Chiral dichlorophthalic acid amide, an improved chiral auxiliary useful for enantioresolution and X-Ray crystallographic determination of absolute stereochemistry

Enantiomer

Volumn 2, Issue 3-4, 1997, Pages 303-309

  Harada, Nobuyuki ^a   Koumura, Nagatoshi ^a   Robillard, Marc ^a  

^a TOHOKU UNIVERSITY   (Japan)

Author keywords

Absolute Stereochemistry; Chiral Auxiliary; Chiral Dichlorophthalic Acid Amide; Enantioresolution by HPLC; X ray Crystallography

Indexed keywords

ALCOHOL DERIVATIVE; LIGAND; PHTHALIC ACID ESTER; SILICA GEL;

CHIRALITY; CIRCULAR DICHROISM; CONFERENCE PAPER; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; STEREOCHEMISTRY; X RAY CRYSTALLOGRAPHY;

EID: 0030878397     PISSN: 10242430     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Conference Paper

References (10)

1. (a) Harada, N., Soutome, T., Murai, S. and Uda, H. (1993). Tetrahedron: Asymmetry, 4, 1755-1758.
2. (b) Harada, N., Hattori, T., Suzuki, T., Okamoto, A., Ono, H., Miyano, S. and Uda, H. (1993). Tetrahedron: Asymmetry, 4, 1789-1792.
3. (c) Harada, N., Soutome, T., Nehira, T., Uda, H., Oi, S., Okamura, A. and Miyano, S., (1993). J. Am. Chem. Soc., 115, 7547-7548.
4. (d) Hattori, T., Harada, N., Oi, S., Abe, H. and Miyano, S. (1995). Tetrahedron: Asymmetry, 6, 1043-1046.
5. (e) Hagiwara, H., Okamoto, T., Harada, N. and Uda, H. (1995). Tetrahedron, 51, 9891-9898.
6. See also: (a) Toyota, S., Miyasaka, T. and Oki, M. (1993). Chem. Lett., 1571-1574.
7. (b) Toyota, S., Miyasaka, T., Matsumoto, Y., Matsuo, T. and Oki, M. (1994). Bull. Chem. Soc. Jpn., 67, 1680-1693.
8. Harada, N., Nehira, T., Soutome, T., Hiyoshi, N. and Kido, R (1996). Enantiomer, 1, 35-39.
9. See also: Toyota, S., Yasutomi, A. and Oki, M. (1995). Tetrahedron Lett., 36, 6297-6300.
10. w = 0.0485 for the mirror image structure.