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note
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41 The quinones 16 and 19 were purchased from Aldrich and sublimated before use. α-Lapachone (20) and β-lapachone (21) were a kind gift from Prof. A. Ventura (NPPN/UFRJ, Rio de Janeiro, Brazil). All the new quinones show analytical and spectral (IR, NMR, MS) data in full accordance with the indicated structures and details of their synthesis will be published elsewhere.
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0342570112
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34
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0342570113
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note
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-1 was calculated for each flat-bottomed test tube (4 mL, 56 x 13 mm); control experiments with the diluent and GV were run in parallel. After incubation at 4 °C by 24 h, the suspensions were examined microscopically. Each experiment was repeated 3 times, with duplicate tubes.
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