Speciation and quantitation of degradation products of silicones (silane/siloxane diols) by gas chromatography-mass spectrometry and stability of dimethylsilanediol

Journal of Environmental Polymer Degradation

Volumn 5, Issue 1, 1997, Pages 17-31

  Varaprath, Sudarsanan ^a   Lehmann, Robert G ^a  

^a DOW CORNING CORPORATION   (United States)

Author keywords

dimethylsilanediol; gas chromatography mass spectroscopy; high performance liquid chromatography; nuclear magnetic resonance; silanols

Indexed keywords

CHEMICAL IONIZATION MODE; DIMETHYLSILANEDIOL; ELECTRON IMPACT (EI) IONIZATION MODE; POLYDIMETHYLSILOXANE (PDMS);

DEGRADATION; ELECTRONS; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONIZATION OF SOLIDS; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE; SOLUTIONS;

SILICONES;

EID: 0030850387     PISSN: 10647546     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (16)

1. S. Varaprath, C. L. Frye, and J. L. Hamelink (1996) Environ. Toxicol. Chem. 15, 1263-1265.
2. E. J. Hobbs, M. L. Keplinger, and J. C. Calandra. (1975) Environ. Res. 10, 397-406.
3. R. J. Watts, S. Kong, C. S. Haling, L. Gearhart, C. L. Frye, and B. W. Vigon (1995) Water Res. 29, 2405-241.
4. R. G. Lehmann, S. Varaprath, and C. L. Frye (1994) Environ. Toxicol. Chem. 13, 1753-1759.
5. J. C. Carpenter, J. A. Cella, and S. B. Dorn (1995) Environ. Sei. Technol. 29, 864-868.
6. R. G. Lehmann, S. Varaprath, R. B. Annelin, and J. Arndt (1995) Environ. Toxicol. Chem. 14, 1299-1305.
7. R. G. Lehmann, S. Varaprath, and C. L. Frye (1994) Environ. Toxicol. Chem. 13, 1061-1064.
8. R. G. Lehmann, C. L. Frye, D. A. Tolle, and T. C. Zwick (1996) Water Air Soil Fallut. 87, 231-243.
9. J. C. Carpenter, T. K. Leib, C. L. Sabourin, and J. L. Spivack (1996) Manuscript in preparation.
10. J. Spivak and S. B. Dorn (1994) Environ. Sei. Technol. 28,23452352.
11. S.B. Dorn and E. M. Skelly-Frame (1994) Analyst 119(8), 16871694.
12. J. F. Hyde (1953) J. Am. Chem. Soc. 75, 2166.
13. E. P. Lebedev, V. G. Zavada, and A. D. Fedorov (1979) 7h. Obshch. Khim 49(1), 151-155 (English translation, p. 131).
14. George M. Omietenski and N. Y. Tanawanda (1967) U.S. Patent 3,309,390, March 14.
15. J. K. Klebe (1966) J. Am. Chem. Soc. 88, 3390.
16. C. Eaborn (1960) in Organosilicon Compounds, Butterworth Scientific, London, Chapter 8.