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The authors thank Dr. John Minter at the Eastman Kodak Research Laboratories and Dr. Michael Bench in the Department of Chemical Engineering, University of Minnesota, for the help with Cryo-TEM studies
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The transition dipole associated with the A band lies along the long axis of the azobenzene while that for the B band is perpendicular to the long axis. The head-to-head alignment of the dipoles for the A band in the proposed trimeric structure corresponds to a head-to-tail arrangement of the dipoles of the B band, which should lead to a red shift in the latter transition.
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8EPC is estimated from light scattering to be ∼200 nm. Although, as a reviewer has pointed out, this may seem inconsistent with extrusion of cis through a 100 nm membrane, the light-scattering data are generally somewhat skewed toward larger sizes since big particles make larger contribution. Additionally, the measurements in Table 3 were made at times following irradiaition during which some thermal isomerization to trans had occurred.
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No attempt has been made to determine a quantitative (e.g., quantum yield) relationship between absorbed light intensity and CF release
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No attempt has been made to determine a quantitative (e.g., quantum yield) relationship between absorbed light intensity and CF release.
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53 with similar intermolecular interaction to those in the trimer "unit aggregate". This, of course, does not explain the observation that the limiting spectral shifts appear, in most cases, with the formation of the unit aggregate. At present, we have no satisfactory explanation for this.
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An alternative explanation is that the difference in absorption spectral shift is attributed to the different orientation of azobenzene chromophores in the aggregates.
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