The synthesis of 3-amidinio-2-aminopyridine-4-carboxylate

Tetrahedron Letters

Volumn 38, Issue 25, 1997, Pages 4455-4456

  Nasakin, Oleg E ^a   Sheverdov, Vladimir P ^a   Moiseeva, Inna V ^a   Lyschikov, Anatoli N ^a   Ershov, Oleg V ^a   Nesterov, Vladimir N ^b  

^a CHUVASH STATE UNIVERSITY   (Russian Federation)

^b A N NESMEYANOV INSTITUTE OF ORGANOELEMENT COMPOUNDS   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

ISONICOTINIC ACID; PYRIDINE DERIVATIVE;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; DRUG SYNTHESIS; REACTION ANALYSIS;

EID: 0031005722     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00899-X     Document Type: Article

References (11)

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2. Thorpe, J.F. J.Chem.Soc. 1905, 87, 1675.
3. Little, E.L.; Middleton, W.J.; Coffman, D.D.; Engelhardt, V.A.; Sausen, G.N. J.Am.Chem.Soc. 1958, 80, 2832-2838.
4. Carboni, R. A.; Coffman, D.D.; Howard, E.G. J.Am.Chem.Soc. 1958, 80, 2838-2840.
5. Nasakin, O.E.; Nikolaev, E.G.; Terentjev, P.B.; Bulai, A.Kh.; Khaskin, B.A.; Mikhailov, V.K. Khim.Geterotsikl.Soedin. 1984, 11, 1574.
6. Nasakin, O.E.; Nikolaev, E.G.; Terentjev, P.B.; Bulai, A.Kh.; Zakharov, V.Ya. Khim.Geterotsikl.Soedin. 1985, 9, 1225-1228.
7. Nasakin, O.E.; Nikolaev, E.G.; Terentjev, P.B.; Bulai, A.Kh.; Lavrentjeva, I.V. Khim.Geterotsikl.Soedin. 1987, 5, 653-656.
8. Middleton, W.J.; Heckert, R.E.; Little, E.L.; Krespan, C.G. J.Am.Chem.Soc. 1958, 80, 2783-2788.
9. -1): 3a; 75; 298-300; 3530-3500, 1750, 1700, 1620. 3b; 34; 229-230; 3510-3490, 1750, 1700, 1620. 3c; 62; 216-218; 3520-3500, 1760, 1700, 1600.
10. w=0.038 (S=0.55) for 1685 reflections with I>3σ(I). All the calculations were carried out using the SHELXTL PLUS program. Atomic coordinates, bond lengths and bond angles were deposited at the Cambridge Crystallographic Data Centre.
11. Blomquist, A.T.; Meinwald, Y.C. J.Am.Chem.Soc. 1959, 81, 667-672.