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Volumn 3, Issue 9, 1997, Pages 1466-1471

Self-assembly of dinuclear CH2-bridged titanium(IV)/catecholate complexes: Influence of the counterions and of methyl substituents in the ligand

(1) Albrecht, Markus a

a UNIVERSITY OF KARLSRUHE (Germany)

Author keywords

Alkali metals; Catechol ligands; NMR spectroscopy; Supramolecular chemistry; Titanium

Indexed keywords

EID: 0030827704 PISSN: 09476539 EISSN: None Source Type: Journal
DOI: 10.1002/chem.19970030913 Document Type: Article

Times cited : (46)

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16
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- For selected recent examples see: a) P. Baxter, J.-M. Lehn, A. De Cian, J. Fischer, Angew. Chem. 1993, 105, 92; Angew. Chem. Int. Ed. Engl. 1993, 32, 69; b) P. N. W. Baxter, J.-M. Lehn, J. Fischer, M.-T. Youinou, ibid. 1994, 106, 2432 and 1994, 33, 2284; c) A. Harriman, F. Odobel, J.-P. Sauvage, J. Am. Chem. Soc. 1994, 116, 5481; d) R. W. Saalfrank, R. Burak, A. Breit, D. Stalke, R. Herbst-Irmer, J. Daub, M. Porsch, E. Bill, M. Müther, A. X. Trautwein, Angew. Chem. 1994, 106, 1697; Angew. Chem. Int. Ed. Engl. 1994, 33, 1621; e) M. Fujita, F. Ibukuro, H. Hagihara, K. Ogura, Nature 1994, 367, 720; f) K. L. Taft, C. D. Delfs, G. C. Papaefthymiou, S. Foner, D. Gatteschi, S. J. Lippard, J. Am. Chem. Soc. 1994, 116, 823; g) C. Piguet, G. Bernardinelli, A. F. Williams, B. Bocquet, Angew. Chem. 1995, 107, 618; Angew. Chem. Int. Ed. Engl. 1995, 34, 582; h) M. Fujita, D. Oguro, M. Miyazawa, H. Oka, K. Yamaguchi, K. Ogura, Nature 1995, 378, 469; i) E. C. Constable, P. Harverson, Chem. Commun. 1996, 33; j) P. J. Stang, B. Olenyuk, Angew. Chem. 1996, 108, 798; Angew. Chem. Int. Ed. Engl. 1996, 35, 732; k) T. Beissel, R. E. Powers, K. N. Raymond, Angew. Chem. 1996, 108, 1166; Angew. Chem. Int. Ed. Engl. 1996, 35, 1084.
- (1996) Chem. Commun. , pp. 33
- Constable, E.C.¹ Harverson, P.²

17
- 0342517600
- For selected recent examples see: a) P. Baxter, J.-M. Lehn, A. De Cian, J. Fischer, Angew. Chem. 1993, 105, 92; Angew. Chem. Int. Ed. Engl. 1993, 32, 69; b) P. N. W. Baxter, J.-M. Lehn, J. Fischer, M.-T. Youinou, ibid. 1994, 106, 2432 and 1994, 33, 2284; c) A. Harriman, F. Odobel, J.-P. Sauvage, J. Am. Chem. Soc. 1994, 116, 5481; d) R. W. Saalfrank, R. Burak, A. Breit, D. Stalke, R. Herbst-Irmer, J. Daub, M. Porsch, E. Bill, M. Müther, A. X. Trautwein, Angew. Chem. 1994, 106, 1697; Angew. Chem. Int. Ed. Engl. 1994, 33, 1621; e) M. Fujita, F. Ibukuro, H. Hagihara, K. Ogura, Nature 1994, 367, 720; f) K. L. Taft, C. D. Delfs, G. C. Papaefthymiou, S. Foner, D. Gatteschi, S. J. Lippard, J. Am. Chem. Soc. 1994, 116, 823; g) C. Piguet, G. Bernardinelli, A. F. Williams, B. Bocquet, Angew. Chem. 1995, 107, 618; Angew. Chem. Int. Ed. Engl. 1995, 34, 582; h) M. Fujita, D. Oguro, M. Miyazawa, H. Oka, K. Yamaguchi, K. Ogura, Nature 1995, 378, 469; i) E. C. Constable, P. Harverson, Chem. Commun. 1996, 33; j) P. J. Stang, B. Olenyuk, Angew. Chem. 1996, 108, 798; Angew. Chem. Int. Ed. Engl. 1996, 35, 732; k) T. Beissel, R. E. Powers, K. N. Raymond, Angew. Chem. 1996, 108, 1166; Angew. Chem. Int. Ed. Engl. 1996, 35, 1084.
- (1996) Angew. Chem. , vol.108 , pp. 798
- Stang, P.J.¹ Olenyuk, B.²

