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note
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3 (490 mg, 2.48 mmol) and 4-fluoroaniline (141 μL, 1.49 mmol) were added successively. The mixture was stirred overnight at room temperature, then filtered and concentrated under reduced pressure. Flash chromatography on silica gel with cyclohexane/ethyl acetate : 3/1 as eluent gave 322 mg of 2 (52%). Spectral data, specific rotation, and mp agree with those in the literature. 5
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