Preparation and structure of a novel methano[60]fullerene containing a stable P-ylid

Tetrahedron Letters

Volumn 38, Issue 20, 1997, Pages 3529-3530

  Yamaguchi, Hiroshi ^a   Murata, Shizuaki ^a   Akasaka, Takeshi ^b   Suzuki, Toshiyasu ^c  

^a NAGOYA UNIVERSITY   (Japan)

^b NIIGATA UNIVERSITY   (Japan)

^c NEC CORPORATION   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

FULLERENE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION ANALYSIS; THIN LAYER CHROMATOGRAPHY;

EID: 0030922519     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00694-1     Document Type: Article

References (10)

1. Hirsch, A., "The Chemistry of the Fullerenes," Georg Thieme Verlag, Stuttgart, 1994, pp. 66-73 and p. 111.
2. Prato, M.; Wudl, F., in "The Chemistry of the Fullerenes," ed by Taylor, R., World Scientific Publishing, Singapore, 1995, Chap. 9.
3. 4P (1125.06): C, 89.68; H, 1.88. Found: C, 89.70; H,1.81.
4. Liou, K.-F.; Cheng, C.-H., J. Chem. Soc., Chem. Commun., 1995, 2473-2474.
5. Shu, L.-H.; Sun, W.-Q.; Zhang, D.-W.; Wu, S.-H.; Wu, H.-M.; Xu, J.-F.; Lao, X.-F., J. Chem. Soc., Chem. Commun., 1997, 79-80.
6. O'Donovan, B. F.; Hitchcock, P. B.; Meidine, M. F.; Kroto, H. W.; Taylor, R.; Walton, D. R. M., J. Chem. Soc., Chem. Commun., 1997, 81-82.
7. Caesar, J. C.; Griffiths, D. V.; Griffiths, P. A.; Tebby, J. C., J. Chem. Soc., Perkin Trans. I, 1989, 2425-2430.
8. Caesar, J. C.; Griffiths, D. V.; Griffiths, P. A.; Tebby, J. C., J. Chem. Soc., Perkin Trans. I, 1990, 2329-2334.
9. Albright, T. A.; Gordon, M. D.; Freeman, W. J.; Schweizer, E. E., J. Am. Chem. Soc., 1976, 98, 6249-6252.
10. 1H NMR spectra, and its FAB MS spectrum has no characteristic signals except m/z 720, we are now trying crystallization.