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note
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2) = 0.0980 for 3289 unique data with I > 2σ(I). Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100423. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: int. code + (1223) 336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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