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Volumn 3, Issue 2, 1997, Pages 249-252

Edge-sharing SiN4 tetrahedra in the highly condensed nitridosilicate BaSi7N10

Author keywords

high temperature synthesis; network structures; nitridosilicates; silicon; structure elucidation

Indexed keywords


EID: 0030939233     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/chem.19970030213     Document Type: Article
Times cited : (102)

References (66)
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    • II complex in a similar system was also reported: B. N. Chaudret, D. J. Cole-Hamilton, G. Wilkinson, Acta Chem. Scand. A 1978, 32, 763-769. Spectral data of a saturated hydrido - olefin rhodium(I) complex were reported in: C. Bianchini, C. Mealli, A. Meli, Sabat, M. J. Chem. Soc. Chem. Commun. 1986, 777-779.
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    • II complex in a similar system was also reported: B. N. Chaudret, D. J. Cole-Hamilton, G. Wilkinson, Acta Chem. Scand. A 1978, 32, 763-769. Spectral data of a saturated hydrido - olefin rhodium(I) complex were reported in: C. Bianchini, C. Mealli, A. Meli, Sabat, M. J. Chem. Soc. Chem. Commun. 1986, 777-779.
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    • and references cited therein
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    • The nitrogen solubility at various temperatures can be calculated with the known solubility and ΔH of solubilization at 298.15 K, see: E. Wilhelm, R. Battino, Chem. Rev. 1973, 73, 1-9.
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    • note
    • a) The use of saturation transfer kinetics is limited to slow exchange processes, where the relaxation times of the nuclei involved are comparable with the rate constants, see ref. [15b];
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    • c) The method has been recently applied for the exchange between a hydride and an agostic hydrogen atom in a ruthenium coordination sphere: M. Ogasawara, M. Saburi, Organometallics 1994, 13, 1911-1917.
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    • Other examples of two similar metal complexes co-crystallizing within one crystal lattice are reported: a) D. Coucouvanis, S. Al-Ahmad, C. G. Kim, S.-M. Koo, Inorg. Chem. 1992, 31, 2996-2998; b) W. Purcell, S. S. Bason, J. G. Leipoldt, A. Roodt, H. Preston, Inorg. Chim. Acta 1995, 234, 153-156.
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    • Other examples of two similar metal complexes co-crystallizing within one crystal lattice are reported: a) D. Coucouvanis, S. Al-Ahmad, C. G. Kim, S.-M. Koo, Inorg. Chem. 1992, 31, 2996-2998; b) W. Purcell, S. S. Bason, J. G. Leipoldt, A. Roodt, H. Preston, Inorg. Chim. Acta 1995, 234, 153-156.
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    • 2J(P-P) = 193 Hz for the proposed cis intermediate (low-temperature observation) is somewhat unusual for a square-planar system having two magnetically nonequivalent phosphorus atoms in cis positions to each other, which normally does not exceed 70 Hz. See, for example: K. Wong, G. P. Rosini, S. P. Nolan, A. S. Goldman, J. Am. Chem. Soc. 1995, 117, 5082-5088.
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    • a) The synthesis and characterization of this "transition state-like" complex were reported: R. B. Cracknell, A. G. Orpen, J. L. Spencer, J. Chem. Soc. Chem. Commun. 1984, 326-328; b) For theoretical study see: N. Koga, S. Obara, K. Kitatira, K. Morokuma, J. Am. Chem. Soc. 1985, 107, 7109-7116.
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    • For reviews see: a) J. Chatt, J. R. Dilworth, R. L. Richards, Chem. Rev. 1978, 78, 589-625; b) A. D. Allen, R. O. Harris, B. R. Loescher, J. R. Stevens, R. N. Whiteley, Chem. Rev. 1973, 73, 11-20; c) M. Hidai, Y. Mizobe, Chem. Rev. 1995, 95, 1115-1133 and references therein.
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    • For reviews see: a) J. Chatt, J. R. Dilworth, R. L. Richards, Chem. Rev. 1978, 78, 589-625; b) A. D. Allen, R. O. Harris, B. R. Loescher, J. R. Stevens, R. N. Whiteley, Chem. Rev. 1973, 73, 11-20; c) M. Hidai, Y. Mizobe, Chem. Rev. 1995, 95, 1115-1133 and references therein.
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    • and references therein
    • For reviews see: a) J. Chatt, J. R. Dilworth, R. L. Richards, Chem. Rev. 1978, 78, 589-625; b) A. D. Allen, R. O. Harris, B. R. Loescher, J. R. Stevens, R. N. Whiteley, Chem. Rev. 1973, 73, 11-20; c) M. Hidai, Y. Mizobe, Chem. Rev. 1995, 95, 1115-1133 and references therein.
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    • It has been recently shown that, due to strong competition between dinitrogen and other incoming ligands, a catalytic cycle based on the formation of an unsaturated metal complex can be retarded by performing the reactions under a dinitrogen atmosphere: C. Bianchini, E. Farnetti, M. Graziani, M. Peruzzini, A. Polo, Organometallics 1993, 12, 3753-3761.
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    • Bianchini, C.1    Farnetti, E.2    Graziani, M.3    Peruzzini, M.4    Polo, A.5


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