Syntheses, structures, and reactions of the first rotational isomers of stable selenobenzaldehydes, 2,4,6-tris[bis(trimethylsilyl)methyl]selenobenzaldehydes, and their η1-tungsten complexes

Tetrahedron

Volumn 53, Issue 36, 1997, Pages 12167-12182

  Takeda, Nobuhiro ^a   Tokitoh, Norihiro ^a   Okazaki, Renji ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

METAL COMPLEX; ORGANOSELENIUM DERIVATIVE; TUNGSTEN DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; NUCLEAR OVERHAUSER EFFECT; PRIORITY JOURNAL; REACTION ANALYSIS; X RAY CRYSTALLOGRAPHY;

STAPHYLOCOCCUS PHAGE 3A;

EID: 0030801194     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4020(97)00550-4     Document Type: Article

References (100)

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33. Okazaki, R.; Ishii, A.; Inamoto, N. J. Chem. Soc., Chem. Commun. 1986, 71; Kirby, G. W.; Tretheway, A. N. J. Chem. Soc., Chem. Commun. 1986, 1152; Nakayama, J.; Akimoto, K.; Niijima, J.; Hoshino, M. Tetrahedron Lett. 1987, 28, 4423; Okuma, K.; Sakata, Y.; Tachibana, Y.; Honda, T.; Ohta, H. Tetrahedron Lett. 1987, 28, 6649; Erker, G.; Hock, R.; Notle, R. J. Am. Chem. Soc. 1988, 110, 624; Segi, M.; Nakajima, S.; Suga, S.; Murai, S.; Ryu, S.; Ogawa, A.; Sonoda, N. J. Am. Chem. Soc. 1988, 110, 1976; Meinke, P. T.; Krafft, G. A. J. Am. Chem. Soc. 1988, 110, 8671; Nakayama, J.; Akimoto, K.; Hoshino, M. J. Phys. Org. Chem. 1988, 1, 53; Okuma, K.; Komiya, Y.; Kaneko, I.; Tachibana, Y.; Iwata, E.; Ohta, H. Bull. Chem. Soc. Jpn. 1990, 63, 1653; Shimada, K.; Jin, N.; Fujimura, M.; Nagano, Y.; Kudoh, E.; Takikawa, Y. Chem. Lett. 1992, 1843, and references therein.
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63. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
64. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
65. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
66. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
67. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
68. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
69. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
70. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
71. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
72. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
73. Morita, K.; Kobayashi, S. Chem. Pharm. Bull. 1967, 15, 988; Francis, E.; Rahman, R.; Safe, S.; Taylor, A. J. Chem. Soc., Perkin Trans 1. 1972, 470; Krespan, C. G.; Brasen, W. R. J. Org. Chem. 1962, 27, 3995; Chenard, B. L.; Harlow, R. L.; Johnson, A. L.; Vladuchick, S. A. J. Am. Chem. Soc. 1985, 107, 3871; Bartlett, P. D.; Ghosh, T. J. Org. Chem. 1987, 52, 4937; Sato, R.; Kimura, T.; Goto, T.; Saito, M.; Kabuto, C. Tetrahedron Lett. 1989, 30, 3453; Tokitoh, N.; Okano, Y.; Ando, W.; Goto, M.; Maki, H. Tetrahedron Lett. 1990, 31, 5323; Steudel, R.; Kustos, M. Phosphorus, Sulfur, and Silicon 1991, 62, 127; Davidson, B. S.; Molinski, T. F.; Barrows, L. R.; Ireland, C. H. J. Am. Chem. Soc. 1991, 113, 4709; Behar, V.; Danishefsky, S. J. Am. Chem. Soc. 1993, 115, 7017; Fehér, F.; Glinka, K. Z. Naturforsh. 1979, 34b, 1031; Steudel, R.; Strauss, R.; Jensen, D. Chem. -Ztg. 1985, 109, 349; Lutz, W.; Pilling, T.; Rihs, G.; Waespe, H. R.; Winkler, T. Tetrahedron Lett. 1990, 31, 5457; Ishii, A.; Akasaka, T.; Maruta, T.; Nakayama, J.; Hoshino, M.; Shiro, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 777; Ishii, A.; Yinan, J.; Sugihara, Y.; Nakarama, J. J. Chem. Soc., Chem. Commun. 1996, 2681 and references therein.
