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0343244715
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note
-
Alcohols 14 and 15 were only partially separable and the optical rotation for (+)-14 was determined on a mixture 92:8 (after purification by flash-chromatography) of (+)-14 and 15 respectively. Alcohol 15 could not be isolated pure because of its very similar Retention factor to that of (+)-14 and its low percentage in the mixture.
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23
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0003546549
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27
-
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0342375094
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-
246=-775
-
246=-775.
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-
-
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28
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0000679433
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Trujillo, M.; Morales, E. Q.; Vazquez, J. T. J. Org. Chem. 1994, 59, 6637-6642.
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29
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0343680301
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224=+2804
-
224=+2804.
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