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7 alcohol resulting only from removal of the THP ether. However, longer reaction times or increased temperatures led to numerous side products.
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In practice, our Wittig reactions led to crude product with some hydrolytic opening of the valerolactone. Submission to Yamaguchi conditions (procedure: Suzuki, K.; Tomooka, K.; Katayama, E.; Matsumoto, T.; Tsuchihashi, G. J. Am. Chem. Soc. 1986, 108, 5221) recovered this material prior to purification.
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