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L. S. Hegedus, Transition Metals in the Synthesis of Complex Organic Molecules, University Science Books, Mill Valley, California, 1994; W. A. Herrmann, W. R. Thiel, C. Brossmer, K. Öfele, T. Priermeier, W. Scherer, J. Organomet. Chem. 1993, 461, 51; W. A. Herrmann, M. Elison, J. Fischer, C. Köcher, G. R. J. Artus, Angew. Chem. 1995, 107, 2602; Angew. Chem. Int. Ed. Engl. 1995, 34, 2371; A. de Meijere, F. E. Meyer, ibid. 1994, 106, 2473 bzw. 1994, 33, 2379; O. Reiser, ibid. 1993, 105, 576 bzw. 1993, 32, 547; B. M. Trost, D. L. Van Vranken, Chem. Rev. 1996, 96, 395; B. M. Trost, J. Dumas, M. Villa, J. Am. Chem. Soc. 1992, 114, 9836.
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L. S. Hegedus, Transition Metals in the Synthesis of Complex Organic Molecules, University Science Books, Mill Valley, California, 1994; W. A. Herrmann, W. R. Thiel, C. Brossmer, K. Öfele, T. Priermeier, W. Scherer, J. Organomet. Chem. 1993, 461, 51; W. A. Herrmann, M. Elison, J. Fischer, C. Köcher, G. R. J. Artus, Angew. Chem. 1995, 107, 2602; Angew. Chem. Int. Ed. Engl. 1995, 34, 2371; A. de Meijere, F. E. Meyer, ibid. 1994, 106, 2473 bzw. 1994, 33, 2379; O. Reiser, ibid. 1993, 105, 576 bzw. 1993, 32, 547; B. M. Trost, D. L. Van Vranken, Chem. Rev. 1996, 96, 395; B. M. Trost, J. Dumas, M. Villa, J. Am. Chem. Soc. 1992, 114, 9836.
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Trost, B.M.1
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44
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0642384292
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unpublished
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Metal complexes of octaethylcorrphycene are the object of joint studies by J. L. Sessler and E. Vogel (unpublished).
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Sessler, J.L.1
Vogel, E.2
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45
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0642292470
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note
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1/2. Structure determination with the program MolEN (Enraf-Nonius), refinement with the program SHELXL-93 (G. M. Sheldrick, University of Göttingen). Calculated on the computer systems of the Regionales Rechenzentrum der Universität zu Köln. The crystallographic data (without the structure factors) of the structure described in this publication have been deposited as supplementary publication no. CCDC-179-154 at the Cambridge Crystallographic Data Centre. Copies of the data can be requested free of charge from: The Director, CCDC, 12 Union Road, GB-Cambridge CB21EZ (fax: Int. code +(1223)336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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46
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0642384289
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note
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[15-Cyano-(Z)-octaethylisoporphycenato]palladium(II) was obtained from 10 via the oxime and its subsequent dehydration with acetic anhydride; crystals (flakes) from hexane/dichloromethane (5/1); m.p. >300°C, yield 45%.
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47
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0001244171
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T. J. Katz, P. J. Garratt, J. Am. Chem. Soc. 1963, 85, 2852; E. A. LaLancette, R. E. Benson, ibid. 1963, 85, 2853; H. E. Simmons, D. B. Chesnut, E. A. LaLancette, ibid. 1965, 87, 982.
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J. Am. Chem. Soc.
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Katz, T.J.1
Garratt, P.J.2
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48
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0003081848
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T. J. Katz, P. J. Garratt, J. Am. Chem. Soc. 1963, 85, 2852; E. A. LaLancette, R. E. Benson, ibid. 1963, 85, 2853; H. E. Simmons, D. B. Chesnut, E. A. LaLancette, ibid. 1965, 87, 982.
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LaLancette, E.A.1
Benson, R.E.2
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49
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0003089797
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T. J. Katz, P. J. Garratt, J. Am. Chem. Soc. 1963, 85, 2852; E. A. LaLancette, R. E. Benson, ibid. 1963, 85, 2853; H. E. Simmons, D. B. Chesnut, E. A. LaLancette, ibid. 1965, 87, 982.
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Simmons, H.E.1
Chesnut, D.B.2
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50
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0001563101
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-
B. Franck, A. Nonn, Angew. Chem. 1995, 107, 1941: Angew. Chem. Int. Ed. Engl. 1995, 34, 1795; for isophlorines as [4n]annulenes see M. Pohl, H. Schmickler, J. Lex, E. Vogel, ibid. 1991, 103, 1737 and 1991, 30, 1693.
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51
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33748216387
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B. Franck, A. Nonn, Angew. Chem. 1995, 107, 1941: Angew. Chem. Int. Ed. Engl. 1995, 34, 1795; for isophlorines as [4n]annulenes see M. Pohl, H. Schmickler, J. Lex, E. Vogel, ibid. 1991, 103, 1737 and 1991, 30, 1693.
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52
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0009852753
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B. Franck, A. Nonn, Angew. Chem. 1995, 107, 1941: Angew. Chem. Int. Ed. Engl. 1995, 34, 1795; for isophlorines as [4n]annulenes see M. Pohl, H. Schmickler, J. Lex, E. Vogel, ibid. 1991, 103, 1737 and 1991, 30, 1693.
