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note
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A solution of phenyl4-O-(3,6-di-O-pivaloyl-2,4-di-O-methoxymethyl-β-D-mannopyranosyl)-3, 6-di-O-benzyl-2-deoxy2-phtalimido-I-thio-β-D-glucopyranoside (52 mg) in 70% aceticacid (2 ml) was stirred at 80 °C for 3 h and evaporated under reduced pressure to give the corresponding demethoxymethylated compound, phenyl 4-O-(3,6-di-O-pivaloyl-β-D-mannopyranosyl)3,6-di-O-benzyl-2-deoxy-2- phtalimido-1-thio-β-D-glucopyranoside in quantitative yield (47 mg).
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