18
- 33748234364
- For selected recent examples see: a) P. Baxter, J.-M. Lehn, A. De Cian, J. Fischer, Angew. Chem. 1993, 105, 92; Angew. Chem. Int. Ed. Engl. 1993, 32, 69; b) P. N. W. Baxter, J.-M. Lehn, J. Fischer, M.-T. Youinou, ibid. 1994, 106, 2432 and 1994, 33, 2284; c) A. Harriman, F. Odobel, J.-P. Sauvage, J. Am. Chem. Soc. 1994, 116, 5481; d) R. W. Saalfrank, R. Burak, A. Breit, D. Stalke, R. Herbst-Irmer, J. Daub, M. Porsch, E. Bill, M. Müther, A. X. Trautwein, Angew. Chem. 1994, 106, 1697; Angew. Chem. Int. Ed. Engl. 1994, 33, 1621; e) M. Fujita, F. Ibukuro, H. Hagihara, K. Ogura, Nature 1994, 367, 720; f) K. L. Taft, C. D. Delfs, G. C. Papaefthymiou, S. Foner, D. Gatteschi, S. J. Lippard, J. Am. Chem. Soc. 1994, 116, 823; g) C. Piguet, G. Bernardinelli, A. F. Williams, B. Bocquet, Angew. Chem. 1995, 107, 618; Angew. Chem. Int. Ed. Engl. 1995, 34, 582; h) M. Fujita, D. Oguro, M. Miyazawa, H. Oka, K. Yamaguchi, K. Ogura, Nature 1995, 378, 469; i) E. C. Constable, P. Harverson, Chem. Commun. 1996, 33; j) P. J. Stang, B. Olenyuk, Angew. Chem. 1996, 108, 798; Angew. Chem. Int. Ed. Engl. 1996, 35, 732; k) T. Beissel, R. E. Powers, K. N. Raymond, Angew. Chem. 1996, 108, 1166; Angew. Chem. Int. Ed. Engl. 1996, 35, 1084.
- (1996) Angew. Chem. Int. Ed. Engl. , vol.35 , pp. 732

19
- 0000324304
- For selected recent examples see: a) P. Baxter, J.-M. Lehn, A. De Cian, J. Fischer, Angew. Chem. 1993, 105, 92; Angew. Chem. Int. Ed. Engl. 1993, 32, 69; b) P. N. W. Baxter, J.-M. Lehn, J. Fischer, M.-T. Youinou, ibid. 1994, 106, 2432 and 1994, 33, 2284; c) A. Harriman, F. Odobel, J.-P. Sauvage, J. Am. Chem. Soc. 1994, 116, 5481; d) R. W. Saalfrank, R. Burak, A. Breit, D. Stalke, R. Herbst-Irmer, J. Daub, M. Porsch, E. Bill, M. Müther, A. X. Trautwein, Angew. Chem. 1994, 106, 1697; Angew. Chem. Int. Ed. Engl. 1994, 33, 1621; e) M. Fujita, F. Ibukuro, H. Hagihara, K. Ogura, Nature 1994, 367, 720; f) K. L. Taft, C. D. Delfs, G. C. Papaefthymiou, S. Foner, D. Gatteschi, S. J. Lippard, J. Am. Chem. Soc. 1994, 116, 823; g) C. Piguet, G. Bernardinelli, A. F. Williams, B. Bocquet, Angew. Chem. 1995, 107, 618; Angew. Chem. Int. Ed. Engl. 1995, 34, 582; h) M. Fujita, D. Oguro, M. Miyazawa, H. Oka, K. Yamaguchi, K. Ogura, Nature 1995, 378, 469; i) E. C. Constable, P. Harverson, Chem. Commun. 1996, 33; j) P. J. Stang, B. Olenyuk, Angew. Chem. 1996, 108, 798; Angew. Chem. Int. Ed. Engl. 1996, 35, 732; k) T. Beissel, R. E. Powers, K. N. Raymond, Angew. Chem. 1996, 108, 1166; Angew. Chem. Int. Ed. Engl. 1996, 35, 1084.
- (1996) Angew. Chem. , vol.108 , pp. 1166
- Beissel, T.¹ Powers, R.E.² Raymond, K.N.³