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Pohl, M.1
Schmickler, H.2
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53
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33748458194
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B. Franck, A. Nonn, Angew. Chem. 1995, 107, 1941: Angew. Chem. Int. Ed. Engl. 1995, 34, 1795; for isophlorines as [4n]annulenes see M. Pohl, H. Schmickler, J. Lex, E. Vogel, ibid. 1991, 103, 1737 and 1991, 30, 1693.
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0038231759
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G. Boche, D. Martens, W. Danzer, Angen: Chem. 1969, 81, 1003; Angew. Chem. Int. Ed. Engl. 1969, 8, 984; see also G. Boche, H. Weber, A. Bieberbach, Chem. Ber. 1978, 111, 2833; G. Boche, A. Bieberbach, ibid. 1978, 111, 2850.
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Boche, G.1
Martens, D.2
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55
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0642292468
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G. Boche, D. Martens, W. Danzer, Angen: Chem. 1969, 81, 1003; Angew. Chem. Int. Ed. Engl. 1969, 8, 984; see also G. Boche, H. Weber, A. Bieberbach, Chem. Ber. 1978, 111, 2833; G. Boche, A. Bieberbach, ibid. 1978, 111, 2850.
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0011627811
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G. Boche, D. Martens, W. Danzer, Angen: Chem. 1969, 81, 1003; Angew. Chem. Int. Ed. Engl. 1969, 8, 984; see also G. Boche, H. Weber, A. Bieberbach, Chem. Ber. 1978, 111, 2833; G. Boche, A. Bieberbach, ibid. 1978, 111, 2850.
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Boche, G.1
Weber, H.2
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0038231761
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G. Boche, D. Martens, W. Danzer, Angen: Chem. 1969, 81, 1003; Angew. Chem. Int. Ed. Engl. 1969, 8, 984; see also G. Boche, H. Weber, A. Bieberbach, Chem. Ber. 1978, 111, 2833; G. Boche, A. Bieberbach, ibid. 1978, 111, 2850.
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Ed.: G. Wilkinson, Pergamon, Oxford
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C. O. Dietrich-Buchecker, J.-P. Sauvage, J.-M. Kern, J. Am. Chem. Soc. 1984, 106, 3043; D. S. C. Black in Comprehensive Coordination Chemistry, Vol. 6 (Ed.: G. Wilkinson), Pergamon, Oxford, 1987, p. 156; F. Vögtle, Supramolekulare Chemie, Teubner, Stuttgart, 1992, p. 163; J.-M. Lehn, Supramolecular Chemistry, VCH, Weinheim, 1995, p. 186; E. C. Constable, Metals and Ligand Reactivity, VCH, Weinheim, 1996, p. 138.
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Black, D.S.C.1
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Teubner, Stuttgart
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C. O. Dietrich-Buchecker, J.-P. Sauvage, J.-M. Kern, J. Am. Chem. Soc. 1984, 106, 3043; D. S. C. Black in Comprehensive Coordination Chemistry, Vol. 6 (Ed.: G. Wilkinson), Pergamon, Oxford, 1987, p. 156; F. Vögtle, Supramolekulare Chemie, Teubner, Stuttgart, 1992, p. 163; J.-M. Lehn, Supramolecular Chemistry, VCH, Weinheim, 1995, p. 186; E. C. Constable, Metals and Ligand Reactivity, VCH, Weinheim, 1996, p. 138.
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Supramolekulare Chemie
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Vögtle, F.1
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VCH, Weinheim
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C. O. Dietrich-Buchecker, J.-P. Sauvage, J.-M. Kern, J. Am. Chem. Soc. 1984, 106, 3043; D. S. C. Black in Comprehensive Coordination Chemistry, Vol. 6 (Ed.: G. Wilkinson), Pergamon, Oxford, 1987, p. 156; F. Vögtle, Supramolekulare Chemie, Teubner, Stuttgart, 1992, p. 163; J.-M. Lehn, Supramolecular Chemistry, VCH, Weinheim, 1995, p. 186; E. C. Constable, Metals and Ligand Reactivity, VCH, Weinheim, 1996, p. 138.
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Supramolecular Chemistry
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Lehn, J.-M.1
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VCH, Weinheim
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C. O. Dietrich-Buchecker, J.-P. Sauvage, J.-M. Kern, J. Am. Chem. Soc. 1984, 106, 3043; D. S. C. Black in Comprehensive Coordination Chemistry, Vol. 6 (Ed.: G. Wilkinson), Pergamon, Oxford, 1987, p. 156; F. Vögtle, Supramolekulare Chemie, Teubner, Stuttgart, 1992, p. 163; J.-M. Lehn, Supramolecular Chemistry, VCH, Weinheim, 1995, p. 186; E. C. Constable, Metals and Ligand Reactivity, VCH, Weinheim, 1996, p. 138.
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(1996)
Metals and Ligand Reactivity
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Constable, E.C.1
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63
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0642292469
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note
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3), 1.57 (br. s, 2H, NH), -1.87 (t, 1H, H-15).
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