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0343758427
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note
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Attempts to employ normal-phase preparative HPLC for separation of cyclic oligosaccharides larger than the octamer were unsuccessful.
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60
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0342453118
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note
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4-catalyzed poly-condensation leading to acylated (1 → 4)-α-D-mannan and α-L-rhamnan respectively. See ref. [18].
-
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62
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0342453117
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note
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Each of the achiral molecules 20-24 and 28 incorporates 5n chiral centres, where n is the number of monosaccharide constituents.
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The use of a number of mass spectrometric techniques for the characterization of CD inclusion complexes has been reported over the years. See: L. Szente, in Comprehensive Supramolecular Chemistry, Vol. 3 (Eds.: J. Szejtli, T. Osa), Elsevier, Oxford, 1996, pp. 253-278, and references cited therein.
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0343758425
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note
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Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100129. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: int. code +(1223)336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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