Amination of chiral β-silylated silyl ketene acetals by (ethoxycarbonyl)nitrene

Tetrahedron Letters

Volumn 38, Issue 32, 1997, Pages 5717-5718

  Loreto, M Antonietta ^a   Tardella, Paolo A ^a   Tedeschi, Livio ^a   Tofani, Daniela ^a  

^a SAPIENZA UNIVERSITY OF ROME   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

AMINO ACID DERIVATIVE;

AMINATION; ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; PHOTOLYSIS; REACTION ANALYSIS; STEREOCHEMISTRY;

EID: 0030810726     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)01254-9     Document Type: Article

References (8)

1. Cipollone, A.; Loreto, M.A.; Pellacani, L.; Tardella, P.A. J. Org. Chem. 1987, 52, 2584-2586.
2. Fioravanti, S.; Loreto, M.A.; Pellacani, L.; Sabbatini, F.; Tardella, P.A. Tetrahedron: Asymmetry 1994, 5, 473-478.
3. Fleming, I.; Kilburn, J.D. J. Chem. Soc., Perkin Trans, 1 1992, 3295-3302.
4. α,β-Unsaturated esters not commercially available were synthesised by Horner-Emmons reaction of the corresponding aldehydes: Boutagy, J.; Thomas, R. Chem. Rev. 1974, 74, 87-99.
5. Crump, R.A.N.C.; Fleming, I.; Hill, J.H.M.; Parker, D.; Reddy, N.L.; Waterson, D.J. J. Chem. Soc., Perkin Trans. 1 1992, 3277-3294. The synthesis of 1d and 1e carrying bulky substituent were run at -40°C and -20°C respectively.
6. Lwowski, W.; Mattingly, T.W. J. Am. Chem. Soc. 1965, 87, 947-958.
7. C-O);.
8. Fleming, I.; Henning, R.; Parker, D.C.; Plaut, H.E.; Sanderson, P.E.J. J. Chem. Soc., Perkin Trans. 1 1995, 317-337.