Direct lithiation of methyl isothiocyanate: A new convenient synthesis of mono-, bis- and tris(trimethylsilyl)methyl isothiocyanate

Synthesis

Volumn , Issue 4, 1997, Pages 423-424

  Brandsma, Lambert ^a   Nedolya, Nina A ^b   Verkruijsse, Hermann D ^a   Trofimov, Boris A ^b  

^a UTRECHT UNIVERSITY   (Netherlands)

^b A E FAVORSKY IRKUTSK INSTITUTE OF CHEMISTRY   (Russian Federation)

Author keywords

methyl isothiocyanata metallation of; methyl isothiocyanate trimethylsilylation of

Indexed keywords

ISOTHIOCYANIC ACID DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; REACTION ANALYSIS;

EID: 0030927127     PISSN: 00397881     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-1997-1202     Document Type: Article

References (23)

1. Hirao, T.; Yamada, A.; Ohshiro, Y.; Agawa, T. Angew. Chem. 1981, 93, 95; Angew. Chem. Intl. Ed. Engl. 1981, 20, 126.
2. Hirao, T.; Yamada, A.; Ohshiro, Y.; Agawa, T. Angew. Chem. 1981, 93, 95; Angew. Chem. Intl. Ed. Engl. 1981, 20, 126.
3. Hirao, T.; Yamada, A.; Hayashi, K.; Ohshiro, Y.; Agawa, T. Bull. Chem. Soc. Jpn. 1982, 55, 1163.
4. Hoppe, D. Angew. Chem. 1972, 84, 956; Angew. Chem. Int. Ed. Engl. 1972, 11, 933.
5. Hoppe, D. Angew. Chem. 1972, 84, 956; Angew. Chem. Int. Ed. Engl. 1972, 11, 933.
6. Hoppe, D.; Follmann, R. Chem. Ber. 1976, 109, 3047.
7. Hoppe, D.; Follmann, R. Chem. Ber. 1976, 109, 3062.
8. Hoppe, D.; Kloft M. Liebigs Ann. Chem. 1976, 1850.
9. Hoppe, I.; Hoppe, D.; Schöllkopf, U. Tetrahedron Lett. 1976, 609.
10. Nedolya, N. A.; Brandsma, L.; Trofimov, B. A., to be published.
11. Nedolya, N. A.; De Lang, R.-J.; Brandsma, L.; Trofimov, B. A. Abstracts of 11th Intern. Conf. on the Org. Synth., Amsterdam, The Netherlands, 1996, p 251.
12. Brandsma, L.; Trofimov, B.; Nedolya, N.; Mal'kina, A. Abstracts of 17th Intern. Symp. on the Org. Chem. of Sulfur, Tsukuba, Japan, 1996, p 233.
13. Brandsma, L.; Trofimov, B.; Nedolya, N.; Mal'kina, A. Abstracts of 17th Intern. Symp. on the Org. Chem. of Sulfur, Tsukuba, Japan, 1996, p 234.
14. Nedolya, N. A.; De Lang, R.-J.; Brandsma, L.; Trofimov, B. A. Zh. Org. Khim. 1996, in press.
15. Nedolya, N. A.; Brandsma, L.; Zinov'eva, V. P.; Trofimov, B. A. Zh. Org. Khim. 1996, in press.
16. Nedolya, N. A.; Brandsma, L.; Trofimov, B. A. Zh. Obshch. Khim. 1996, in press.
17. Nedolya, N. A.; Brandsma, L.; Trofimov, B. A. Dokl. Akad. Nauk. 1996, in press.
18. Nedolya, N. A.; Brandsma, L.; Trofimov, B. A. Izv. Akad. Nauk. Ser. Khim. 1996, in press.
19. Nedolya, N. A.; Brandsma L.; Trofimov, B. A. Khim. Geterotsikl. Soedin. 1996, in press.
20. Brandsma, L.; Verkruijsse, H. D. Preparative Polar Organometallic Chemistry; Springer-Verlag: Berlin, 1987; Vol. 1, p 19.
21. Noll, J. E. J. Am. Chem. Soc. 1955, 55, 3149.
22. Noll, J. E. US Patent 2762826 (1956); Chem. Abstr. 1957, 51, 5827.
23. Noll, J. E. US Patent 2762826 (1956); Chem. Abstr. 1957, 51, 5827.