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Volumn 119, Issue 12, 1997, Pages 2915-2920

15N nuclear magnetic resonance spectroscopy. Changes in nuclear Overhauser effects and T1 with viscosity

Author keywords

[No Author keywords available]

Indexed keywords

AMIDE; AMINE; HISTIDINE; PYRIDINE;

EID: 0030932089     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja963263v     Document Type: Article
Times cited : (7)

References (44)
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    • (b) Blomberg, F.; Reuterjans, H. In Biological Magnetic Resonance; Berliner, L. J., Reuben, J., Eds.; Plenum Press: New York, 1984; Vol. 5, pp 21-71.
    • (1984) Biological Magnetic Resonance , vol.5 , pp. 21-71
    • Blomberg, F.1    Reuterjans, H.2
  • 16
    • 0003884417 scopus 로고
    • Academic Press: New York
    • 1 relaxation, see: Noggle, J. H.; Shirmer, R. E. The Nuclear Overhauser Effect; Academic Press: New York, 1971. Neuhaus, D.; Williamson, M. P. The Nuclear Overhauser Effect in Structural and Conformational Analysis; VCH Publishers: New York, 1989.
    • (1971) The Nuclear Overhauser Effect
    • Noggle, J.H.1    Shirmer, R.E.2
  • 18
    • 0001484114 scopus 로고
    • and references therein
    • Although eq 5 is of heuristic value, at best it can only approximate overall spin-lattice relaxation as the sum of separate components because of cross-correlation effects: Boyd, J.; Hommel, U.; Campbell, I. D. Chem. Phys. Lett. 1990, 175, 477 and references therein.
    • (1990) Chem. Phys. Lett. , vol.175 , pp. 477
    • Boyd, J.1    Hommel, U.2    Campbell, I.D.3
  • 24
    • 0000589170 scopus 로고
    • Berliner, L. J., Reuben, J., Eds.; Plenum Press: New York
    • Deslauriers, R.; Smith, I. C. P. In Biological Magnetic Resonance; Berliner, L. J., Reuben, J., Eds.; Plenum Press: New York, 1980; Vol. 2, pp 243-344.
    • (1980) Biological Magnetic Resonance , vol.2 , pp. 243-344
    • Deslauriers, R.1    Smith, I.C.P.2
  • 25
    • 1842303019 scopus 로고
    • Ph.D. Thesis, University of Illinois
    • Bond length from neutron-diffraction studies: Keiter, E. A. Ph.D. Thesis, University of Illinois, 1986.
    • (1986)
    • Keiter, E.A.1
  • 30
    • 1842386727 scopus 로고    scopus 로고
    • note
    • 1 measurements seem consistent with a single rate constant.
  • 32
    • 0003348417 scopus 로고
    • Emsley, J. W., Feeney, J., Sutcliffe, L. H., Eds.; Pergamon Press: Oxford
    • Ebraheem, K. A. K.; Webb, G. A. In Progress in NMR Spectroscopy; Emsley, J. W., Feeney, J., Sutcliffe, L. H., Eds.; Pergamon Press: Oxford, 1977; Vol. 11, pp 149-181.
    • (1977) Progress in NMR Spectroscopy , vol.11 , pp. 149-181
    • Ebraheem, K.A.K.1    Webb, G.A.2
  • 34
    • 33644625296 scopus 로고
    • Woessner, D. E. J. Chem. Phys., 1962, 37, 647. Veeman, W. S. In Progress in NMR Spectroscopy; Emsley, J. W., Feeney, J., Sutcliffe, L. H., Eds.; Pergamon Press: Oxford, 1984; Vol. 16, p 193.
    • (1962) J. Chem. Phys. , vol.37 , pp. 647
    • Woessner, D.E.1
  • 35
    • 0345776618 scopus 로고
    • Emsley, J. W., Feeney, J., Sutcliffe, L. H., Eds.; Pergamon Press: Oxford
    • Woessner, D. E. J. Chem. Phys., 1962, 37, 647. Veeman, W. S. In Progress in NMR Spectroscopy; Emsley, J. W., Feeney, J., Sutcliffe, L. H., Eds.; Pergamon Press: Oxford, 1984; Vol. 16, p 193.
    • (1984) Progress in NMR Spectroscopy , vol.16 , pp. 193
    • Veeman, W.S.1
  • 36
    • 0001512654 scopus 로고
    • 15N chemical shifts and shielding parameters has been discussed in detail: (a) Christi, M.; Warren, J. P.; Hawkins, B. L.; Roberts, J. D. J. Am. Chem. Soc. 1973, 95, 4392. (b) Hagen, R.; Warren, J. P.; Hunter, D. H.; Roberts, J. D. J. Am. Chem. Soc. 1973, 95, 5712. (c) Roberts, J. D. Rice University Studies; (Felix Bloch and Twentieth Century Physics); Rice University, 1980; Vol. 66, No. 3, pp 147-178.
    • (1973) J. Am. Chem. Soc. , vol.95 , pp. 4392
    • Christi, M.1    Warren, J.P.2    Hawkins, B.L.3    Roberts, J.D.4
  • 37
    • 0642298511 scopus 로고
    • 15N chemical shifts and shielding parameters has been discussed in detail: (a) Christi, M.; Warren, J. P.; Hawkins, B. L.; Roberts, J. D. J. Am. Chem. Soc. 1973, 95, 4392. (b) Hagen, R.; Warren, J. P.; Hunter, D. H.; Roberts, J. D. J. Am. Chem. Soc. 1973, 95, 5712. (c) Roberts, J. D. Rice University Studies; (Felix Bloch and Twentieth Century Physics); Rice University, 1980; Vol. 66, No. 3, pp 147-178.
    • (1973) J. Am. Chem. Soc. , vol.95 , pp. 5712
    • Hagen, R.1    Warren, J.P.2    Hunter, D.H.3    Roberts, J.D.4
  • 38
    • 1842355908 scopus 로고
    • Rice University
    • 15N chemical shifts and shielding parameters has been discussed in detail: (a) Christi, M.; Warren, J. P.; Hawkins, B. L.; Roberts, J. D. J. Am. Chem. Soc. 1973, 95, 4392. (b) Hagen, R.; Warren, J. P.; Hunter, D. H.; Roberts, J. D. J. Am. Chem. Soc. 1973, 95, 5712. (c) Roberts, J. D. Rice University Studies; (Felix Bloch and Twentieth Century Physics); Rice University, 1980; Vol. 66, No. 3, pp 147-178.
    • (1980) Rice University Studies; (Felix Bloch and Twentieth Century Physics) , vol.66 , Issue.3 , pp. 147-178
    • Roberts, J.D.1
  • 42
    • 1842282878 scopus 로고    scopus 로고
    • note
    • 24
  • 43
    • 1842275096 scopus 로고    scopus 로고
    • note
    • 15N NMR spectrum then showed a clear quintet.


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