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Volumn 38, Issue 21, 1997, Pages 3763-3764

Isolation of dephosphonocalyculin A from the marine sponge, discodermia calyx

Author keywords

[No Author keywords available]

Indexed keywords

CALYCULIN A; ENZYME INHIBITOR; PHOSPHOPROTEIN PHOSPHATASE 1;

EID: 0030904582     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00748-X     Document Type: Article
Times cited : (35)

References (12)
  • 4
    • 0027050190 scopus 로고
    • Total synthesis of calyculin A: Evans, D. A.; Gage, J. R.; Leighton, J. L. J. Am. Chem. Soc. 1992, 114, 9434-9453.; Tanimoto, N.; Gerritz, S. W.; Sawabe, A.; Noda, T.; Filla, S. A.; Masamune, S. Angew. Chem. 1994, 106, 674-677.
    • (1992) J. Am. Chem. Soc. , vol.114 , pp. 9434-9453
    • Evans, D.A.1    Gage, J.R.2    Leighton, J.L.3
  • 9
    • 0342664594 scopus 로고    scopus 로고
    • note
    • 3OD); δ 95.5 (C-2), 159.0 (C-3), 129.2 (C-4), 135.1 (C-5), 125.7 (C-6), 146.0 (C-7), 137.5 (C-8), 132.4 (C-9), 37.5 (C-10), 78.9 (C-11), 44.2 (C-12), 70.9 (C-13), 30.0 (C-14), 81.2 (C-15), 87.1 (C-16), 80.5 (C-17), 48.5 (C-18), 109.5 (C-19), 34.1 (C-20), 71.8 (C-21), 38.5 (C-22), 68.2 (C-23), 37.5 (C-24), 130.0 (C-25), 122.5 (C-26), 139.5 (C-27), 136.5 (C-28), 169.7 (C-29), 32.9 (C-30), 35.4 (C-31), 38.0 (C-32), 175.0 (C-33), 76.1 (C-34), 71.2 (C-35), 65.0 (C-36), 70.1 (C-37), 58.4 (C-38), 42.5 (C-39,40) 18.6 (C-41), 11.6 (C-42), 22.0 (C-43), 16.6 (C-44), 60.1 (C-45), 11.4 (C-46), 18.4 (C-47), 14.2 (C-48), 14.6 (C-49), 19.2 (C-50).
  • 10
    • 0343098911 scopus 로고    scopus 로고
    • note
    • + m/z 1049]. Subsequently, 3 was heated with a mixture of pyridine/dioxane (1:1, 0.3 mL) at 120 °C for 4 days. The reaction mixture was separated by HPLC on ODS to afforded 4 (1 mg).
  • 11
    • 0343098910 scopus 로고    scopus 로고
    • note
    • + m/z 969].


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.