Dehydration studies of a high-surface-area alumina (Pseudo-boehmite) using solid-state 1H and 27Al NMR

Journal of the American Chemical Society

Volumn 119, Issue 33, 1997, Pages 7832-7842

  Fitzgerald, John J ^a   Piedra, Gilberto ^a   Dec, Steven F ^b   Seger, Mark ^b   Maciel, Gary E ^b  

^a SOUTH DAKOTA STATE UNIVERSITY   (United States)

^b Department of Environmental and Radiological Health Sciences   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINUM OXIDE;

ARTICLE; CHEMICAL BOND; CHEMICAL STRUCTURE; DEHYDRATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SURFACE PROPERTY; THERMODYNAMICS;

EID: 0030986453     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja970788u     Document Type: Article

References (40)

1. Wefers, K.; Misra, C. Oxides and Hydroxides of Aluminum; Alcoa Technical Paper No. 19, Alcoa Laboratories, 1987.
2. Gitzen, W. H. Alumina as a Ceramic Material; The American Ceramic Society: Columbus, OH, p 15.
3. Walter, T. H.; Oldfield, E. J. Phys. Chem. 1989, 93, 6744-6752.
4. Cocke, D. L.; Johnson, E. D.; Merril, R. P. Catal. Rev.-Sci. Eng. 1984, 26, 163-231.
5. Peri, J. B. J. Phys. Chem. 1965, 69, 211-219.
6. DeBoer, J. H.; Fortuin, J. M. H.; Lippens, B. C.; Meijs, W. H. J. Catalysis 1963, 2, 1-7.
7. Peri, J. B.; Hannan, R. B. J. Phys. Chem. 1960, 64, 1526-1530.
8. Gates, B. C.; Katzer, J. R.; Schuit, G. C. A. Chemistry of Catalytic Processes; McGraw-Hill: New York, 1979; pp 249-260.
9. Peri, J. B. J. Phys. Chem. 1965, 69, 220-230.
10. Knozinger, H.; Ratnasamy, P. Catal. Rev.-Sci. Eng. 1978, 17, 31-70.
11. Parkyns, N. D. J. Phys. Chem. 1971, 75, 526-531.
12. Peri, J. B. J. Phys. Chem. 1965, 69, 231-239.
13. Morris, H. D.; Ellis, P. D. J. Am. Chem. Soc. 1989, 111, 6045-6049.
14. Huggins, B. A.; Ellis, P. D. J. Am. Chem. Soc. 1992, 114, 2098-2108.
15. Coster, D.; Blumenfeld, A. L.; Fripiat, J. J. J. Phys. Chem. 1994, 98, 6201-6211.
16. Bronnimann, C. E.; Chuang, I.; Hawkins, B. L.; Maciel, G. E. J. Am. Chem. Soc.1987, 109, 1562-1564.
17. Bronnimann, C. E.; Zeigler, R. C.; Maciel, G. E. J. Am. Chem. Soc.1988, 110, 2023-2026.
18. Pfeifer, H. Applications of NMR Spectroscopy to Surfaces and Catalysts: Acidic Sites and Absorbed Species. In Nuclear Magnetic Resonance in Modern Technology; Maciel, G. E., Ed.; NATO ASI Series, Vol. 447; Kluwer Academic Publishers: Dordrecht, The Netherlands, 1994; p 504.
19. Gay, I. D. J. Magn. Reson. 1984, 58, 413.
20. Burum, D. P.; Rhim, W. K. J. Phys. Chem. 1979, 71, 944-956.
21. Christoph, G. G.; Corbató, C. E.; Hofmann, D. A.; Tettenhorst, R. T. Clay Clay Miner. 1979, 27, 81-86.
22. Hill, R. J. Clay Clay Miner. 1981, 29, 435-445.
23. Christensen, A. N.; Lehman, M. S.; Convert, P. Acta Chem. Scand. 1982, A36, 303-308.
24. Corbató, C. E.; Tettenhorst, R. T.; Christoph, G. G. Clay Clay Miner. 1985, 33, 71-75.
25. Haase, J.; Freude, D.; Frlich, T.; Himpel, G.; Kerbe, F.; Lippmaa, E.; Pfiefer, H.; Sarv, P.; Schfer, H.; Seiffert, B. Chem. Phys. Lett. 1989, 156, 328-332.
26. John, C. S.; Alma, N. C.; Hays, G. R. Appl. Catal. 1982, 6, 341-346.
27. Dec, S. F.; Maciel, G. E.; Fitzgerald, J. J. J. Am. Chem. Soc. 1990, 112, 9069-9077.
28. Fitzgerald, J. J.; Dec, S. F.; Hamza, A. I. Am. Mineral. 1989, 74, 1405-1408.
29. Lambert, S. F.; Millman, W. S.; Fripiat, J. J. Am. Chem. Soc. 1989, 111, 3517-3522.
30. Cruickshank, M. C.; Dent Glasser, L. S.; Barri, A. I.; Poplett, I. J. F. J. Chem. Soc., Chem. Commun. 1986, 23-24. Alemany, L. B.; Kirker, G. W. J. Am. Chem. Soc. 1986, 108, 6158-6162.
31. Cruickshank, M. C.; Dent Glasser, L. S.; Barri, A. I.; Poplett, I. J. F. J. Chem. Soc., Chem. Commun. 1986, 23-24. Alemany, L. B.; Kirker, G. W. J. Am. Chem. Soc. 1986, 108, 6158-6162.
32. Dec, S. F.; Fitzgerald, J. J.; Frye, J. S.; Shatlock, M. P.; Maciel, G. E. J. Magn. Reson. 1991, 93, 403-406.
33. Gilson, J.-P.; Edwards, G. C.; Peters, A. W.; Rajagopalan, K.; Wormsbecker, R. F.; Roberie, T. G.; Shatlock, M. P. J. Chem. Soc., Chem. Commun. 1987, 91-92.
34. Lippens, B. C.; de Boer, J. H. Acta Crystallogr. 1964, 17, 1312-1321.
35. O'Reilly, D. E. Adv. Catal. 1960,12, 31.
36. Pearson, R. M.; Schramm, C. M. Colloids Surf. 1990, 45, 323-334 and references therein.
37. Haase, J.; Oldfield, E. J. Magn. Reson. A 1993, 104, 1-9.
38. Schmitt, K. D.; Haase, J.; Oldfield, E. Zeolites 1994, 14, 89-100.
39. 1H Nuclear Magnetic Resonance in Solids by CRAMPS. In Advances in Magnetic Resonance; The Waugh Symposium, Vol. 14; Warren, S., Ed.; Academic Press; San Diego, CA, 1990; pp 125-150.
40. Fitzgerald, J. J.; Kohl, S. D.; Piedra, G.; Dec, S. F.; Maciel, G. E.; Chem. Mater. 1994, 6 (11), 1915-1917