A preparation of haloalkylidene cyclopentanones

Tetrahedron Letters

Volumn 38, Issue 16, 1997, Pages 2919-2922

  Cornwall, Nicholas J ^a   Linehan, Shaun ^a   Weavers, Rex T ^a  

^a UNIVERSITY OF OTAGO   (New Zealand)

Author keywords

[No Author keywords available]

Indexed keywords

CYCLOPENTANONE DERIVATIVE; ORGANOBROMINE DERIVATIVE; ORGANOCHLORINE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; STEREOCHEMISTRY;

EID: 0030914644     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00503-0     Document Type: Article

References (11)

1. Haaima, G.; Lynch, M.-J.; Routledge, A.; Weavers, R.T. Tetrahedron. 1993, 49, 4229-4252.
2. Liu, Z.-X.; Shi, W.; Zhang, L.; Synthesis, 1990, 235-236 and references contained therein.
3. Giannetti, B.M.; Steffan, B.; Steglich, W.; Kupka, J.; Anke, T. Tetrahedron 1986, 42, 3587-3593.
4. Schwab, J.M.; Lin, D.C.T. J. Am. Chem. Soc. 1985, 107, 6046-6052.
5. 3 (1 ml, 25% w/v) were added to the crude product. The reaction mixture was stirred at room temperature until TLC showed no DBP. Concentration under reduced pressure was followed by work up as for A.
6. Isolated yields. All new substrates (2) and all products (3) were characterised fully.
7. Hoye, T.R.; Suriano, J.A. J. Org. Chem. 1993, 58, 1659-1660.
8. Mawson, S.D.; Routledge, A.; Weavers, R.T. Tetrahedron 1995, 51, 4665-4678.
9. PCModel for Windows, Version 1.0, Serena Software, Box 3076, Bloomington, IN 47402-3076, U.S.A. J values are calculated according to the algorithm described by Haasnoot, C.A.G.; de Leeuw, F.A.A.M.; Altona, C. Tetrahedron 1980, 36, 2783-2792.
10. Haaima, G.; Lynch, M.-J.; Routledge, A; Weavers, R.T. Tetrahedron 1991, 47, 5203-5214.
11. Haaima, G.; Mawson, S.D.; Routledge, A.; Weavers, R.T. Tetrahedron 1994, 50, 3557-3570.