A, Sjovall J. Identification of steroids in urine from newborn infants. Steroids 1970; 17: 265-80
9. Midgley PC. Adrenal function in preterm infants (MD thesis). University of Aberdeen, 1993
10. Wallace AM, Beesley J, Thomson M, Giles CA, Ross AM, Taylor NF. Adrenal status during the first month of life in mature and premature infants. J Endocrinol 1987; 112: 473-80
11. Taylor NF, Curnow DH, Shackleton CHL. Analysis of glucocorticosteroid metabolites in the neonatal period. Catabolism of cortisone acetate by an infant with 21-hydroxylase deficiency. Clin Chim Acta 1978; 85: 219-29
12. Kornel L. Studies on steroid conjugates. III Separation of conjugated steroids by high voltage paper electrophoresis. J Clin Endocrinol Metab 1964; 24: 956-68
13. Schoneshofer M, Dulce HJ. Comparison of different high-performance liquid chromatography systems for the purification of adrenal and gonadal steroids prior to immunoassay. J Chromatogr 1979; 164: 17-26
14. Horning EC. Gas phase analytical methods for the study of steroid hormones and their metabolites. In: Eik-Nes KB, Horning EC, eds. Gas-phase Chromatography of Steroids. New York: Springer-Verlag, 1968: 1-71
15. Shackleton CHL, Mattox VR, Honour JW. Analysis of intact steroid conjugates by secondary ion mass spectrometry (including FAB-MS) and by gas chromatography. J Steroid Biochem 1983; 19: 209-17
16. Bradlow HL. Extraction of steroid conjugates with a neutral resin. Steroids 1968; 11: 265-72
17. Bradlow HL. Modified technique for the elution of polar steroid conjugates from Amberlite XAD-2. Steroids 1977; 30: 581-2
18. Shackleton CHL, Whitney JO. Use of Sep-Pak cartridges for urinary steroid extraction. Evaluation of the method for use prior to gas chromatography analysis. Clin Chim Acta 1980; 107: 231-43
19. Shackleton CHL. Mass Spectrometry: Application in steroid and peptide research. Endocr Revs 1985; 6: 441-86
20. Shackleton CHL. Mass spectrometry in the diagnosis of steroid-related disorders and in hypertension research. J Steroid Biochem Mol Biol 1993; 45: 127-40
21. Ulick S, Chan CK, Wang JZ. Measurements of 4 urinary C-18 oxygenated corticosteroids by stable isotope dilution mass fragmentography. J Steroid Biochem 1991; 32: 33-52
22. Gaskell SJ, Pike AN, Griffiths K. Analysis of testosterone and dehydroepiandrosterone in saliva by GC-MS. Steroids 1980; 36: 219-28
23. Wong T, Shackleton CHL, Covery RT, Ellis G. Identification of the steroids in neonatal plasma that interfere with 17α-hydroxyprogesterone radioassays. Clin Chem 1992; 38: 1830-7
24. Liberato DJ, Yergey AL, Esteban N, Gomez-Sanchez CE, Shackleton CHL. Thermospray HPLC/MS: A new mass spectrometric technique for the profiling of steroids. J Steroid Biochem 1987; 27: 61-70
25. Shackleton CHL, Kletke C, Wudy S, Pratt JH. Dehydroepiandrosterone sulphate quantification using high-performance liquid chromatography/ mass spectrometry and a deuterated internal standard: a technique suitable for routine use or as a reference method. Steroids 1990; 55: 472-7
26. Esteban NV, Yergey AL, Liberato DJ, Loughlin T, Lorimer DL. Stable isotope dilution method using thermospray liquid chromatography/mass spectrometry for quantification of daily cortisol production in humans. Biomed Environ Mass Spectrom 1988; 15: 603-8
27. Shackleton CHL. Profiling steroid hormones and urinary steroids. J Chromatogr 1986; 379: 91-156
28. Axelson M, Sahlberg B-L. Group separation and GC-MS of conjugated steroids in plasma. J Steriod Biochem 1983; 18: 313-21