20
- 0029815987
- For selected recent examples see: a) P. Baxter, J.-M. Lehn, A. De Cian, J. Fischer, Angew. Chem. 1993, 105, 92; Angew. Chem. Int. Ed. Engl. 1993, 32, 69; b) P. N. W. Baxter, J.-M. Lehn, J. Fischer, M.-T. Youinou, ibid. 1994, 106, 2432 and 1994, 33, 2284; c) A. Harriman, F. Odobel, J.-P. Sauvage, J. Am. Chem. Soc. 1994, 116, 5481; d) R. W. Saalfrank, R. Burak, A. Breit, D. Stalke, R. Herbst-Irmer, J. Daub, M. Porsch, E. Bill, M. Müther, A. X. Trautwein, Angew. Chem. 1994, 106, 1697; Angew. Chem. Int. Ed. Engl. 1994, 33, 1621; e) M. Fujita, F. Ibukuro, H. Hagihara, K. Ogura, Nature 1994, 367, 720; f) K. L. Taft, C. D. Delfs, G. C. Papaefthymiou, S. Foner, D. Gatteschi, S. J. Lippard, J. Am. Chem. Soc. 1994, 116, 823; g) C. Piguet, G. Bernardinelli, A. F. Williams, B. Bocquet, Angew. Chem. 1995, 107, 618; Angew. Chem. Int. Ed. Engl. 1995, 34, 582; h) M. Fujita, D. Oguro, M. Miyazawa, H. Oka, K. Yamaguchi, K. Ogura, Nature 1995, 378, 469; i) E. C. Constable, P. Harverson, Chem. Commun. 1996, 33; j) P. J. Stang, B. Olenyuk, Angew. Chem. 1996, 108, 798; Angew. Chem. Int. Ed. Engl. 1996, 35, 732; k) T. Beissel, R. E. Powers, K. N. Raymond, Angew. Chem. 1996, 108, 1166; Angew. Chem. Int. Ed. Engl. 1996, 35, 1084.
- (1996) Angew. Chem. Int. Ed. Engl. , vol.35 , pp. 1084

21
- 0026591881
- Reviews: a) E. C. Constable, Tetrahedron 1992, 48, 10013; b) E. C. Constable, Progr. Inorg. Chem. 1994, 42, 67; c) E. C. Constable, Chem. Ind. (London) 1994, 56; d) J.-M. Lehn, Chem. & Biol. 1994, Introductary Issue, xviii; e) A. F. Williams, Chem. Eur. J. 1997, 3, 15.
- (1992) Tetrahedron , vol.48 , pp. 10013
- Constable, E.C.¹

22
- 0026591881
- Reviews: a) E. C. Constable, Tetrahedron 1992, 48, 10013; b) E. C. Constable, Progr. Inorg. Chem. 1994, 42, 67; c) E. C. Constable, Chem. Ind. (London) 1994, 56; d) J.-M. Lehn, Chem. & Biol. 1994, Introductary Issue, xviii; e) A. F. Williams, Chem. Eur. J. 1997, 3, 15.
- (1994) Progr. Inorg. Chem. , vol.42 , pp. 67
- Constable, E.C.¹

23
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- Reviews: a) E. C. Constable, Tetrahedron 1992, 48, 10013; b) E. C. Constable, Progr. Inorg. Chem. 1994, 42, 67; c) E. C. Constable, Chem. Ind. (London) 1994, 56; d) J.-M. Lehn, Chem. & Biol. 1994, Introductary Issue, xviii; e) A. F. Williams, Chem. Eur. J. 1997, 3, 15.
- (1994) Chem. Ind. , pp. 56
- Constable, E.C.¹

24
- 50749135873
- Reviews: a) E. C. Constable, Tetrahedron 1992, 48, 10013; b) E. C. Constable, Progr. Inorg. Chem. 1994, 42, 67; c) E. C. Constable, Chem. Ind. (London) 1994, 56; d) J.-M. Lehn, Chem. & Biol. 1994, Introductary Issue, xviii; e) A. F. Williams, Chem. Eur. J. 1997, 3, 15.
- (1994) Chem. & Biol. , Issue.INTRODUCTARY ISSUE
- Lehn, J.-M.¹

25
- 0030946387
- Reviews: a) E. C. Constable, Tetrahedron 1992, 48, 10013; b) E. C. Constable, Progr. Inorg. Chem. 1994, 42, 67; c) E. C. Constable, Chem. Ind. (London) 1994, 56; d) J.-M. Lehn, Chem. & Biol. 1994, Introductary Issue, xviii; e) A. F. Williams, Chem. Eur. J. 1997, 3, 15.
- (1997) Chem. Eur. J. , vol.3 , pp. 15
- Williams, A.F.¹

