Palladium-catalysed carbomethoxyvinylation and thienylation of 5-iodo(bromo)-2,4-dimethoxypyrimidine in water

Tetrahedron Letters

Volumn 38, Issue 27, 1997, Pages 4869-4872

  Basnak, Ivan ^a   Takatori, Satoshi ^a   Walker, Richard T ^a  

^a UNIVERSITY OF BIRMINGHAM   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

PALLADIUM; PYRIMIDINE DERIVATIVE;

AQUEOUS SOLUTION; ARTICLE; CATALYSIS; CHEMICAL MODIFICATION; CHEMICAL REACTION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 0030912872     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)01015-0     Document Type: Article

References (11)

1. Basnak, I.; Sun, M.; Coe, P. L. and Walker, R. T. Nucleosides & Nucleotides, 1996, 15, 121-134.
2. Whale, R. F.; Coe, P. L. and Walker, R. T. Nucleosides & Nucleotides, 1992, 11, 1425-1442.
3. Lubineau, A.; Augé, J., Queneau, Y. Synthesis, 1994, 741-760.
4. Jeffery, T. Tet.Lett., 1994,35, 3051-3054.
5. 3).
6. 2S: Calculated C = 54.04 %, H = 4.54 %, N = 12.60 %, S = 14.43; Found C = 54.29 %, H = 4.81 %, N = 12.31 %, S = 14.27 %.
7. Hillers, S.; Sartori, S.; Reiser, O. J. Amer. Chem. Soc., 1996, 118, 2087-2088.
8. Sugihara, T.; Takebayashi, M.; Kaneko, Ch. Tet. Lett. 1995, 36, 5547-5550.
9. Voight, K., Schick, U.; Meyer, F. E.; de Meijere, A. SYNLETT, 1994, 189-190.
10. Kuhlmann, B.; Arnett, E. M.; Siskin, M. J. Org. Chem. 1994, 59, 3098-3101.
11. max = 262 nm (ε = 10 200), 319 nm (ε 9 660).