'Fullerene fragments:' Synthesis and crystall structure determination of 1,4,5,6,7,10,11,12-octamethylindeno[1,2,3-cd]fluoranthene

Tetrahedron Letters

Volumn 38, Issue 29, 1997, Pages 5095-5098

  Sygula, Andrzej ^a   Fronczek, Frank R ^a   Rabideau, Peter W ^a  

^a LOUISIANA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AROMATIC HYDROCARBON; FULLERENE DERIVATIVE;

ARTICLE; CONFORMATION; CRYSTAL STRUCTURE; DRUG SYNTHESIS; REACTION ANALYSIS; STEREOSPECIFICITY; X RAY CRYSTALLOGRAPHY;

EID: 0030788364     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)01135-0     Document Type: Article

References (10)

1. (a) Rabideau, P. W.; Sygula, A. In Advances in Theoretically Interesting Molecules; Thummel, R. P., Ed.; Jai Press Inc.: Greenwich, CT, 1995; Vol. 3, pp. 1-36.
2. (b) Rabideau, P. W.; Sygula, A. Acc. Chem. Res., 1996, 29, 235-242.
3. 13C NMR, and by mass spectral analysis.
4. Buu-Hoi; Cagniant, P. Revue. Scientifique 1942, 80, 130-133.
5. Borchardt, A.; Hardcastle, K.; Gantzel, P.; Siegel, J. S. Tetrahedron Lett. 1993, 34, 273-276.
6. Dozen, Y.; Hatta, M. Bull. Chem. Soc. Jpn., 1975, 48, 2842-2847.
7. 3) 21.50, 24.46, 130.51, 131.03, 131.48, 133.90, 136.91, 143.07. MS (m/e, rel. intensity) 389(32), 388(100), 373(22), 194(64), 186(23), 179(47), 172(16), 171(30), 170(31), 169(29), 164(30), 163(77), 162(12), 157(41), 150(19).
8. c=1.290, MoKα radiation, T=100K, R=0.096, Rw=0.065 for 4272 observed data having 1<θ<32° and I>1σ(I).
9. (a) Dewar, M. J. S. ; Zoebisch, E. G.; Healy, E. F.; Stewart, J. J. P. J. Am. Chem. Soc. 1985, 107, 3902-3909.
10. (b) Stewart, J. J. P. MOPAC, QCPE Program No. 455 (Version 6.0).