26
- 33847800056
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1976) J. Am. Chem. Soc. , vol.98 , pp. 278
- Struckmeier, G.¹ Thewalt, U.² Fuhrhop, J.-H.³

27
- 0023335034
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1987) Proc. Natl. Acad. Sci. USA , vol.84 , pp. 2565
- Lehn, J.-M.¹ Rigault, A.² Siegel, J.³ Harrowfield, J.⁴ Chevrier, B.⁵ Moras, D.⁶

28
- 0000374288
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1992) New. J. Chem. , vol.16 , pp. 649
- Crane, J.D.¹ Sauvage, J.P.²

29
- 0000611145
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1993) Inorg. Chem. , vol.32 , pp. 5477
- Potts, K.T.¹ Keshavarz-K, M.² Tham, F.S.³ Raiford, K.A.G.⁴ Arana, C.⁵ Abruña, H.D.⁶

30
- 37049076133
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1994) J. Chem. Soc. Dalton Trans. , pp. 2669
- Constable, E.C.¹ Hannon, M.J.² Edwards, A.J.³ Raithby, P.R.⁴

31
- 37049066527
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1994) J. Chem. Soc. Dalton Trans. , pp. 2783
- Bilyk, A.¹ Harding, M.M.² Turner, P.³ Hambley, T.W.⁴

32
- 0028762422
- For selected examples of double-stranded helicates see: a) G. Struckmeier, U. Thewalt, J.-H. Fuhrhop, J. Am. Chem. Soc. 1976, 98, 278; b) J.-M. Lehn, A. Rigault, J. Siegel, J. Harrowfield, B. Chevrier, D. Moras, Proc. Natl. Acad. Sci. USA 1987, 84, 2565; c) J. D. Crane, J. P. Sauvage, New. J. Chem. 1992, 16, 649; d) K. T. Potts, M. Keshavarz-K, F. S. Tham, K. A. G. Raiford, C. Arana, H. D. Abruña, Inorg. Chem. 1993, 32, 5477; e) E. C. Constable, M. J. Hannon, A. J. Edwards, P. R. Raithby, J. Chem. Soc. Dalton Trans. 1994, 2669; f) A. Bilyk, M. M. Harding, P. Turner, T. W. Hambley, ibid. 1994, 2783; g) T. W. Bell, H. Jousselin, Nature 1994, 367, 441.
- (1994) Nature , vol.367 , pp. 441
- Bell, T.W.¹ Jousselin, H.²

33
- 0000955567
- For selected examples of triple-stranded helicates see: a) R. C. Scarrow, D. L. White, K. N. Raymond, J. Am. Chem. Soc. 1985, 107, 6540; b) A. F. Williams, C. Piguet, G. Bernardinelli, Angew. Chem. 1991, 103, 1530; Angew. Chem. Int. Ed. Engl. 1991, 30, 1490; c) G. Bernardinelli, C. Piguet, A. F. Williams, ibid. 1992, 104, 1626 and 1992, 31, 1622; d) K. T. Potts, C. P. Horwitz, A. Fessak, M. Keshavarz-K, K. E. Nash, P. J. Toscano, J. Am. Chem. Soc. 1993, 115, 10 444; e) D. Zurita, P. Baret, J.-L. Pierre, New. J. Chem. 1994, 18, 1143; f) S. L. Larson, S. M. Hendrickson, S. Ferrere, D. L. Derr, C. M. Elliott, J. Am. Chem. Soc. 1995, 117, 5881; g) E. J. Enemark, T. D. P. Stack, Angew. Chem. 1995, 107, 1082; Angew. Chem. Int. Ed. Engl. 1995, 34, 996.
- (1985) J. Am. Chem. Soc. , vol.107 , pp. 6540
- Scarrow, R.C.¹ White, D.L.² Raymond, K.N.³

