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For biologically active polymeric or cyclic pyridinium alkaloids relevant to the bisdihydropyridine intermediate 3, see: reference 1 and (a) Davies-Coleman, M. T.; Faulkner, D. J.; Dubowchik, G. M.; Roth, G. P.; Polson, C.; Fairchild, C. J. Org. Chem. 1993, 58, 5925-5930.
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19
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85036684456
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note
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2, O °C → rt, 5 h, 94%; 2) n-BuLi, THF, -15 °C, 30 min.
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20
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0025951384
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Torisawa, Y.; Hashimoto, A.; Nakagawa, M.; Seki, H.; Hara, R.; Hino, T. Tetrahedron 1991, 47, 8067-8078.
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Seki, H.4
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Hino, T.6
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21
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85036685101
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note
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+) 452.4130, found 452.4110.
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22
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0030581344
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For total synthesis of cyclostellettamine C related to this bispyridinium macrocycle 31, see: Anan, H.; Seki, N.; Noshiro, O.; Honda, K.; Yasumuro, K.; Ozasa, T.; Fusetani, N. Tetrahedron 1996, 52, 10849-10860.
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Anan, H.1
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Fusetani, N.7
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24
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0000886036
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Lewis, R.G.3
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