74. 5 has been used in the syntheses of organic selenium compounds as a selenium source; Giolando, D. M.; Paravassiliou, M.; Pickardt, J.; Rauchfuss, T. B.; Steudel, R. Inorg. Chem. 1988, 27, 2596; Steudel, R.; Paravassiliou, M.; Strauss, E.-M.; Laitinen, R. Angew. Chem., Int. Ed. Engl. 1986, 25, 99; Bolinger, C. M.; Hoots, J. E.; Rauchfuss, T. B. Organometallics 1982, 1, 223; Bolinger, C. M.; Rauchfuss, T. B. Inorg. Chem. 1982, 27, 3947 and references therein.
75. 5 has been used in the syntheses of organic selenium compounds as a selenium source; Giolando, D. M.; Paravassiliou, M.; Pickardt, J.; Rauchfuss, T. B.; Steudel, R. Inorg. Chem. 1988, 27, 2596; Steudel, R.; Paravassiliou, M.; Strauss, E.-M.; Laitinen, R. Angew. Chem., Int. Ed. Engl. 1986, 25, 99; Bolinger, C. M.; Hoots, J. E.; Rauchfuss, T. B. Organometallics 1982, 1, 223; Bolinger, C. M.; Rauchfuss, T. B. Inorg. Chem. 1982, 27, 3947 and references therein.
76. 5 has been used in the syntheses of organic selenium compounds as a selenium source; Giolando, D. M.; Paravassiliou, M.; Pickardt, J.; Rauchfuss, T. B.; Steudel, R. Inorg. Chem. 1988, 27, 2596; Steudel, R.; Paravassiliou, M.; Strauss, E.-M.; Laitinen, R. Angew. Chem., Int. Ed. Engl. 1986, 25, 99; Bolinger, C. M.; Hoots, J. E.; Rauchfuss, T. B. Organometallics 1982, 1, 223; Bolinger, C. M.; Rauchfuss, T. B. Inorg. Chem. 1982, 27, 3947 and references therein.
77. 5 has been used in the syntheses of organic selenium compounds as a selenium source; Giolando, D. M.; Paravassiliou, M.; Pickardt, J.; Rauchfuss, T. B.; Steudel, R. Inorg. Chem. 1988, 27, 2596; Steudel, R.; Paravassiliou, M.; Strauss, E.-M.; Laitinen, R. Angew. Chem., Int. Ed. Engl. 1986, 25, 99; Bolinger, C. M.; Hoots, J. E.; Rauchfuss, T. B. Organometallics 1982, 1, 223; Bolinger, C. M.; Rauchfuss, T. B. Inorg. Chem. 1982, 27, 3947 and references therein.
78. 5 has been used in the syntheses of organic selenium compounds as a selenium source; Giolando, D. M.; Paravassiliou, M.; Pickardt, J.; Rauchfuss, T. B.; Steudel, R. Inorg. Chem. 1988, 27, 2596; Steudel, R.; Paravassiliou, M.; Strauss, E.-M.; Laitinen, R. Angew. Chem., Int. Ed. Engl. 1986, 25, 99; Bolinger, C. M.; Hoots, J. E.; Rauchfuss, T. B. Organometallics 1982, 1, 223; Bolinger, C. M.; Rauchfuss, T. B. Inorg. Chem. 1982, 21, 3947 and references therein.
79. 8-10 because of the absence of the signals for its rotamer in the NMR spectra, although experimental confirmation of the structures was not performed.
80. Erker, G.; Hock, R.; Krüger, C.; Werner, S.; Klärner, F. G.; Artschwager-Perl, U. Angew. Chem., Int. Ed. Engl. 1990, 29, 1067; Wilker, S.; Erker, G. J. Am. Chem. Soc. 1995, 117, 10922.
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