29. Janne O, Vihko R, Sjovall J, Sjovall K. Determination of steroid mono and disulphates in human plasma. Clin Chim Acta 1969; 23: 331-5
30. Setchell KDR, Aime B, Axelson M, Sjovall J. Multi-component analysis of conjugates of neutral steroids in urine by lipophilic ion exchange chromatography and computerised GC-MS. J Steroid Biochem 1976; 7: 615-29
31. Burstein S, Lieberman S. Hydrolysis of ketosteroid hydrogen sulfates by solvolysis procedures. J Biol Chem 1958; 233: 331-5
32. Messen G, Cugnetto G, Moneti G, Serio M. Helix pomatia induced conversion of some 3β-hydroxysteroids. J Steroid Biochem 1984; 20: 793-6
33. Setchell KDR, Shackleton CHL. The group separation of plasma and urinary steroids by column chromatography on Sephadex LH-20. Clin Chim Acta 1973; 47: 381-8
34. Thenot J-P, Horning EC. MO-TMS derivatives of human urinary steroids for GC and GC-MS studies. Analyt Lett 1972; 5: 21-33
35. Shackleton CHL, Irias J, McDonald C, Imperato-McGinley. Late-onset 21-hydroxylase deficiency: Reliable diagnosis by steroid analysis of random urine collections. Steroids 1986; 48: 239-50
36. Ellingboe J, Nystrom E, Sjovall J. Liquid gel chromatography on lipophilic-hydrophobic Sephadex derivatives. J Lipid Res 1970; 11: 266-73
37. Egerton M, Fry EE. The excretion of cortisol precursor metabolites in Cushing's syndrome. Ann Clin Biochem 1987; (suppl 24): 192-4
38. Honour JW, Shackleton CHL. Mass spectrometric analysis of tetrahydroaldosterone. J Steroid Biochem 1977; 8: 293-305
39. Shackleton CHL, Honour JW. Identification and measurement of 18-hydroxycorticosterone metabolites by GC-MS. J Steroid Biochem 1977; 8: 199-203
40. Chambaz EM, Defaye G, Madani C. Trimethylsilyl ether-enol-trimethylsilyl ethers - a new type of derivative for gas phase study of hormonal steroids. J Steroid Biochem 1973; 3: 741-7
41. Dehennin L, Matsumoto AM. Long term administration of testosterone enanthate to normal men: alterations of the urinary profile of androgen metabolites potentially useful for detection of testosterone misuse in sport. J Steroid Biochem Mol Biol 1993; 44: 179-89
42. Phillipou G, Bigham DA, Saemark RF. Steroid t-butyldimethylsilyl ethers as derivatives for mass fragmentography. Steroids 1975; 26: 516-24
43. Vrbanac JJ, Sweeley CC, Pingston JD. Automatic metabolic profiling analysis of urinary steroids by a gas chromatography mass spectrometry data system. Biomed Mass Spectrom 1983; 10: 155-61
44. Shackleton CHL, Honour JW. Simultaneous estimation of urinary steroids by semi-automated gas chromatography: Investigations of neonatal infants and children with abnormal steroid synthesis. Clin Chim Acta 1976; 69: 267-83
45. Setchell KDR, Lawson AM, Mitchell FL, Adlercreutz H, Kirk DN, Axelson M. Lignans in man and animal species. Nature 1980; 287: 740-2
46. Adlercreutz H, Fotsis T, Bannwart C, Wahala K, Brunow G, Hase T. Isotope dilution gas chromatographic-mass spectrometric method for determination of lignans and isoflavinoids in human urine including identification of genistein. Clin Chim Acta 1991; 199: 263-78
47. Weykamp CW, Penders TJ, Borbrugh AJ, van de Calseyde JE, Wolthers BJ. Steroid profile for urine. Reference values. Clin Chem 1989; 35: 2281-4
48. Shackleton CHL, Lawson AM. Steroid and bile acid analyses. In: McEwen CN, Larsen BS, eds. Mass Spectrometry of Biological Materials, New York: Marcel Dekker, 1990: 297-377
49. Catlin DH, Kammerer RC, Hatton CK, Sekera MH, Merdink JL. Analytical Chemistry at the games of the XXIIIrd Olympiad in Los Angeles 1984. Clin Chem 1987; 33: 319-27