34
- 0000894411
- For selected examples of triple-stranded helicates see: a) R. C. Scarrow, D. L. White, K. N. Raymond, J. Am. Chem. Soc. 1985, 107, 6540; b) A. F. Williams, C. Piguet, G. Bernardinelli, Angew. Chem. 1991, 103, 1530; Angew. Chem. Int. Ed. Engl. 1991, 30, 1490; c) G. Bernardinelli, C. Piguet, A. F. Williams, ibid. 1992, 104, 1626 and 1992, 31, 1622; d) K. T. Potts, C. P. Horwitz, A. Fessak, M. Keshavarz-K, K. E. Nash, P. J. Toscano, J. Am. Chem. Soc. 1993, 115, 10 444; e) D. Zurita, P. Baret, J.-L. Pierre, New. J. Chem. 1994, 18, 1143; f) S. L. Larson, S. M. Hendrickson, S. Ferrere, D. L. Derr, C. M. Elliott, J. Am. Chem. Soc. 1995, 117, 5881; g) E. J. Enemark, T. D. P. Stack, Angew. Chem. 1995, 107, 1082; Angew. Chem. Int. Ed. Engl. 1995, 34, 996.
- (1991) Angew. Chem. , vol.103 , pp. 1530
- Williams, A.F.¹ Piguet, C.² Bernardinelli, G.³

35
- 33748235965
- For selected examples of triple-stranded helicates see: a) R. C. Scarrow, D. L. White, K. N. Raymond, J. Am. Chem. Soc. 1985, 107, 6540; b) A. F. Williams, C. Piguet, G. Bernardinelli, Angew. Chem. 1991, 103, 1530; Angew. Chem. Int. Ed. Engl. 1991, 30, 1490; c) G. Bernardinelli, C. Piguet, A. F. Williams, ibid. 1992, 104, 1626 and 1992, 31, 1622; d) K. T. Potts, C. P. Horwitz, A. Fessak, M. Keshavarz-K, K. E. Nash, P. J. Toscano, J. Am. Chem. Soc. 1993, 115, 10 444; e) D. Zurita, P. Baret, J.-L. Pierre, New. J. Chem. 1994, 18, 1143; f) S. L. Larson, S. M. Hendrickson, S. Ferrere, D. L. Derr, C. M. Elliott, J. Am. Chem. Soc. 1995, 117, 5881; g) E. J. Enemark, T. D. P. Stack, Angew. Chem. 1995, 107, 1082; Angew. Chem. Int. Ed. Engl. 1995, 34, 996.
- (1991) Angew. Chem. Int. Ed. Engl. , vol.30 , pp. 1490

36
- 0007550637
- For selected examples of triple-stranded helicates see: a) R. C. Scarrow, D. L. White, K. N. Raymond, J. Am. Chem. Soc. 1985, 107, 6540; b) A. F. Williams, C. Piguet, G. Bernardinelli, Angew. Chem. 1991, 103, 1530; Angew. Chem. Int. Ed. Engl. 1991, 30, 1490; c) G. Bernardinelli, C. Piguet, A. F. Williams, ibid. 1992, 104, 1626 and 1992, 31, 1622; d) K. T. Potts, C. P. Horwitz, A. Fessak, M. Keshavarz-K, K. E. Nash, P. J. Toscano, J. Am. Chem. Soc. 1993, 115, 10 444; e) D. Zurita, P. Baret, J.-L. Pierre, New. J. Chem. 1994, 18, 1143; f) S. L. Larson, S. M. Hendrickson, S. Ferrere, D. L. Derr, C. M. Elliott, J. Am. Chem. Soc. 1995, 117, 5881; g) E. J. Enemark, T. D. P. Stack, Angew. Chem. 1995, 107, 1082; Angew. Chem. Int. Ed. Engl. 1995, 34, 996.
- (1992) Angew. Chem. Int. Ed. Engl. , vol.104 , pp. 1626
- Bernardinelli, G.¹ Piguet, C.² Williams, A.F.³

37
- 33748241810
- For selected examples of triple-stranded helicates see: a) R. C. Scarrow, D. L. White, K. N. Raymond, J. Am. Chem. Soc. 1985, 107, 6540; b) A. F. Williams, C. Piguet, G. Bernardinelli, Angew. Chem. 1991, 103, 1530; Angew. Chem. Int. Ed. Engl. 1991, 30, 1490; c) G. Bernardinelli, C. Piguet, A. F. Williams, ibid. 1992, 104, 1626 and 1992, 31, 1622; d) K. T. Potts, C. P. Horwitz, A. Fessak, M. Keshavarz-K, K. E. Nash, P. J. Toscano, J. Am. Chem. Soc. 1993, 115, 10 444; e) D. Zurita, P. Baret, J.-L. Pierre, New. J. Chem. 1994, 18, 1143; f) S. L. Larson, S. M. Hendrickson, S. Ferrere, D. L. Derr, C. M. Elliott, J. Am. Chem. Soc. 1995, 117, 5881; g) E. J. Enemark, T. D. P. Stack, Angew. Chem. 1995, 107, 1082; Angew. Chem. Int. Ed. Engl. 1995, 34, 996.
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