O-Nitromandelic acid: A chiral solvating agent for the NMR determination of chiral diamine enantiomeric purity

Chirality

Volumn 9, Issue 5-6, 1997, Pages 556-562

  Haiza, Mohammed A ^a   Sanyal, Amitav ^b   Snyder, John K ^b  

^a KING SAUD UNIVERSITY   (Saudi Arabia)

^b Boston University   (United States)

Author keywords

Chiral solvating agent; Enantiomeric purity; Mandelic acid; NMR; O nitromandelic acid

Indexed keywords

DIAMINE; MANDELIC ACID DERIVATIVE; NITRO DERIVATIVE; PHENYLACETIC ACID DERIVATIVE;

ARTICLE; CHIRALITY; ENANTIOMER; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; PURIFICATION; SOLVATION;

EID: 0030982540     PISSN: 08990042     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1520-636X(1997)9:5/6<556::AID-CHIR24>3.0.CO;2-M     Document Type: Article

References (5)

1. For reviews: (a) Rinaldi, P. The determination of absolute stereochemistry using nuclear magnetic resonance techniques. Prog. NMR Spec. 15:291-352, 1982.
2. (b) Pirkle, W.H., Hoover, D.J. NMR chiral solvating agents. Top. Stereochem. 13:263-331, 1982.
3. (c) Weissman, G.R. Nuclear magnetic analysis using chiral solvating agents. Morrison, J.H., ed. In: Asymmetric Synthesis. Vol. 1. New York: Academic Press, 1983: 153-171.
4. (d) Parker, D. NMR determination of enantiomeric purity. Chem. Rev. 91:1441-1457, 1991.
5. Derome, A.E. In: Modern NMR Techniques for Chemistry Research. New York: Pergamon, 1987:58-61.