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II complex in a similar system was also reported: B. N. Chaudret, D. J. Cole-Hamilton, G. Wilkinson, Acta Chem. Scand. A 1978, 32, 763-769. Spectral data of a saturated hydrido - olefin rhodium(I) complex were reported in: C. Bianchini, C. Mealli, A. Meli, Sabat, M. J. Chem. Soc. Chem. Commun. 1986, 777-779.
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a) The use of saturation transfer kinetics is limited to slow exchange processes, where the relaxation times of the nuclei involved are comparable with the rate constants, see ref. [15b];
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Other examples of two similar metal complexes co-crystallizing within one crystal lattice are reported: a) D. Coucouvanis, S. Al-Ahmad, C. G. Kim, S.-M. Koo, Inorg. Chem. 1992, 31, 2996-2998; b) W. Purcell, S. S. Bason, J. G. Leipoldt, A. Roodt, H. Preston, Inorg. Chim. Acta 1995, 234, 153-156.
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2J(P-P) = 193 Hz for the proposed cis intermediate (low-temperature observation) is somewhat unusual for a square-planar system having two magnetically nonequivalent phosphorus atoms in cis positions to each other, which normally does not exceed 70 Hz. See, for example: K. Wong, G. P. Rosini, S. P. Nolan, A. S. Goldman, J. Am. Chem. Soc. 1995, 117, 5082-5088.
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It has been recently shown that, due to strong competition between dinitrogen and other incoming ligands, a catalytic cycle based on the formation of an unsaturated metal complex can be retarded by performing the reactions under a dinitrogen atmosphere: C. Bianchini, E. Farnetti, M. Graziani, M. Peruzzini, A. Polo, Organometallics 1993, 12, 3753-3761.
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