Convenient enantioselective preparation of salsolinol-1-carboxylic acid

Tetrahedron Asymmetry

Volumn 8, Issue 9, 1997, Pages 1487-1490

  Kawai, Masao ^a   Deng, Yulin ^a   Kimura, Ikuko ^a   Yamamura, Hatsuo ^a   Araki, Shuki ^a   Naoi, Makoto ^a  

^a NAGOYA INSTITUTE OF TECHNOLOGY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

1 CARBOXYSALSOLINOL; SALSOLINE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CRYSTALLIZATION; DRUG PURIFICATION; DRUG SYNTHESIS; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IN VITRO STUDY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; REACTION ANALYSIS;

EID: 0030970535     PISSN: 09574166     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0957-4166(97)00149-3     Document Type: Article

References (9)

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3. Naoi, M.; Maruyama, W.; Dostert, P.; Kohda, K.; Kaiya, T. Neurosci. Lett. 1996, 212, 1-4.
4. Deng, Y.; Maruyama, W.; Dostert, P.; Takahashi, T.; Kawai, M.; Naoi, M. J. Chromatogr. B 1995, 670, 47-54.
5. Dostert, P.; Strolin Benedetti, M.; Bellotti, V.; Allievi, C.; Dordain, G. J. Neural Transm. [GenSect] 1990, 81, 215-223.
6. Dostert, P.; Varasi, M.; Della Torre, A.; Monti, C.; Rizzo, V. Eur. J. Med. Chem. 1992, 27, 57-59.
7. Whaley, W. M.; Govindachari, T. R. Organic Reactions vol 6, John Wiley: New York, 1951; pp 151-190.
8. Matsumoto, K.; Harada, K. J. Org. Chem. 1966, 31, 1956-1958.
9. The reaction at higher temperature (85°C) resulted in lower stereoselectivity (d.e. 4%).